• 동력기계공학회지
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• 제12권1호
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• pp.47-52
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• 2008

This study was investigated the effect of subzero treatment in austempered ductile cast iron. Retained austenite transformed to martensite by subzero treatment and strain. With decreasing subzero treatment temperature and increasing strain, retained austenite transformed more to martensite and transformed 30% above by subzero treatment at $-196^{\circ}C$. With decreasing subzero treatment temperature, the value of strength and ratio of increasing of strength, hardness and ratio of increasing of hardness increased but the value of elongation and ratio of decreasing of elongation decreased. With decreasing subzero treatment temperature, impact value and ratio of decreasing of impact value decreased. In case of subzero treatment at $-196^{\circ}C$, hardness value increased about 18% and impact value decreased above 20%. We could find that in subzero treated specimens had a little of effect on the tensile properties but had very much effect on the hardness and value of the impact.

• 동력기계공학회지
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• 제11권4호
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• pp.86-91
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• 2007

This study was investigated to know the effect of subzero treatment in austempered ductile cast iron. Retained austenite transformed to martensite by subzero treatment. With decreasing subzero treatment temperature, more volume fraction of retained austenite transformed to martensite and transformed to martensite above 30% by subzero treatment temperature at $-196^{\circ}C$. With decreasing subzero treatment temperature, the value of strength and hardness increased but the value of elongation and impact value decreased. In case of subzero treatment at $-196^{\circ}C$, hardness value increased about 18% and impact value decreased by above 20%. We could find that subzero treated specimens had a little of effect on the tensile properties but had very much effect on the hardness and value of the impact.

• 열처리공학회지
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• 제25권5호
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• pp.233-238
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• 2012

The effect of subzero treatment on the mechanical properties of cold rolled high manganese austenitic stainless steel was investagated. ${\alpha}$'-martensite was formed by cold rolling, and it was formed with surface relief and specific direction or crossing each other. The volume fraction of martensite increased by subzero treatment, and it was increased with longer time of subzero treatment and higher temperature of subzero treatment. The hardness and strength increased by subzero treatment, while the elongation decreased. With the increase of volume fraction of martensite, the hardness and strength was increased steeply with proportional relationship, elongation was decreased slowly. The results show that the hardness and strength was strongly controlled by the volume fraction of martensite, and the elongation was affected by transformation behavior of deformation induced martensite in the initial stage of deformation.

• 대한금속재료학회지
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• 제47권3호
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• pp.169-174
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• 2009

The effect of sub zero treatment on the damping capacity in austempered ductile cast iron investigated. Austenite transformed in to martensite by subzero treatment, and with the decrease of subzero treatment temperature, volume fraction of martensite increased. Damping capacity of austempered ductile cast iron was highly increased by subzero treatment, with the decrease of subzero treatment temperature, damping capacity was slowly increased. With the decrease of subzero treatment time, damping capacity was rapidly increased to 30 min. and then slowly increased. With the increase of volume fraction of martensite, damping capacity rapidly increasing to 5% and then slowly increased.

• 한국산업융합학회 논문집
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• 제25권5호
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• pp.783-789
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• 2022

In this study, STS316L rolled at five rolling degrees were treated with two types of subzero temperatures for 10, 30, and 60 minutes, respectively, and the dominant frequencies of elastic waves was investigated. The dominant frequency was higher as the subzero temperature was lower and the subzero treatment time was longer at each rolling degree. On the other hand, the dominant frequency was higher as the elongation decreased. In the time-frequency analysis for subzero temperature and time of the specimen with a rolling degree of 33%, the dominant frequency was higher at a subzero temperature of -196℃ than -50℃ regardless of subzero treatment time.

• 열처리공학회지
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• 제20권2호
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• pp.65-71
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• 2007

Microstructural changes and hardness variations in STS 304 steel have been investigated during the processes of carbide dispersion (CD) carburization; carburization, austenitization, subzero treatment and tempering. The carbon content of the surface layer increased up to maximum 4.0% after carburization, and the content was homogenized with the value of 2.3% to the $95{\mu}m$ from the surface after austenitization. The carbide appeared during CD carburization process was $Cr_7C_3$ type, which was composed network carbides along the austenite grain boundaries, square type carbides in the interior of the grain and fine nano-sized carbides. The fine nano-sized carbides precipitated at the austenitization stage and possibly subzero treatment stage were coarsened after tempering at $200^{\circ}C$, resulting the hardness decrease. The tempered steel without subzero treatment increased hardness with increasing time due to the continuous precipitation of fine carbides during tempering. The nano-sized carbide appeared square type morphology.

• 한국산업융합학회 논문집
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• 제24권3호
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• pp.295-300
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• 2021

This study investigated the dominant frequency of the elastic waves from the tensile test. The specimen was rolled with five different rolling degrees (10, 22, 33, 42 and 50%), which was treated subzero. The specimen was rolled at room temperature, which was transformed from austenite to martensite (only α'-martensite). The dominant frequency increased with an increase in the rolling degree regardless of the subzero temperature, and decreased after 33% of the rolling degree. On the other hand, higher frequency band was obtained at lower temperature and long time. The dominant frequency increased when the amount of α'-martensite increased and decreased with the α'-martensite amount between 50-65%. The lower subzero treatment temperature increased the amount of α'-martensite, which resulted in the higher dominant frequency. The longer treatment time at the same subzero temperature led to an increase in the amount of α'-martensite, leading to high dominant frequency.

• 열처리공학회지
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• 제15권6호
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• pp.255-259
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• 2002

Effect of martensite on the mechanical properties of austempered ductile cast iron was investigated after obtained the martensite by subzero treatment. Retained austenite was transformed to martensite by subzero treatment, and with decreasing subzero treatment temperature, volume fraction of martensite was increased. With increasing of the volume fraction of martensite, tensile strength was increased and elongation was decreased, ratio of increasing of strength and decreasing of elongation was higher in case of specimens with lot's of Cu contents. With increasing of the volume fraction of martensite, hardness slowly increased until only about 5% and it rapidly increased in a straight proportion when it is above 5%, while impact value was rapidly decreased until about 7% but it had a little change when it is above 7%.

• 한국해양공학회지
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• 제22권6호
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• pp.46-51
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• 2008

The effect of the addition of Co and N and subzero treatment on tensile strength and damping capacity was investigated in Fe-Cr-Mn alloy. Austenite was transformed into martensite by cold rollins increasing the degree of cold rollins led to an increase in the volume fraction of martensite. The damping capacity linearly increased with increasing volume fraction of ${\varepsilon}$ martensite in cold rolled specimens and subzero treated specimens after cold rolling. The volume fraction of ${\varepsilon}$ martensite, tensile strength and damping capacity was also increased by the addition of Co, while this treatment decreased the elongation. However, the volume fraction of ${\varepsilon}$ martensite, elongation and damping capacity were reduced by the addition of N, although the tensile strength increased. Tensile strength and damping capacity werealso increased by subzero treatment, while elongation decreased.

• 열처리공학회지
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• 제22권5호
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• pp.282-289
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• 2009

The effects of the high temperature gas nitriding (HTGN), tempering and subzero treatment of STD11 steel have been investigated. HTGN treatment was carried out at $1050^{\circ}C$, $1100^{\circ}C$ and $1150^{\circ}C$ for 1 hr. in an atmosphere of $1\;kg/cm^2$ nitrogen gas. Tempering and double-tempering were performed at $550^{\circ}C$ for 1 hr. The surface layer of HTGN-treated steel appeared the precipitates of $M_2N$, $M_7C_3$ and $M_{23}C_6$ in the matrix of austenite. However, the interior region exhibited martensite with the precipitation of carbides. The nitrogen content of the surface layer appeared ~1.35 wt.%, ~0.83 wt.% and ~0.56 wt.% at the HTGN treatment temperature of $1050^{\circ}C$, $1100^{\circ}C$ and $1150^{\circ}C$, respectively. The surface hardness of double-tempered and subzero-treated steel measured the maximum value of 828 Hv, 960 Hv, 750 HV after HTGN treatment at the $1050^{\circ}C$, $1100^{\circ}C$ and $1150^{\circ}C$, respectively. These hardness value increased above 230~420 Hv compared with the HTGN-treated steel due to the decrease in retained austenite and existence of fine precipitates.