• 제목/요약/키워드: Sublimation technique

검색결과 109건 처리시간 0.021초

이차 냉각 유로를 가진 회전덕트에서 열/물질전달 특성 (I) - 요철 설치에 따른 영향 - (Detailed Measurement of Heat/Mass Transfer in a Rotating Two-Pass Duct (I) - Effects of Rib Tubulators -)

  • 김경민;김상인;김윤영;이동호;조형희
    • 대한기계학회논문집B
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    • 제28권8호
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    • pp.910-920
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    • 2004
  • The heat/mass transfer characteristics in a rotating two-pass duct with and without rib turbulators are investigated in the present study. The square duct has a hydraulic diameter ($D_h$) of 26.7 mm, and $1.5\;mm{\times}1.5\;mm$ square $90^{\circ}$-rib turbulators are attached on the leading and trailing walls. The pitch-to-rib height ratio (p/e) is 10. The Reynolds number based on the hydraulic diameter is kept constant at 10,000 to exclude the Reynolds effect, and the rotation number is varied from 0.0 to 0.20. In the smooth duct, the curvature of the $180^{\circ}$-turn produces Dean vortices that enhance heat/mass transfer in the post-turn region. When rib turbulators are installed, heat/mass transfer is augmented 2.5 times higher than that of the smooth duct since the main flow is turbulated by reattaching and separating in the vicinity of the duct surfaces. The duct rotation results in heat/mass transfer discrepancy so that Sherwood number ratios are higher on the trailing surface in the first-pass and on the leading surface in the second-pass. In the turning region, Dean vortices shown in the stationary case transform into one large asymmetric vortex cell, and subsequent heat/mass transfer characteristics also change. As the rotation number increases, the heat/mass transfer discrepancy enlarges.

Effects of Combustor-Level High Inlet Turbulence on the Endwall Flow and Heat/Mass Transfer of a High-Turning Turbine Rotor Cascade

  • Lee, Sang-Woo;Jun, Sang-Bae;Park, Byung-Kyu;Lee, Joon-Sik
    • Journal of Mechanical Science and Technology
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    • 제18권8호
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    • pp.1435-1450
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    • 2004
  • Experimental data are presented which describe the effects of a combustor-level high free-stream turbulence on the near-wall flow structure and heat/mass transfer on the endwall of a linear high-turning turbine rotor cascade. The end wall flow structure is visualized by employing the partial- and total-coverage oil-film technique, and heat/mass transfer rate is measured by the naphthalene sublimation method. A turbulence generator is designed to provide a highly-turbulent flow which has free-stream turbulence intensity and integral length scale of 14.7% and 80mm, respectively, at the cascade entrance. The surface flow visualizations show that the high free-stream turbulence has little effect on the attachment line, but alters the separation line noticeably. Under high free-stream turbulence, the incoming near-wall flow upstream of the adjacent separation lines collides more obliquely with the suction surface. A weaker lift-up force arising from this more oblique collision results in the narrower suction-side corner vortex area in the high turbulence case. The high free-stream turbulence enhances the heat/mass transfer in the central area of the turbine passage, but only a slight augmentation is found in the end wall regions adjacent to the leading and trailing edges. Therefore, the high free-stream turbulence makes the end wall heat load more uniform. It is also observed that the heat/mass transfers along the locus of the pressure-side leg of the leading-edge horseshoe vortex and along the suction-side corner are influenced most strongly by the high free-stream turbulence. In this study, the end wall surface is classified into seven different regions based on the local heat/mass transfer distribution, and the effects of the high free-stream turbulence on the local heat/mass transfer in each region are discussed in detail.

ZnO thin films with Cu, Ga and Ag dopants prepared by ZnS oxidation in different ambient

  • Herrera, Roberto Benjamin Cortes;Kryshtab, Tetyana;Andraca Adame, Jose Alberto;Kryvko, Andriy
    • Advances in nano research
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    • 제5권3호
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    • pp.193-201
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    • 2017
  • ZnO, ZnO: Cu, Ga, and ZnO: Cu, Ga, Ag thin films were obtained by oxidization of ZnS and ZnS: Cu, Ga films deposited onto glass substrates by electron-beam evaporation from ZnS and ZnS: Cu, Ga targets and from ZnS: Cu, Ga film additionally doped with Ag by the closed space sublimation technique at atmospheric pressure. The film thickness was about $1{\mu}m$. The oxidation was carried out at $600-650^{\circ}C$ in air or in an atmosphere containing water vapor. Structural characteristics were investigated by X-ray diffraction (XRD) and atomic force microscopy (AFM). Photoluminescence (PL) spectra of the films were measured at 30-300 K using the excitation wavelengths of 337, 405 and 457.9 nm. As-deposited ZnS and ZnS: Cu, Ga films had cubic structure. The oxidation of the doped films in air or in water vapors led to complete ZnO phase transition. XRD and AFM studies showed that the grain sizes of oxidized films at wet annealing were larger than of the films after dry annealing. As-deposited doped and undoped ZnS thin films did not emit PL. Shape and intensity of the PL emission depended on doping and oxidation conditions. Emission intensity of the films annealed in water vapors was higher than of the films annealed in the air. PL of ZnO: Cu, Ga films excited by 337 nm wavelength exhibits UV (380 nm) and green emission (500 nm). PL spectra at 300 and 30 K excited by 457.9 and 405 nm wavelengths consisted of two bands - the green band at 500 nm and the red band at 650 nm. Location and intensities ratio depended on the preparation conditions.

회전하는 덕트내 설치된 $70^{\circ}$ 경사요철의 열전달 특성 (Heat Transfer in Rotating Duct with $70^{\circ}$ Angled Ribs)

  • 최청;이세영;원정호;조형희;박병규
    • 한국유체기계학회 논문집
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    • 제4권3호
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    • pp.7-13
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    • 2001
  • The present study investigates convective heat/mass transfer and flow characteristics inside a cooling passage of rotating gas-turbine blades. The rotating duct has staggered ribs with $70^{\circ}$ attack angle, which are attached on leading and trailing surfaces. Naphthalene sublimation technique is employed to determine detailed local heat transfer coefficients using the heat and mass transfer analogy. Additional numerical calculations are conducted to analyze the flow patterns in the cooling passage. The present experiments employ two-surface heating conditions in the rotating duct because the exposed surfaces to hot gas stream are pressure and suction side surfaces in the middle passages of an actual gas-turbine blade. Secondary flows are generated by Coriolis and centrifugal forces in the spanwise and streamwise directions. The ribs attached on the walls disturb the mainflow resulting in recirculation and secondary flows near the ribbed wall. The local heat transfer and flow patterns in the passage are changed significantly according to rib configurations and duct rotation speeds. Therefore, the geometry and arrangement of the ribs are important for the advantageous cooling performance. The experimental results show that the ribs enhance the heat transfer more than $70\%$ from that of the smooth duct. The duct rotation generates the heat transfer discrepancy between the leading and trailing walls due to the secondary flows induced by the Coriolis force. The overal heat transfer pattern on the leading and trailing walls for the first and second passes are depended on the rotating speed, but the local heat transfer trend is affected mainly by the rib arrangements.

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복합각도 요철을 가지는 사각 덕트 내의 열전달 및 압력강하 특성 (Characteristics of Heat/Mass Transfer and Pressure Drop in a Square Duct with Compound-Angled Rib Turbulaters)

  • 최청;이동호;조형희
    • 유체기계공업학회:학술대회논문집
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    • 유체기계공업학회 2001년도 유체기계 연구개발 발표회 논문집
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    • pp.325-333
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    • 2001
  • The present study investigates convective heat/mass transfer and flow characteristics inside the cooling passage of the gas-turbine blades. It is important to increase not only the heat transfer rates but also the uniformity of heat transfer in the cooling passage. The square duct has compound-angled ribs with $60^{\circ},\;70^{\circ}$ and $90^{\circ}$ attack angles, which are installed on the test plate surfaces. a naphthalene sublimation technique is employed to determine the detailed local heat transfer coefficients using the heat and mass transfer analogy. The ribs disturb the main flow resulting in the recirculation and secondary flows near the ribbed wall and the vertices near the side-wall. The local heat transfer and the secondary flow in the duct are changed largely according to the rib orientation. Therefore, geometry and arrangement of the ribs are important fur the advantageous cooling performance. The angled ribs increase the heat transfer discrepancy between the wall and center regions because of the interaction of the secondary flows. The average heat/mass transfer coefficient and pressure drop of the ribs with the $60^{\circ}$ $-90^{\circ}$ compound-angle are higher than those with the $60^{\circ}$ attack angle. Also, the thermal efficiency of the compound-angled rib is higher than that with the $60^{\circ}$ attack angle. The uniformity of heat/mass transfer coefficient on the cross ribs may is higher than that on the parallel ribs array.

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단락 요철이 설치된 내부 냉각유로에서 회전에 따른 열/물질전달 특성 연구 (Experimental Study of Heat/Mass Transfer in Rotating Cooling Passages with Discrete Ribs)

  • 김경민;김상인;이동호;조형희
    • 대한기계학회논문집B
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    • 제29권5호
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    • pp.590-598
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    • 2005
  • The present study has been conducted to investigate the effect of discrete ribs and rotation on heat/mass transfer characteristics in a two-pass square duct with $90^{\circ}-rib$ turbulators. The rib turbulator has a square cross section of 1.5 mm. The rib height-to-hydraulic diameter ratio $({e/D_{h})$ is 0.056, and the rib pitch-to-rib height ratio (p/e) is 10. The gap width is the same as the rib height. The rotation number ranges from 0.0 to 0.2 while Reynolds number is fixed to 10,000. In a stationary duct, the heat/mass transfer on the surfaces with discrete ribs is enhanced because the gap flow promotes local turbulence and flow mixing near the ribbed surface. In a rotating duct, the gap flow affects differently the heat/mass transfer on leading and trailing surfaces with discrete ribs. On the leading surface of the first pass, heat/mass transfer is increased due to the gap flow. On the trailing surface of the first pass, however, heat/mass transfer is decreased because the gap flow disturbs reattachment of main flow. The phenomenon, that is, the difference of heat transfer between the leading and the trailing surfaces is distinctly presented by rotation.

곡관부를 가지는 내부 냉각유로에서 회전수 변화에 따른 열전달 및 유동 특성 ( I ) - 엇갈린 요철배열 덕트 - (Effects of Rotation Speed on Heat Transfer and Flow in a Coolant Passage with Turning Region ( I ) - Cross Ribbed Duct -)

  • 김경민;김윤영;이동호;조형희
    • 대한기계학회논문집B
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    • 제29권6호
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    • pp.737-746
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    • 2005
  • The present study investigates heat/mass transfer and flow characteristics in a ribbed rotating passage with turning region. The duct has an aspect ratio (W/H) of 0.5 and a hydraulic diameter ($D_h$) of 26.67 mm. Rib turbulators are attached in the cross arrangement on the leading and trailing surfaces of the passage. The ribs have a rectangular cross section of $2\;mm\;(e){\times}\;mm\;(w)$ and an attack angle of $70^{\circ}$. The pitch-to-rib height ratio (p/e) is 7.5, and the rib height-to-hydraulic diameter ratio ($e/D_h$) is 0.075. The rotation number ranges from 0.0 to 0.20 while the Reynolds number is constant at 10,000. To verify the heat/mass transfer augmentation, internal flow structures are calculated for the same conditions using a commercial code FLUENT 6.1. The heat transfer data of the smooth duct for various Ro numbers agree well with not only the McAdams correlation but also the previous studies. The cross-rib turbulators significantly enhance heat/mass transfer in the passage by disturbing the main flow near the surfaces and generating one asymmetric cell of secondary flow skewing along the ribs. Because the secondary flow is induced in the first-pass and turning region, heat/mass transfer discrepancy is observed in the second-pass even for the stationary case. When the passage rotates, heat/mass transfer and flow phenomena change. Especially, the effect of rotation is more dominant than the effect of the ribs at the higher rotation number in the upstream of the second-pass.

곡관부를 가지는 내부 냉각유로에서 회전수 변화에 따른 열전달 및 유동 특성 (II) - 평행한 요철배열 덕트 - (Effects of Rotation Speed on Heat Transfer and Flow in a Coolant Passage with Turning Region (II) - Parallel Ribbed Duct -)

  • 김경민;김윤영;이동현;조형희
    • 대한기계학회논문집B
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    • 제29권8호
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    • pp.911-920
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    • 2005
  • The present study investigates heat/mass transfer and flow characteristics in a ribbed rotating passage with turning region. The duct has an aspect ratio (W/H) of 0.5 and a hydraulic diameter ($D_h$) of 26.67 mm. Rib turbulators are attached in the parallel arrangement on the leading and trailing surfaces of the passage. The ribs have a rectangular cross section of 2 m (e) $\times$ 3 m (w) and an attack angle of $70^{\circ}$. The pitch-to-rib height ratio (p/e) is 7.5, and the rib height-to-hydraulic diameter ratio (e/$D_h$) is 0.075. The rotation number ranges from 0.0 to 0.20 while the Reynolds number is constant at 10,000. To verify the heat/mass transfer augmentation, internal flow structures are calculated for the same conditions using a commercial code FLUENT 6.1. The results show that a pair of vortex cells are generated due to the symmetric geometry of the rib arrangement, and heat/mass transfer is augmented up to $Sh/Sh_0=2.9$ averagely, which is higher than that of the cross-ribbed case presented in the previous study for the stationary case. With the passage rotation, the main flow in the first-pass deflects toward the trailing surface and the heat transfer is enhanced on the trailing surface. In the second-pass, the flow enlarges the vortex cell close to the leading surface, and the small vortex cell on the trailing surface side contracts to disappear as the passage rotates faster. At the highest rotation number ($R_O=0.20$), the turn-induced single vortex cell becomes identical regardless of the rib configuration so that similar local heat/mass transfer distributions are observed in the fuming region for the cross- and parallel-ribbed case.

회전하는 터빈 블레이드 이차유로내 요철 배열이 열/물질전달에 미치는 영향 (Effect of Heat/Mass Transfer in the turbine blade internal passage with various rib arrangement)

  • 이세영;조형희
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 추계학술대회논문집B
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    • pp.22-29
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    • 2001
  • The present study investigates the effects of various rib arrangements and rotating on heat/mass transfer in the cooling passage of gas turbine blades. The cooling passage has very complex flow structure, because of the rib turbulator and rotating effect. Experiments and numerical calculation are conducted to investigate the complex flow structures and heat transfer characteristics; the numerical computation is performed using a commercial code, FLUENT ver.5, to calculate the flow structures and the experiments are conducted to measure heat/mass transfer coefficients using a naphthalene sublimation technique. For the rotating duct tests, the test duct, which is the cross section of is $20mm\times40mm$ (the hydraulic diameter, $D_h$, of 26.7 mm, has two-pass with $180^{\circ}$ turning and the rectangular ribs on the wall. The rib angle of attack is $70^{\circ}$ and the maximum radius of rotation is $21.63D_h$. The partition wall has 10 mm thickness, which is 0.5 times to the channel width, and the distance between the tip of the partition wall and the outer wall of the turning region is 26.7 mm $(1D_h)$. The turning effect of duct flow makes the very complex flow structure including Dean type vortex and high turbulence, so that the heat/mass transfer increases in the turning region and at the entrance of the second pass. The Coriolis effect deflects the flow to the trailing surface, resulting in enhancement of the heat/mass transfer on the trailing surface and reduction on the leading surface in the first pass. However, the opposite phenomena are observed in the second pass. The each rib arrangement makes different secondary flow patterns. The complex heat/mass transfer characteristics are observed by the combined effects of the rib arrangements, duct rotation and flow turning.

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유기 분자선 증착법(OMBD)에 의한 $alpha-sexithiophene$ 박막의 제조와 특성 (The preparation of $alpha-sexithiophene$ thin films by organic molecular beam deposition method and their characteristics)

  • 권오관;김영관;손병청;박주상;변대현;신동명;최종선
    • 한국진공학회지
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    • 제7권4호
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    • pp.361-367
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    • 1998
  • 유기 박막 트렌지스터의 활성층으로 사용하기 위하여 공액성 소중합체인 $\alpha$ -sexithiophene($\alpha$-6T)이라는 시료를 가지고 유기 분자선 증착법(OMBD)을 이용하여 박막 을 제작하였으며 $\alpha$-6T박막의 성막 조건에 따른 박막의 분자 배향, 결정구조 그리고 표면 특성을 알아보기 위해 angle-resolved UV/visible absorption spectroscopy, X-ray diffractometry(XRD) 그리고 atomic force microscopy(AFM)를 이용하였으며 그 분석 결과 성막 조건에 관계없이 모두 monoclinic한 결정구조를 갖으나, 초고진공, 낮은 성막 속도, 기 판의 온도가 높은 조건일 경우 $\alpha$-6T 분자들이 기판에 수직적으로 배열한다는 것을 확일할 수 있었다.

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