• 한국표면공학회지
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• 제56권6호
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• pp.401-411
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• 2023

This study investigates the synthesis, characterization, and application of zinc oxide (ZnO) nanoparticles for corrosion resistance and stress corrosion cracking (SCC) mitigation in high-temperature and high-pressure environments. The ZnO nanoparticles are synthesized using plasma discharge in water, resulting in rod-shaped particles with a hexagonal crystal structure. The ZnO nanoparticles are applied to Alloy 600 tubes in simulated nuclear power plant atmospheres to evaluate their effectiveness. X-ray diffraction and X-ray photoelectron spectroscopy analysis reveals the formation of thermodynamically stable ZnCr₂O₄and ZnFe₂O₄ spinel phases with a depth of approximately 35 nm on the surface after 240 hours of treatment. Stress corrosion cracking (SCC) mitigation experiments reveal that ZnO treatment enhances thermal and mechanical stability. The ZnO-treated specimens exhibit increased maximum temperature tolerance up to 310 ℃ and higher-pressure resistance up to 60 bar compared to non-treated ZnO samples. Measurements of crack length indicate reduced crack propagation in ZnO-treated specimens. The formation of thermodynamically stable Zn spinel structures on the surface of Alloy 600 and the subsequent improvements in surface properties contribute to the enhanced durability and performance of the material in challenging high-temperature and high-pressure environments. These findings have significant implications for the development of corrosion-resistant materials and the mitigation of stress corrosion cracking in various industries.

• Structural Engineering and Mechanics
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• 제3권6호
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• pp.541-553
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• 1995

The determination of the stress intensity factors is investigated by using the surface integral defined around the crack tip of the structure. In this work, the integral method is derived naturally from the standard path integral J. But the use of the surface integral is also extended to the case where body forces act. Computer program for obtaining the stress intensity factors $K_I$ and $K_{II}$ is developed, which prepares input variables from the result of the conventional finite element analysis. This paper provides a parabolic smooth curve function. By the use of the function and conventional element meshes in which the aspect ratio (element length at the crack tip/crack length) is about 25 percent, relatively accurate $K_I$ and K_{II}$ values can be obtained for the outer integral radius ranging from 1/3 to 1 of the crack length and for inner one zero.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 1999년도 춘계학술대회 논문집
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• pp.263-268
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• 1999

With HAZ of A 106 Gr B steel weldment, fatigue test in air, electrochemical polarization test and corrosion fatigue test in 3.5wt.% NaCl solution were performed changing load ratio. Obtained results are as follows. 1) K$\sub$op/ was independent of K$\sub$max/ and load ratio in fatigue crack growth. 2) In variation of load ratio, the scatter band of crack growth curve was reduced by half considering crack closure 3) In the result of electrochemical polarization test, current density was increased abruptly when potential was larger than corrosion potential. 4) Fatigue crack growth rate in corrosive environment was markly higher than the rate in air because of corrosion characteristics of the material and anodization of inner surface crack.

• 한국산업융합학회 논문집
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• 제26권6_2호
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• pp.1011-1017
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• 2023

In this study, the harmless crack size (a_hml) by double shot peening (DSP) using shot balls with different diameters was evaluated on carburized, quenched-tempered SCM822H steel. The minimum crack size (a_NDI) detectable by non-destructive inspection was also evaluated. The relationship between the crack size (a_25,50) that reduces the fatigue limit by 25% and 50% and a_hml was evaluated. The residual stress of DSP was greater in SP_(0.6+0.08) than SP_(0.8+0.08) and appeared deeper in the depth direction. In addition, the hardness below the surface appeared larger. The fatigue limit of DSP increased 2.07 times and 1.95 times compared to non-SP. All a_hml of the DSP specimen was determined at the depth (a). The compressive residual stress distribution affects a_hml, and the a_hml of SP_(0.6+0.08), which has a large compressive residual stress and a high fatigue limit, appeared large. a_hml of SP_(0.6+0.08) introduced deeper than the residual stress of SP_(0.8+0.08) is larger in the range of As=1.0-0.3. Since the residual stress in the thickness direction has a greater effect on a_hml than the residual stress at the surface, it is necessary to introduce it more deeply. The relation of a_hml, a_25,50, and a_NDI were evaluated in the point for safety and reliability.

• 한국표면공학회지
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• 제55권1호
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• pp.18-23
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• 2022

Presence of cracks in electrodeposited hard chromium layer, which provide a path of corrosive media to steel substrate, is a serious issue in metal finishing with chromium electroplating. In this study, we added sodium molybdate in an electrolyte for chromium electroplating bath. 130g/L of sodium molybdate in Sargent bath for chromium electroplating causes a codepostion of molybdenum with chromium in a rage of 0.61 ~ 3.14 wt.%. The co-deposited molybdenum enhances the crystallinity of chromium layer, thus the hardness is slightly decreases by the addition of molybdate in electrolyte. However, due to the co-deposition of molybdenum, a crack-free chromium layer could be electrodeposited. Such crack-free chromium layer shows a significantly improved corrosion resistance.

• 한국전산구조공학회:학술대회논문집
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• 한국전산구조공학회 2004년도 봄 학술발표회 논문집
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• pp.309-316
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• 2004

A probabilistic structural integrity assessment is performed for a reactor pressure vessel under PTS(Pressurized Thermal Shock). A semi-elliptical finite axial crack is assumed to he in the beltline region(either base metal or weld meta)1 of the reactor vessel inside surface. The selected random variables are initial crack depth, neutron fluence on the vessel inside surface, copper, nickel, and phosphorus content of the vessel material, and RT/sub NDT/. The probabilities of crack initiation or vessel failure where the crack is propagated through vessel wall are calculated. The probabilities obtained with random crack size are compared to these obtained with deterministic us. Since the failure function cannot to explicitly by selected by selected random variables, Monte Carlo Simulation is applied to perform probabilistic analysis The influence of the amount of neutron fluence is also examined to assess the structural reliability for vessel life time.

• 비파괴검사학회지
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• 제31권1호
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• pp.1-10
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• 2011

Nonlinear harmonic waves generated at cracked interfaces are investigated both experimentally and theoretically. A compact tension specimen is fabricated and the amplitude of transmitted wave is analyzed as a function of position along the fatigued crack surface. In order to measure as many nonlinear harmonic components as possible a broadband Lithium Niobate ($LiNbO_3$) transducers are employed together with a calibration technique for making absolute amplitude measurements with fluid-coupled receiving transducers. Cracked interfaces are shown to generate high acoustic nonlinearities which are manifested as harmonies in the power spectrum of the received signal. The first subharmonic (f/2) and the second harmonic (2f) waves are found to be dominant nonlinear components for an incident toneburst signal of frequency f. To explain the observed nonlinear behavior a partially closed crack is modeled by planar half interfaces that can account for crack parameters such as crack opening displacement and crack surface conditions. The simulation results show reasonable agreements with the experimental results.

• 한국산업융합학회 논문집
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• 제10권1호
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• pp.39-46
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• 2007

The objective of this paper is to examine the detection limit, growth characteristics and notch curvature radius in short crack problem. Measurement techniques such as ultrasonic method and back-face strain compliance method were adapted. The fatigue crack growth rate of the short crack is slower than that of a long crack for a notched specimen. The short crack is detected effectively by ultrasonic method. A short surface crack occurs in the middle of specimen thickness and is transient to a through crack when maximum crack depth is larger than the notch curvature radius.

• 한국정밀공학회지
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• 제14권11호
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• pp.69-76
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• 1997

The rotating bending fatigue tests were performed using the specimens taken from Cr-Mo-V steel, widely sued in thermal power plant turbines, at various temperatures such as room temperature, 300 .deg. C, 425 .deg. C and 550 .deg. C. The characteristics of fatigue crack propagation were examined and analyzed by using fracture mechanics parameter. The plastic replica method was also applied in order to measure the crack length on the basis of serial observation of fatigue crack propagation behavior on the defected specimen surface. The fatigue crack propagation behavior of Cr-Mo-V steel was investigated within the frame work of elastic-plastic fracture mechanics. The propagation law of fatigue crack is obtained uniquely by using the term .sigma. $^{n}$ sub a/where .sigma. $_{a}$ is the service stress, a is the crack length and n is a constant. The values of constant n are nearly equal to 2.48, 2.60 and 8.61 at room temperature, 300 .deg. C and 425 .deg. C.

• 대한기계학회논문집A
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• 제26권2호
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• pp.380-386
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• 2002

Damage behaviors induced in silicon carbide by an impact of particle having different material and size were investigated. Especially, the influence of the impact velocity of particle on the cone crack shape developed was mainly discussed. The damage induced by spherical impact was different depending on the material and size of particles. Ring cracks on the surface of specimen were multiplied by increasing the impact velocity of particle. The steel particle impact produced larger ring cracks than that of SiC particle. In the case of high velocity impact of SiC particle, radial cracks were produced due to the inelastic deformation at the impact site. In the case of the larger particle impact, the damage morphology developed was similar to the case of smaller particle one, but a percussion cone was farmed from the back surface of specimen when the impact velocity exceeded a critical value. The zenithal angle of cone cracks developed into SiC material decreased monotonically with increasing of the particle impact velocity. The size and material of particle influenced more or less on the extent of cone crack shape. An empirical equation, $\theta$= $\theta$$\sub$st/, v$\sub$p/(90-$\theta$$\sub$st/)/500 R$\^$0.3/($\rho$$_1$/$\rho$$_2$)$\^$$\frac{1}{2}$/, was obtained as a function of impact velocity of the particle, based on the quasi-static zenithal angle of cone crack. It is expected that the empirical equation will be helpful to the computational simulation of residual strength in ceramic components damaged by the particle impact.