• Title/Summary/Keyword: Submicron sized particle

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Photoluminescence Characteristics of Eu-doped Yttrium Oxide Submicron-sized Particles Prepared by Aerosol Pyrolysis

  • Park, Il-Woo;Park, Chang-Kyun;Lee, Deok-Jin;Yoo, Jea-Soo
    • Transactions on Electrical and Electronic Materials
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    • v.4 no.1
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    • pp.29-33
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    • 2003
  • Europium doped yttrium oxide submicron-sized particles were prepared by ultrasonic aerosol pyrolysis. To examine the size effect of submicron-sized-particle, the photoluminescence of the particles was investigated. The particle size was controlled by pH, reaction temperature, molar concentration of yttrium in precursor solution. The PL intensity of submicron-sized particles was decreased with particles size. When the particle size is above about 150 times of Bohr radius of Y$_2$O$_3$, the optical property of the particles shows the bulk characteristics.

Nano and Submicron Sized Particle Collection with Various Voltage Waveforms for Dielectric Barrier Discharge Type 2-Stage ESP (유전체 베리어 방전형 2단 전기집진기의 인가전압 파형별 나노 및 서브마이크론 입자 집진 특성)

  • Park, Jae-Hong;Byeon, Jeong-Hoon;Hwang, Jung-Ho
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.1261-1266
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    • 2004
  • Dielectric Barrier Discharge (DBD) in air, which has been established for the production of large quantities of ozone, is more recently being applied to a wider range of aftertreatment processes for HAPs (Hazardous Air Pollutants). Although DBD has high electron density and energy, its potential use as precharging nano and submicron particles are not well known. In this work, we measured I-V characteristics of DBD and estimated collection efficiency of the particles by DBD type 2-stage ESP. To examine the particle collection with various applied voltage waveforms of DBD for nano and submicron sized, bimodal particles were generated by a electrical tube furnace and an atomizer.

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Removal of Endotoxins and Nucleic Acids Using Submicron-sized Polymeric Particles

  • Kim, Chan Wha;Chokyun Rha
    • Journal of Microbiology and Biotechnology
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    • v.6 no.3
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    • pp.189-193
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    • 1996
  • Submicron-sized polymeric particles (SSPP) were used to remove nucleic acids and endotoxins from cell lysates. The positively charged SSPP selectively adsorb nucleic acids and endotoxins and form complexes with them. The complexes can be easily removed by sedimentation or centrifugation. The removal of nucleic acids and endotoxins using SSPP also can be accomplished in the presence of cell and cell debris. Therefore, nucleic acids and endotoxins can be removed in an initial step of the down-stream processes. In bakers yeast and E. coli lysate systems, the level of DNA could be reduced more than three orders of magnitudes and endotoxins more than seven orders of magnitudes concurrently willi the cell debris removal process using SSPP.

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Particle Agglomeration of a Bipolar Charging System with a Control Grid (제어전극을 갖는 쌍극성 하전장치의 입자응집 특성)

  • Moon, Jae-Duk;Ahn, Chang-Jin
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.54 no.10
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    • pp.465-470
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    • 2005
  • In this paper. an experimental study, for method of increasing the efficiency of electrostatic precipitator for the collection of submicron-sized particles has been studied. All AC electric field was used to induce agglomeration of bipolory charged Particles. .4 bipolar AC-agglomeration system. consisted with a multineedle-mesh discharge system with a control grid, was proposed and investigated. Systematic experiments were carried out to investigate the agglomeration ratio of the AC-agglomeration system as a function of the different grid spacings and grid resistances for the submicron particles generated from liquid prorhane gas burning. The agglomeration ratios, which indicate the particle numbers before and after agglomeration of the test particles in number concentration base, were found to be 0.87, 1.80, 3.86, 9.50 and, 11.00 times for the particle sizes of 0.3. 0.5, 0.7, 1.0, and 2.0$\mu$m at applied voltage of 3.5kV, respectively which showed that the fine particle numbers were decreased while the larger particle numbers were increase greatly.

Electrorhelological Properties of Monodispersed Submicron-sized Hollow Polyaniline Adipate Suspension

  • Sung, Bo-Hyun;Choi, Ung-Su
    • KSTLE International Journal
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    • v.6 no.1
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    • pp.28-32
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    • 2005
  • The electrorheoloRical (ER) fluids are composed of a colloidal dispersion of polarizable particles in insulating oil, and it's the rheological property changes by the applied electric field. These changed are reversible and occur fast within a fewmilliseconds. The ER properties of the ER fluid such as increment of viscosity and yield stress come from the particle chain structure induced by electric fleld. When formulating the ER fluid for a speciflc application, some requirement must besatisfled, which are high yield stress under electric field, rapid response, and dispersion stability. While this characteristic makes valuable ER fluids in valious industrial applications, their lung term and quiescent application has been limited because ofproblems with particle sedimentation. In an effort to overcome sedimentation problem of ER fluids, the anhydrous ER materials of monodispersed hollow polyaniline (PANI) and adipate derivative respectively with submicron-sized suspension providing wide operating temperature range and other advantage were synthesized in a four-step procedure. The ER fluidswere characterized by FT-lR, TGA, DLS, SEM, and TEM. Stability of the suspensions was examined by an UV spectroscopy.The rheological and electrical properties of the suspension were investigated Couette-type rheometer with a high voltagegenerator, current density, and conductivity. And the behavior of ER suspensions was observed by a video camera attached toan optical microscope under 3kV/mm. The suspensions showed good ER properties, durability, and particle dispersion.

Visualization of Artificially Deposited Submicron-sized Aerosol Particles on the Surfaces of Leaves and Needles in Trees

  • Yamane, Kenichi;Nakaba, Satoshi;Yamaguchi, Masahiro;Kuroda, Katsushi;Sano, Yuzou;Lenggoro, I. Wuled;Izuta, Takeshi;Funada, Ryo
    • Asian Journal of Atmospheric Environment
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    • v.6 no.4
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    • pp.275-280
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    • 2012
  • To understand the effect of aerosols on the growth and physiological conditions of trees in forests, it is important to know the state of aerosols that are deposited on the surface of the leaves or needles. In this study, we developed methods of visualization of submicron-sized aerosols that were artificially deposited from the gas-phase or liquid phase onto tree leaves or needles in trees. Firstly, we used field-emission scanning electron microscopy (FE-SEM) to observe black carbon (BC) particles that were artificially sprayed onto the leaves or needles. The distribution of BC particles deposited on the leaves and needles were distinguished based on the size and morphological features of the particles. The distribution and agglomerates size of BC particles differed between two spraying methods of BC particles employed. Secondly, we tried to visualize gold (Au) particles that were artificially sprayed onto the leaves using energy dispersive X-ray spectrometry (EDX) coupled to FE-SEM. We detected the Au particles based on the characteristic X-ray spectrum, which was secondarily generated from the Au particles. In contrast to the case of BC particles, the Au particles did not form agglomerates and were uniformly distributed on the leaf surfaces. The present results show that our methods provide useful information of adsorption and/or behavior of fine particles at the submicron level on the surface of the leaves.

Thermal and Mechanical Properties of ZrB2-SiC Ceramics Fabricated by Hot Pressing with Change in Ratio of Submicron to Nano Size of SiC (서브마이크론/나노 크기의 SiC 비율변화에 따른 ZrB2-SiC 세라믹스의 열적, 기계적 특성)

  • Kim, Seongwon;Chae, Jung-Min;Lee, Sung-Min;Oh, Yoon-Suk;Kim, Hyung-Tae
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.410-415
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    • 2013
  • $ZrB_2$-SiC ceramics are fabricated via hot pressing with different ratios of submicron or nano-sized SiC in a $ZrB_2$-20 vol%SiC system, in order to examine the effect of the SiC size ratio on the microstructures and physical properties, such as thermal conductivity, hardness, and flexural strength, of $ZrB_2$-SiC ceramics. Five different $ZrB_2$-SiC ceramics ($ZrB_2$-20 vol%[(1-x)SiC + xnanoSiC] where x = 0.0, 0.2, 0.5, 0.8, 1.0) are prepared in this study. The mean SiC particle sizes in the sintered bodies are highly dependent on the ratio of nano-sized SiC. The thermal conductivities of the $ZrB_2$-SiC ceramics increase with the ratio of nano-sized SiC, which is consistent with the percolation behavior. In addition, the $ZrB_2$-SiC ceramics with smaller mean SiC particle sizes exhibit enhanced mechanical properties, such as hardness and flexural strength, which can be explained using the Hall-Petch relation.

Packing of Alumina Particles in 3D Preform of Mullite Fiber by Slurry Pressure-Infiltration (슬러리 가압함침에 의한 3D Mullite 섬유 Preform의 알루미나 입자 충전)

  • Sim, Soo-Man
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.528-532
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    • 2013
  • Well-dispersed slurries of submicron-sized alumina powders were pressure-infiltrated in 3D preforms of mullite fibers and the effects of the particle size and infiltration pressure on the particle packing characteristics were investigated. Infiltration without pressure showed that the packing density increased as the particle size decreased due to the reduction of the friction between the particles and the fibers. The infiltrated preforms contained large pores in the large voids between the fiber tows and small pores in the narrow voids between the individual fibers. Pressure infiltration resulted in a packing density of 77% regardless of the particle size or the infiltration pressure(210 ~ 620 kPa). Pressure infiltration shortened the infiltration time and eliminated the large pores in preforms infiltrated with the slurries of smaller particles. The slurry pressure-infiltration process is thus an efficient method for the packing of matrix materials in various preforms.

Optimization of Emulsion Polymerization for Submicron-Sized Polymer Colloids towards Tunable Synthetic Opals

  • Kim, Seul-Gi;Seo, Young-Gon;Cho, Young-Jin;Shin, Jin-Sub;Gil, Seung-Chul;Lee, Won-Mok
    • Bulletin of the Korean Chemical Society
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    • v.31 no.7
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    • pp.1891-1896
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    • 2010
  • Submicron-sized polymeric colloidal particles can self assemble into 3-dimensional (3D) opal structure which is a useful template for photonic crystal. Narrowly dispersed polymer microspheres can be synthesized by emulsion polymerization in water using water-soluble radical initiator. In this report, we demonstrate a facile and reproducible emulsion polymerization method to prepare various polymeric microspheres within 200 - 400 nm size ranges which can be utilized as colloidal photonic crystal template. By controlling the amount of monomer and surfactant, monodisperse polymer colloids of polystyrene (PS) and acrylates with various sizes were successfully prepared without complicated synthetic procedures. Such polymer colloids self-assembled into 3D opal structure exhibiting bright colors by reflection of visible light. The colloidal particles and the resulting opal structures were rigorously characterized, and the wavelength of the structural color from the colloidal crystal was confirmed to have quantitative relationship with the size of constituting colloidal particles as predicted by Bragg equation. The tunability of the structural color was achieved not only by varying the particle size but also by infiltration of the colloidal crystal with liquids having different refractive indices.

Generation of Nano/Submicron Particles Using an Electrically Heated Tube Furnace (전기가열 튜브로를 이용한 나노/서브마이크론 입자의 발생)

  • Ji, Jun-Ho;Pae, Yang-Il;Hwang, Jung-Ho;Bae, Gwi-Nam
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.12
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    • pp.1734-1743
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    • 2003
  • Aerosol generator using an electrically heated tube furnace is a stable apparatus to supply nanometer sized aerosols by using the evaporation and condensation processes. Using this method, we can generate highly concentrated polydisperse aerosols with relatively narrow size distribution. In this work, characteristics of particle size distribution, generated from a tube furnace, were experimentally investigated. We evaluated effects of several operation parameters on particle generation: temperature in the tube furnace, air flow rates through the tube, size of boat containing solid sodium chloride(NaCl). As the temperature increased, the geometric mean diameter increased and the total number concentration also increased. Dilution with air affected the size distribution of the particles due to coagulation. A smaller sized boat, which has small surface area to contact with air, brings smaller particles of narrow size distribution in comparison of that of a larger boat. Finally, we changed the electrical mobility diameter of aggregate sodium chloride particles by varying relative humidity of dilution air, and obtained non-aggregate sodium chloride particles, which are easy to generate exact monodisperse particles.