• 한국결정성장학회지
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• 제29권1호
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• pp.24-31
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• 2019

사파이어 단결정을 성장시키는 기존 합성방법들의 원료충진율을 높이기 위한 방법으로 스컬용융법을 사용하여 $Al_2O_3$ 파우더를 용융시켰다. 냉각도가니 크기는 내경 24 cm, 내부 높이 30 cm로서 2.75 MHz 발진주파수에서 15 kg의 $Al_2O_3$ 파우더를 1시간 내에 모두 용융시켰으며, 3시간 동안 융액상태로 유지 후 자연냉각 시켰다. 냉각된 잉곳의 부분별 면밀도 및 성분은 SEM-EDS를 통해 분석하였다. 잉곳의 면밀도 및 $Al_2O_3$ 함량은 고주파유도가열 시 냉각도가니 내부에 형성되는 온도 분포와 관련이 있으며, 온도가 높게 형성되었던 부분이 면밀도 및 순도가 높게 나타나는 경향을 보였다.

• Progress in Superconductivity
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• 제13권3호
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• pp.189-194
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• 2012

Studies on the development of high voltage superconducting apparatuses, such as transmission superconducting fault current limiters (SFCLs) and superconducting cables, have been performed worldwide. In this paper, a study on the electrical insulation characteristics of electro negative gas according to various pressures and utilization factors was conducted as a part of developing a high voltage superconducting coil with a sub-cooled nitrogen cooling system. Some gases such as helium (He), nitrogen ($N_2$), and sulfur hexafluoride ($SF_6$) are considered for pressurizing the sub-cooled nitrogen cooling system of high voltage SFCLs and superconducting cables. $SF_6$ is used to pressurize and enhance the dielectric performance of a superconducting system of a sub-cooled nitrogen cooling system for superconducting cables being developed in the Republic of Korea. In this paper, dielectric experiments on AC voltage, as well as lightning impulse voltage of $SF_6$, are conducted according to various utilization factors by using several kinds of sphere-to-plane electrode systems. As results, it is known that the empirical formulae of $SF_6$, known as an electro negative gas, are derived according to various pressures and utilization factors. Also, the appropriate pressure condition for designing a high voltage superconducting coil is found from the viewpoint of dielectric performance.

• 한국전기화학회:학술대회논문집
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• 한국전기화학회 2005년도 수소연료전지공동심포지움 2005논문집
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• pp.103-110
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• 2005

Fuel cell systems are consisted of various parts, for example fuel cell stack, fuel supplier, electrical converters, controllers and so on. Each components of system should have appropriate specification for their applications as well as simplicity. Because thermal load can be managed simply by using fans without any water cooling system, the air-cooled PEMFC is widely used in sub kW and around 1kW systems. The performance of an air-cooled system is highly dependent on ambient temperature and humidity. In this paper, the air-cooled PEMFC systems are developed and investigated to study the operating characteristics in the aspect of the thermal and water coupled management by the control of the axial fans and compressors. Various experiments were also conducted to get the cell voltage distribution, the relative humidity of the reactant gas and the thermal management by axial cooling fans, which cannot be observed in single cell experiment. After then, as practical applications, portable fuel cell system and a hybrid electric cart were successfully integrated and operated by using this air-cooled stack.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2006년도 제27회 추계학술대회논문집
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• pp.169-174
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• 2006

본 연구는 재생냉각형 고압 축소형 연소기 설계에 관한 것으로 이 연소기를 제작하기 전에 열유속측정을 위한 물냉각 고압 축소형 연소기를 제작하였다. 물냉각 고압 축소형 연소기의 연소시험결과 높은 연소성능 및 냉각성능이 검증된 설계 조건을 얻었고 이를 바탕으로 재생냉각형 고압 축소형 연소기의 형상을 설계하였다. 설계된 연소기의 형상은 제작이 완료된 후 연소시험을 수행하여 실용성을 검증 할 예정이다.

• 항공우주기술
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• 제6권2호
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• pp.141-149
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• 2007

재생냉각과 막냉각 그리고 열차폐 코팅이 적용된 재생냉각 축소형 연소기를 이용하여 연소시험을 수행하였다. 시험결과 적용된 냉각 방식은 설계 조건에서 그 역할을 충실히 수행하였으나 연료 매니폴드 내에 삽입된 구조 보강용 링에 의한 연료 유동의 불안정성으로 인해 고주파 연소불안정이 발생하였다. 연료 유동의 불안정성은 삽입 링을 제거함으로써 개선되었고 추가 연소시험을 통해 수정된 연소기의 연소안정성을 검증할 예정이다.

• 한국추진공학회지
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• 제6권4호
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• pp.1-6
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• 2002

소형 연소기의 냉각 유로 설계를 위하여 열전달 및 냉각 유로의 구조해석을 수행하였다. 연소기의 고온가스에서의 열전달에 관한 2차원 해석을 수행하여 연소실 벽으로의 열유속을 예측한 다음 이를 3차원 해석을 위한 열경계 조건으로 적용하였다. 위 방법으로 예측한 열 유속은 기존의 경험식과 비교하여 검증하였으며 냉각수의 유량에 둔감한 것으로 판명되어 냉각 조건이 변화하더라도 동일한 열경계 조건을 사용할 수 있었다. 단일 냉각 유로에 대한 3차원 해석을 수행하여 연소실 벽의 최대온도 변화를 예측하였으며 이는 재사용 연소기 개발에 적용될 것이다. 냉각 유로의 정적 구조 해석을 통해 응력 분포와 구조 안전성을 예측하였다.

• 한국초전도ㆍ저온공학회논문지
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• 제19권1호
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• pp.30-35
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• 2017

The effects of the crystallographic orientation and sample thickness on the magnetic levitation forces (F) and trapped magnetic field (B) of single grain YBCO bulk superconductors were examined. Single grain YBCO samples with a (001), (110) or (100) surface were used as the test samples. The samples used for the force-distance (F-d) measurement were cooled at 77 K without a magnetic field (zero field cooling, ZFC), whereas the samples used for the B measurement were cooled under the external magnetic field of a Nd-B-Fe permanent magnet (field cooling, FC). It was found that F and B of the (001) surface were higher than those of the (110) or (100) surface, which is attributed to the higher critical current density ($J_c$) of the (001) surface. For the (001) samples with t=5-18 mm, the maximum magnetic levitation forces ($F_{max}s$) of the ZFC samples were larger than 40 N. About 80% of the applied magnetic field was trapped in the FC samples. However, the F and B decreased rapidly as t decreased below 5 mm. There exists a critical sample thickness (t=5 mm for the experimental condition of this study) for maintaining the large levitation/trapping properties, which is dependent on the material properties and magnitude of the external magnetic fields.

• Journal of Magnetics
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• 제13권4호
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• pp.149-152
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• 2008

In this report, we present the results of a study on the effects of the particle size on the properties of the Prussian blue (PB) analog $Na_xMn_y[Fe(CN){_6}]$. A novel synthesis method of the $Na_xMn_y[Fe(CN){_6}]$ nano-particles using an organic solvent, formamide, is employed. The size of the PB particles is found to be 100-150 nm for the samples prepared in the formamide solvent, which is much smaller than that of the samples prepared using water only. The broadening of the X-ray diffraction peaks of the nano-sized PB samples is attributed to the lattice disorder and a dramatic reduction in the particle size. The compositions of the samples are confirmed by an energy-dispersive X-ray analysis (EDAX), and the result proves that the samples are actually $Na_xMn_y[Fe(CN){_6}]$ Prussian blue. The UV-vis spectra show a broad intervalence charge-transfer (CT) band in the visible region between 400 and 700 nm, and the absorption decreases abruptly in the green region for the nano-sized PB sample. A divergence between the field cooled (FC) and zero field cooled (ZFC) magnetization curves is observed for the nano-sized PB sample at 11 K, indicating that nanoparticles in the sample are single domain superparamagnets with a blocking temperature of 11 K. Our results reveal that the nano-sized PB samples show significantly different optical and magnetic properties than those of the bulk PB samples.

• Journal of the Korean Physical Society
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• 제73권12호
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• pp.1863-1866
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• 2018

The sodium-iron phosphate maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ was synthesized using the ball mill method. The crystal structure and magnetic properties of the prepared materials were studied using X-ray diffraction (XRD), vibrating sample magnetometer (VSM), and $M{\ddot{o}}ssbauer$ spectroscopy. Structural refinement of maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ was analyzed using the FullProf program. From the XRD patterns, the crystal structure of maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ was found to be orthorhombic with the space group Pmnb. The lattice parameters of maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ are as follows: $a_0=6.866{\AA}$, $b_0=8.988{\AA}$, $c_0=5.047{\AA}$, and $V=311.544{\AA}^3$. Maricite-$NaFePO_4$ has an edge-sharing structure that consists of $FeO_6$ octahedral. Under an applied field of 100 Oe, the temperature dependences of zero-field-cooled (ZFC) and field-cooled (FC) curves were measured from 4.2 to 295 K. $M{\ddot{o}}ssbauer$ spectra were also recorded at various temperatures ranging from 4.2 to 295 K. We thus confirmed that the $N{\acute{e}}el$ temperature of $NaFe_{0.9}Mn_{0.1}PO_4$ ($T_N=14K$) was lower than that of maricite-$NaFePO_4$ ($T_N=15K$).

• Transactions on Electrical and Electronic Materials
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• 제17권4호
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• pp.227-230
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• 2016

Zn_xMn_3-xO₄ (0.95≤x≤1.20) specimens were prepared using a conventional solid state reaction method. All specimens were sintered in air at 1,200℃ for 12 h, cooled at a rate of 2℃/min to 800℃, and subsequently quenched to room temperature. We investigated the electrical properties of Zn_xMn_3-xO₄ specimens with various amounts of ZnO for use as IR detectors. At a composition of x≥1.15, the ZnO phase precipitates beside the spinel structure. The electrical resistivity at room temperature, activation energy, responsivity, and detectivity of a Zn_1.10Mn_1.90O₄ specimen are 653.2 kΩ-cm, 0.392 eV, 0.016 V/W, and 7.52×10³ cmHz^1/2/W, respectively.