• Title/Summary/Keyword: Surface Profiling

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Growth of Polycrystalline 3C-SiC Thin Films using HMDS Single Precursor (HMDS 단일 전구체를 이용한 다결정 3C-SiC 박막 성장)

  • Chug, Gwiy-Sang;Kim, Kang-San;Han, Ki-Bong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.2
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    • pp.156-161
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    • 2007
  • This paper describes the characteristics of polycrystalline ${\beta}$ or 3C (cubic)-SiC (silicon carbide) thin films heteroepitaxailly grown on Si wafers with thermal oxide. In this work, the poly 3C-SiC film was deposited by APCVD (atmospheric pressure chemical vapor deposition) method using HMDS (hexamethyildisilane: $Si_{2}(CH_{3}_{6})$ single precursor. The deposition was performed under various conditions to determine the optimized growth conditions. The crystallinity of the 3C-SiC thin film was analyzed by XPS (X-ray photoelectron spectroscopy), XRD (X-ray diffraction) and FT-IR (fourier transform-infrared spectometers), respectively. The surface morphology was also observed by AFM (atomic force microscopy) and voids or dislocations between SiC and $SiO_{2}$ were measured by SEM (scanning electron microscope). Finally, depth profiling was invesigated by GDS (glow discharge spectrometer) for component ratios analysis of Si and C according to the grown 3C-SiC film thickness. From these results, the grown poly 3C-SiC thin film is very good crystalline quality, surface like mirror and low defect. Therfore, the poly 3C-SiC thin film is suitable for extreme environment, Bio and RF MEMS applications in conjunction with Si micromaching.

Pulsed DC Bias Effects on Substrate in TiNx Thin Film Deposition by Reactive RF Magnetron Sputtering at Room Temperature (반응성 RF 마그네트론 스퍼터링에 의한 TiNx 상온 성막에 있어서 기판 상의 펄스상 직류 바이어스 인가 효과)

  • Kim, Seiki
    • Journal of the Korean institute of surface engineering
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    • v.52 no.6
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    • pp.342-349
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    • 2019
  • Titanium nitride(TiN) thin films have been deposited on PEN(Polyethylene naphthalate) substrate by reactive RF(13.56 MHz) magnetron sputtering in a 25% N2/Ar mixed gas atmosphere. The pulsed DC bias voltage of -50V on substrates was applied with a frequency of 350 kHz, and duty ratio of 40%(1.1 ㎲). The effects of pulsed DC substrate bias voltage on the crystallinity, color, electrical properties of TiNx films have been investigated using XRD, SEM, XPS and measurement of the electrical properties such as electrical conductivity, carrier concentration, mobility. The deposition rates of TiNx films was decreased with application of the pulsed DC substrate bias voltage. The TiNx films deposited without and with pulsed bias of -50V to substrate exhibits gray and gold colors, respectively. XPS depth profiling revealed that the introduction of the substrate bias voltage resulted in decreasing oxygen concentration in TiNx films, and increasing the electrical conductivities, carrier concentration, and mobility to about 10 times, 5 times, and 2 times degree, respectively.

Assessment for Application of Horizontal Component Wave applied to Surface Wave Method for Ground stiffness Investigation (표면파기법을 이용한 지반강성평가시 수평성분파의 적용성 평가)

  • 이일화;조성호
    • Proceedings of the Korean Geotechical Society Conference
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    • 2003.03a
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    • pp.697-700
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    • 2003
  • The SASW method is a promising and effective way of profiling ground stiffness nondestructively. This method has been successfully applied to many geotechnical sites, but significant lateral variability, embedded obstacles, and pavement lead to the low reliability. To improve these problems, the horizontal wave component has been introduced to improve the reliability of the stiffness profile determined by the SASW method. To understand dispersion character of the horizontal component wave propagation in artificial profiles, FEM analysis had been performed. Used models are homogeneous half-space and two layered half- spaced layers.

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Observation on Neck Form of Young Japanese Women for Clothing Design I - A Method for Approximate Development of 3-D Measure Valuses - (의복설계를 위한 성인여성의 경부형태의 관찰 I - 도형의 자동제도를 위한 3차원 계측지의 처리방법 -)

  • 최영옥
    • Journal of the Korean Society of Costume
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    • v.31
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    • pp.89-99
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    • 1997
  • In order to know what sorts of features of neck fore may be required to make plans for tight fitting collars the neck form of young japanese women were measured three deme-nsionally using. GRASP(Grating projection System for Profiling) and plaster torso. The following results were obtained: 1. We could be known the features of neck form for tight fitting collars by using both plaster torso method and GRASP method. 2. By the BASIC language in NEC computer and EXCEL package program in macin-TOSHI computer it became possible to draft a numble of neck surface automatically there-fore we got analysis of a mass of subjects.

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A Study on the Cold Rolling for the Embossing of Metal Sheet (박판 금속의 엠보싱을 위한 냉간 성형 연구)

  • Lee, K.S.;Kim, S.W.;Shin, M.C.;Lee, J.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.397-400
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    • 2009
  • When the metal sheet is subjected to the housing surface for fitting and insulating from harsh surroundings like fluid ingression or hot steam, both strength and formability have to be equally considered. In this regard, the main aim of this study is to design an apparatus of cost-effectively producing flexible fluted band with increasing the formability of embossed stainless steel sheet, which is utilized as a thermal insulation metal for housing ship engine exhauster. Designed to fabricate a maximum sheet width of 700 mm, this new apparatus consists of upper roll made of hard urethane and the female-etched lower roll made of SKD11, have a producing capacity up to 1-meter homogeneously embossed sheet for just 60 seconds. This machine is devised for the maximum operating efficiency from original sheet handling to machine setting. The embossing properties are characterized by 3-D profiling. After embossing plain metal sheet, both yield strength and elongation properties are improved simultaneously, indicating the effectiveness of the newly designed apparatus.

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Development of Multi-DOF Nano Aligner System for CNT-Tip (탄소 나노 튜브-팁 제작을 위한 다자유도 나노 정렬 시스템 개발)

  • Kang, Gyung-Soo;Lee, Jun-Sok;Choi, Jai-Seong;Kwak, Yoon-Keun;Kim, Soo-Hyun
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.923-928
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    • 2004
  • AFM tip has been used for surface profiling with a fine resolution, but there is a barrier to improve its performance because of the low aspect ratio. Many researchers have solved this problem with attaching carbon nanotube (CNT) to Si-tip. In this paper, we proposed the aligner system that composed of dual type stage system, and these stages could attach a carbon nanotube to tungsten-tip in vacuum condition. We used tungsten tip instead of Si-tip because of its conductivity. The aligner system proposed in this paper has 10 degree-of-freedom that 3 in the first stage and 7 in the second stage. With picomotors and piezotube, the first stage has the resolution about several tens of nm and the second stage has a resolution about a nm. We experimented on characterization of Nano Aligner System and operated picomotors in SEM environment.

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Stress Analysis on the Cam-Roller Contact Parts in a Marine Diesel Engine (박용 디젤기관 캠-롤러 접촉부의 응력 해석)

  • 구영필;김형자;임우조;조용주
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2001.05a
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    • pp.168-172
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    • 2001
  • The subsurface stress field beneath the roller due to the lubricant film pressure acting on the roller surface has been calculated. Main purpose of this study in view of engineering is to prove the validity of the numerical profile roller presented by Koo et al who obtained the lubricant film pressure by elastohydrodynamic lubrication analysis on the cam-roller mechanism. The stress field for the numerical profile roller was compared with the one for the existing dub-off profile roller.

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Biological Effects of Ceramic-coating on Titanium

  • Sohn, Sung-Hwa;Lee, Jae-Bum;Kim, Ki-Nam;Kim, Hye-Won;Kim, In-Kyoung;Lee, Seung-Ho;Seo, Sang-Hui;Kim, Yu-Ri;Lee, Seung-Min;Shin, Sang-Wan;Ryu, Jae-Jun;Kim, Meyoung-Kon
    • Molecular & Cellular Toxicology
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    • v.2 no.2
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    • pp.97-105
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    • 2006
  • Several features of the implant surface, such as roughness, topography, and composition play a relevant role in implant integration with bone. This study was conducted in order to determine the effects of ceramic-coatings on Ti surfaces on the biological responses of a human osteoblast-like cell line (MG63). MG63 cells were cultured on Zr (Zrconium-coated surface), Nb (Niobium-coated surface), and control (Uncoated Titanium) Ti. The morphology of these cells was assessed by SEM. The cDNAs prepared from the total RNAs of the MG63 were hybridized into a human cDNA microarray (1,152 elements). The appearances of the surfaces observed by SEM were different on each of the three dental substrate types. MG63 cells cultured on Zr, Nb and control exhibited cell-matrix interactions. In the expression of several genes were up-, and down-regulated on the different surfaces. The attachment and expression of key osteogenic regulatory genes were enhanced by the surface morphology of the dental materials used.

Nano Bio Imaging for NT and BT

  • Moon, DaeWon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.51.2-51.2
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    • 2015
  • Understanding interfacial phenomena has been one of the main research issues not only in semiconductors but only in life sciences. I have been trying to meet the atomic scale surface and interface analysis challenges from semiconductor industries and furthermore to extend the application scope to biomedical areas. Optical imaing has been most widely and successfully used for biomedical imaging but complementary ion beam imaging techniques based on mass spectrometry and ion scattering can provide more detailed molecular specific and nanoscale information In this presentation, I will review the 27 years history of medium energy ion scattering (MEIS) development at KRISS and DGIST for nanoanalysis. A electrostatic MEIS system constructed at KRISS after the FOM, Netherland design had been successfully applied for the gate oxide analysis and quantitative surface analysis. Recenlty, we developed time-of-flight (TOF) MEIS system, for the first time in the world. With TOF-MEIS, we reported quantitative compositional profiling with single atomic layer resolution for 0.5~3 nm CdSe/ZnS conjugated QDs and ultra shallow junctions and FINFET's of As implanted Si. With this new TOF-MEIS nano analysis technique, details of nano-structured materials could be measured quantitatively. Progresses in TOF-MEIS analysis in various nano & bio technology will be discussed. For last 10 years, I have been trying to develop multimodal nanobio imaging techniques for cardiovascular and brain tissues. Firstly, in atherosclerotic plaque imaging, using, coherent anti-stokes raman scattering (CARS) and time-of-flight secondary ion mass spectrometry (TOF-SIMS) multimodal analysis showed that increased cholesterol palmitate may contribute to the formation of a necrotic core by increasing cell death. Secondly, surface plasmon resonance imaging ellipsometry (SPRIE) was developed for cell biointerface imaging of cell adhesion, migration, and infiltration dynamics for HUVEC, CASMC, and T cells. Thirdly, we developed an ambient mass spectrometric imaging system for live cells and tissues. Preliminary results on mouse brain hippocampus and hypotahlamus will be presented. In conclusions, multimodal optical and mass spectrometric imaging privides overall structural and morphological information with complementary molecular specific information, which can be a useful methodology for biomedical studies. Future challenges in optical and mass spectrometric imaging for new biomedical applications will be discussed.

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Gene Expression of Osteosarcoma Cells on Various Coated Titanium Materials

  • Sohn, Sung-Hwa;Lee, Jae-Bun;Kim, Ki-Nam;Kim, In-Kyoung;Lee, Seung-Ho;Kim, Hye-Won;Seo, Sang-Hui;Kim, Yu-Ri;Shin, Sang-Wan;Ryu, Jae-Jun;Kim, Meyoung-Kon
    • Molecular & Cellular Toxicology
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    • v.3 no.1
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    • pp.36-45
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    • 2007
  • Several features of the implant surface, such as topography, roughness, and composition play a relevant role in implant integration with bone. This study was conducted in order to determine the effects of different-coatings on Ti surfaces on the biological responses of a human osteoblast-like cell line (MG63). MG63 cells were cultured on HA (Hydroxyapatite coating on Titanium), Ano (HA coating on anodized surface Titanium), Zr (zirconium-coating on Titanium), and control (non-coating on Titanium). The morphology of these cells was assessed by SEM. The cDNAs prepared from the total RNAs of the MG63 were hybridized into a human cDNA microarray (1,152 elements). The appearances of the surfaces observed by SEM were different on each of the three dental substrate types. MG63 cells cultured on HA, Ano, Zr, and control exhibited cell-matrix interactions. In the expression of several genes were up-, and down-regulated on the different surfaces. The attachment and expression of key osteogenic regulatory genes were enhanced by the surface morphology of the dental materials used.