• Title/Summary/Keyword: Surface Hardness

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Characterization of Thin Film Materials by Nanoindentation and Scanning Probe Microscopy (나노인덴테이션과 주사탐침현미경을 이용한 박막 재료의 특성평가)

  • Kim, Bong-seob;Yun, Jon-do;Kim, Jong-kuk
    • Korean Journal of Materials Research
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    • v.13 no.9
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    • pp.606-612
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    • 2003
  • Surface and mechanical properties of thin films with submicron thickness was characterized by nanoindentation with Berkovich and Vickers tips, and scanning probe microscopy. Nanoindention was made in a depth range of 15 to 200 nm from the surface by applying tiny force in a range from 150 to $9,000 \mu$N. Stiffness, contact area, hardness, and elastic modulus were determined from the force-displacement curve obtained. Reliability was first tested by using fused quartz, a standard sample. Elastic modulus and hardness values of fused quartz measured were the same as those reported in the literature within two percent of error. Mechanical properties of ITO thin film were characterized in a depth range of 15∼200nm. As indentation depth increased, elastic modulus and hardness decreased by substrate effect. Ion beam deposited DLC thin films were indented in a depth range of 40∼50 nm. The results showed that the DLC thin film using benzene and bias voltage 0∼-50 V has elastic modulus and hardness value of 132 and 18 GPa respectively. Pure DLC thin films showed roughnesses lower than 0.25 nm, but silicon-added DLC thin films showed much higher roughness values, and the wavy surface morphology.

A Characteristics of Thick and Hard Al-Cu Alloy by Overlaying Welding Process (오버레이 용접법에 의한 Al-Cu 합금 경화후막의 특성)

  • 박정식;양변모;박경재
    • Journal of Welding and Joining
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    • v.14 no.4
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    • pp.53-61
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    • 1996
  • It was attempted to improve the wear resistance of Al alloy under the load condition by making a formation of the thicker surface hardening alloy layers. The thicker surface hardening alloy layers were formed on 6061 Al alloys overlayed by MIG and TIG welding process with Cu powders feeding. The characteristics of hardening and wear resistance have been investigated in relation to the microstructures of alloyed layers, with a selection of optimum alloying conditions for formation of overlaying layer. The results obtained were summarized as follows With increasing feeding rate of Cu powders by MIG welding, the hardness and specific wear of the overlay weld alloys were increased. It is considered that these high hardness and specific wear of overlay weld alloys were due to the formation of Θ($Al_2Cu$) phases. With increasing feeding rate of Cu powders by TIG welding, the hardness and specific wear of the overlay weld alloys were increased in feeding rates 12 and 18g/min. However, the hardness and specific wear were decreased in the powder feeding rate 38g/min. It is considered that considered that decrease of hardness and specific wear in the powder feeding rate 38g/min due to formation of ${\gamma}$($Al_4Cu_9$) phases.

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Heat Treatment Using a Laser Beam or an Electron Beam (레이저 및 전자빔을 이용한 표면 열처리)

  • 김홍준;최우천;권영각
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.19 no.2
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    • pp.427-432
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    • 1995
  • Surface heat treatment using a laser beam or an electron beam is studied through numerical analyses and experiments. For the surface heat treatment process, a theoretical model is developed to predict the effects of laser beam power, travel speed and properties of a workpiece on the depth and width of the heat affected zone(HAZ). The shape of HAZ and the hardness of heat-treated surface are experimentally obtained using an electron beam. Three materials(SS41, S45C and S55C) are selected as workpiece materials. The hardness of HAZ is increased up to 3 times for materials of a low carbon content. The results of the numerical analysis are compared with those of experiments. The comparison shows that the numerical model predicts larger depths and widths.

Characterization for selective laser sintered Fe-Cr powder (SLS 공정을 이용한 Fe-Cr 분말의 적층에 관한 연구)

  • Son, Y.M.;Jang, J.J.;Joo, B.D.;Sung, M.Y.;Moon, Y.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.282-285
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    • 2009
  • Selective laser sintering (SLS) is a fast growing process of rapid production fur metallic based parts. To restore damaged mold surface using SLS, single layer experiments of $20{\mu}m$ Fe-Cr powder was performed under various heat input. Process window of $20{\mu}m$ Fe-Cr powder provided feasible process parameters for the smooth regular surface. To estimate coherence between melted powder and basematal, tendency of hardness distribution has been observed. Hardness of melted zone and remelted zone was diversified from 5GPa to 6.5GPa. It is over 2 times compared of hardness of basemetal. Average surface roughness of each direction on surface of melted powder was measured. Experimental results show that the mold restoring process using SLS can be successfully applied in the mold repair industry.

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Surface Morphology, Microstructure and Mechanical Properties of Thin Ag Films

  • Shugurov, Artur;Panin, Alexey;Chun, Hui-Gon;Oskomov, Konstantin
    • Journal of Powder Materials
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    • v.10 no.3
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    • pp.190-194
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    • 2003
  • Thin Ag films deposited onto $SiO_2/Si$ substrates by DC magnetron sputtering and thereafter annealed ,it temperatures 100-50$0^{\circ}C$ are investigated by scanning tunneling and atomic forte microscopy. It is shown that the film surface topography and microstructure are considerably changed as a result of annealing. To provide a quantitative estimation of the surface topography changes of Ag films the surface fractal dimension was calculated. Elasticity and hardness of the films are studied by a nanoindentation technique. The films are found to have value of elastic modulus close to that of bulk silver while their hardness and yield stress are essentially higher.

Development of Wear-Resistant Sliding Parts Material

  • Shioiri, Hironori;Uemoto, Keiichi;Motooka, Naoki
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.116-117
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    • 2006
  • Conventional high-speed steels, which are carbide decentralized materials, are used for sliding parts, but they lack sufficient hardness for some applications. Improvement of surface hardness is possible for high-Cr steels through nitriding. However, nitriding P/M parts is not advisable without sealing the porosity before treatment, as they will become brittle. However, it is difficult to seal the pores with steam treatment, because high-Cr steel has a passive film on the surface. Controlling nitriding by decreasing the amount of oxygen on the surface to be nitrided, and grinding to decrease the porosity of the surface, makes it possible to produce a material that has reasonable and sufficient hardness in the required areas.

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Improvement of corrosion resistance and hardening the back ferrule surface by plasma treatment (Back ferrule 의 내식성과 체결시 기계적특성을 만족시키는 최적의 플라즈마 침질탄화공정조건의 확립)

  • Lee, In-Seop;Debnath, Sanket
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.05a
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    • pp.179-180
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    • 2012
  • Back ferrule is a circular ring shaped metallic object which is used for fastening, joining or reinforcement during the tube fitting as well as to prevent leakage. Therefore, during tube fitting the leading edge of the back ferrule should be sufficiently hard enough to prevent leakage. In our research, we concentrated the improvement of two major factors. Firstly, to improve the surface hardness of the back ferrule made by AISI 316 Stainless Steel. Secondly, the enhancement of corrosion resistance of back ferrule after plasma treatment. Initially, the corrosion resistance and hardness of the back ferrule (both commercial and without treated) was not good enough for tube fitting but after applying plasma treatment with suitable conditions on ferrule, we improved the corrosion resistance and hardness of the back ferrule dramatically.

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A Study on the Estimation of Setting Time for High Strength Concrete Using Durometer (개량형 Durometer를 이용한 고강도 콘크리트의 응결시간 추정 가능성 분석)

  • Sin, Se-Jun;Han, Soo-Hwan;Hyun, Seung-Yong;Kim, Jong;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.11a
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    • pp.87-88
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    • 2020
  • The purpose of this study is to explore the possibility of estimating optimum surface finish time of the fresh concrete placed at the job site by applying a surface hardness test meter(Durometer). Tests are carried out by measuring and comparing the Penetration resistance test and hardness test by Durometer. Penetration resistance tester and improved Durometer are similar, but the higher the temperature, the higher the setting time, and the higher the correlation was shown. When the hardness value of the improved Durometer is about 50 HD, it is found that the initial and 80 HD represent the end. It is expected that this will be useful in determining the finish time of the surface at the actual site.

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A Study on the Estimation of Setting Time for Concrete Using Durometer (개량형 Durometer를 이용한 콘크리트의 응결시간 추정 가능성 분석)

  • Sin, Se-Jun;Han, Soo-Hwan;Hyun, Seung-Yong;Kim, Jong;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.11a
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    • pp.169-170
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    • 2020
  • The purpose of this study is to explore the possibility of estimating optimum surface finish time of the fresh concrete placed at the job site by applying a surface hardness test meter(Durometer). Tests are carried out by measuring and comparing the Penetration resistance test and hardness test by Durometer. Penetration resistance tester and improved Durometer are similar, but the higher the temperature, the higher the setting time, and the higher the correlation was shown. When the hardness value of the improved Durometer is about 50 HD, it is found that the initial and 80 HD represent the end. It is expected that this will be useful in determining the finish time of the surface at the actual site.

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Degradation Behavior and Micro-Hardness Analysis of a Coolant Rubber Hose for Automotive Radiator (자동차용 냉각기 고무호스의 노화거동과 미소경도분석)

  • Kwak, Seung-Bum;Shin, Sei-Moon;Shin, Wae-Gi;Choi, Nak-Sam
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.9
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    • pp.915-923
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    • 2007
  • Rubber hoses for automobile radiators are apt to be degraded and thus failed due to the influence of contacting stresses of air and coolant liquid under thermal and mechanical loadings. The aging behaviors of the skin part of the hoses due to thermo-oxidative and electro-chemical stresses were experimentally analyzed. Through the thermo-oxidative aging test, it was shown that the surface hardness IRHD(International Rubber Hardness Degrees) of the rubber increased with a considerable reduction of failure strain as the aging time and temperature increased. On account of the penetration of coolant liquid into the skin part influenced by the electro-chemical degradation(ECD) test the weight of the rubber hose increased, whereas their failure strain and IRHD hardness decreased. The hardness of the hose in the side of the negative pole was the most deteriorated at the test site of the hose skin just below the coolant surface.