• Proceedings of the Korean Society of Precision Engineering Conference
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• 2013.05a
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• pp.41-42
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• 2013

• Transactions of the Korean hydrogen and new energy society
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• v.21 no.4
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• pp.340-345
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• 2010

For the conversion into hydrogen society, not only studying facilities of hydrogen production, storage, transportation and charging system but also developing technique of ensuring safety are essentially needed. Hence, for the first step of that, evaluated the hydrogen embrittlement of Inconel alloy 617, Ni-based super heat-resisting alloy, by small punch test. Prepared the various specimens through changing electrochemical charging time and measured the toughness degradation of the specimens by small-punch test. The analysis of hydrogen embrittlement behavior were carried out by investigating the fractured surface of specimens. This study has significance on revealing mechanism of hydrogen embrittlement behavior and the factor affecting hydrogen embrittlement in the future study.

• Journal of Welding and Joining
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• v.34 no.3
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• pp.52-60
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• 2016

Recently nickel based superalloys are extensively being regarded as the materials for the steam turbine parts for hyper super critical (HSC) power plants working at the temperature over $700^{\circ}C$, since the materials have excellent strength and corrosion resistance in high temperature. In this paper, alloy 617 of solution strengthened material and alloy 263 of ${\gamma}^{\prime}$-precipitation strengthened material were prepared as the testing materials for HSC plants each other. Post weld heat treatment (PWHT) was conducted with the gas tungsten arc (GTA) welded specimens. The microstructure of the base metals and weld metals were investigated with Electron Probe Micro-Analysis (EPMA) and Scanning Transmission Electron Microscope (STEM). The experimental results revealed that Ti-Mo carbides were formed in both of the base metals and segregation of Co and Mo in both of the weld metals before PWHT and PWHT leaded to precipitation of various carbides such as Mo carbides in the specimens. Furthermore, fine ${\gamma}^{\prime}$ particles, that were not precipitated in the specimens before PWHT, were observed in base metal as well as in the weld metal of alloy 263 after PWHT.

• Korean Journal of Materials Research
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• v.25 no.8
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• pp.403-409
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• 2015

Metastable phase characteristics of beta Ti alloys were investigated to consider the relationship of the microstructure and diffraction pattern in TEM. TEM analysis showed that the microstructure was mottled as a modulated structure, and the diffraction pattern was composed of spot streaks between the main spots of a stable beta phase with a specific lattice relationship. The modulated structure may be induced by short distance slip or atom movement during a very short interval of solution treated and quenched (STQ) materials. The athermal ${\omega}$ phase, which could be precipitated at low temperature aging, is also analysed by the metastable phase. The metastable phases including athermal ${\omega}$ phase had a common characteristic of hardened and brittle behavior because the dislocation slip was restricted by a super lattice effect due to short distance atom movement at the metastable state.

• 연구논문집
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• s.26
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• pp.95-102
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• 1996

The carbide growth behavior of MAR-M247 LC alloy was investigated by directional solidification and quench method. The carbide volume fraction, trapping and growth behavior were correlated with the growth rate. It was found that the carbide volume fraction decreases at slower growth rate. This decreasing was caused by lower solid-liquid interface trapping ability at the slower growth rate.

• The Journal of Korean Academy of Prosthodontics
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• v.40 no.4
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• pp.396-405
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• 2002

The purpose of this study was to evaluate the effects of four metal surface treatments on the shear bond strength of reline resin to Ni-Cr alloy. The denture base metal used in this study was Ni-Cr alloy(Ticonium Premium 100. Ticonium Co., U.S.A.). 120 specimens were divided into five metal surface treatments: sandblasting only, MR. BOND(Tokuyama Corp.. Japan), Cesead Opaque Primer(Kuraray Co., Japan), METALPRIMER II(GC Corp., Japan) and Super-Bond C&B(Sun Medical Co., Japan) after sandblasting. They were bonded with one of three reline resins Mild Rebaron(GC Corp., Japan), Mild Rebaron LC(GC Corp., Japan) and Meta Base M(Sun Medical Co., Japan). Then they were thermocycled 1,000 times at temperature of $4^{\circ}C$ and $60^{\circ}C$. The shear bond strengths were measured using the universal testing machine(Instron, Model 4301, England) with a cross-head speed of 2 mm/min. The results were as follows : 1. All metal primers and adhesive cement significantly improved the bond strength of reline resin to Ni-Cr alloy compared with sandblasted specimens. 2. In Mild Rebaron and Mild Rebaron LC. Cesead Opaque Primer showed the highest bond strength, but the differences among Cesead Opaque Primer, MR. BOND and METALPRIMER II were not significant. The bond strength of Cesead Opaque Primer was significantly different with that of Super-Bond C&B. 3. In Meta Base M, Super-Bond C&B showed the highest bond strength, but there was no difference between Super-Bond C&B and three metal primers. 4. There was no difference in the bond strength between Mild Rebaron and Mild Rebaron LC when metal surface was treated with the same method. 5. The bond strengths of Mild Rebaron and Mild Rebaron LC treated with Cesead Opaque Primer were higher than that of Meta Base M. The bond strengths of Mild Rebaron treated with MR. BOND and METALPRIMER II was higher than that of Meta Base M, However, there was no difference among three reline resins treated with Super-Bond C&B.

• Corrosion Science and Technology
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• v.20 no.6
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• pp.426-434
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• 2021

The effect of two different annealing temperatures on the level of the second phase precipitated in the microstructure and the corrosion behaviors of super austenitic stainless steel were examined. The sample annealed at a higher temperature had a significantly lower fraction of the sigma phase enriched with Cr and Mo elements, showing more stable passivity behavior during the potentiodynamic polarization measurement. However, after the welding process with Inconel-type welding material, severe corrosion damage along the interface between the base metal and the weld metal was observed regardless of the annealing temperature. This was closely associated with the precipitation of the fine sigma phase with a high Mo concentration in the unmixed zone (UMZ) during the welding process, leading to the local depletion of Mo concentrations around the sigma phase. On the other hand, the fraction of the newly precipitated fine sigma phase in the UMZ was greatly reduced by post-weld heat treatment (PWHT), and the corrosion resistance was greatly improved. Based on the results, it is proposed that the alloy composition of welding materials and PWHT conditions should be further optimized to ensure the superior corrosion resistance of welded super austenitic stainless steel.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.24 no.2
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• pp.94-100
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• 1988

Recently with the rapid development in marine and shipbuilding industries such as marine structures, ship, and chemical plants, there occurs much interest in the study of corrosion fatigue characteristics was closed up an important role in mechanical design. In this study, the 5086 Al-Alloy was tested by used of a rotary bending fatigue tester and was investigated under the environments of various specific resistance and air. The specific resistance, as a corrosion environment, was changed 15, 20, 25 and 5000$\Omega$.cm. The corrosion fatigue crack initiation sensitivity was quantitatively inspected for 5086 Al-Alloy in the various specific resistance. The experimental constants of Paris rule were examined in the various specific resistances, and the influences of load and corrosion with affect the crack growth rate were compared with. Main results obtained are as follows: (1) Number of stress cycles to corrosion fatigue crack initiation delaies and corrosion fatigue crack initiation sensitivity decreases with the increasing for the specific resistance. (2) The experimental constant m of Paris rule decreases with the decreasing for specific resistance. Hence the effect of corrosion is more susceptible than that of stress intensity factor. (3) The corrosion fatigue crack of 5086 Aluminium Alloy appears intergranular fracture. (4) Corrosion sensitivity is decreased with the increasing stress intensity factor and is nearly uniform when stress intensity factor is over 40kg.mm super(-3/2)

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.46 no.10
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• pp.806-813
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• 2018

The fracture of a turbine blade of aerospace engine is presented. Although there are a lot of causes and failure modes in blades, the main failure modes are two ways that fracture and fatigue. Degradation of blade material affects most failure modes. Total propagation of failure in this study specifies failure of fracture type. Some section appears fatigue mode. Especially since this study describes analysis of failure for blade in high temperature, it can be a case in point. Analysed blade is Ni super alloy. Investigations of blade are visual inspection, material, microstructure, high temperature stress rupture creep test, analysis and fracture surface, etc. The root cause for fracture was stress rupture due to abnormal thermal environment. Thermal property of Ni super alloy is excellent but if each chemical composition of alloys are different due to change mechanical properties, selection of material is very important.

• Journal of the Korean Society for Heat Treatment
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• v.24 no.5
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• pp.243-250
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• 2011

When alloys are vacuum-deposited on cooled substrates, super-rapidly cooled alloy films in the unequilibrium state can be obtained. As an application of this method, Ag-Cu, Ag-Ni and Ag-C alloys were successfully produced, and their mechanical properties with tempering temperature were investigated. The following results were obtained : (1) In case of Ag-Cu alloys, the solid solution was hardened by tempering at $150^{\circ}C$. The hardening is considered to occur when the solid solution begins to decompose into ${\alpha}$ and ${\beta}$ phases. The Knoop hardness number of a 40 at.%Ag-Cu alloy film deposited on a cooled glass substrate was 390 $kg/mm^2$. The as-deposited films were generally very hard but fractured under stresses below their elastic limits. (2) In case of Ag-Ni and Ag-C alloys, after the tempering of 4 at.%Ni-Ag alloy at $400^{\circ}C$ and of 1 and 2 at.%C-Ag alloys at $200^{\circ}C$, they were hardened by the precipitation of fine nickel and carbon particles. The linear relationship between proof stress vs. $(grain\;diameter)^{-l/2}$ for bulk silver polycrystals can be applied to vacuum-deposited films up to about 0.1 ${\mu}m$ grain diameter, but the proof stress of ultra-fine grained silver with grain diameters of less than 0.1 ${\mu}m$ was smaller than the value expected from the Petch's relation.