• Title/Summary/Keyword: Structure determination

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Structure Determination of Nano-crystalline, $BaTiO_3$, using Precession Electron Diffraction (세차전자회절을 이용한 $BaTiO_3$ 나노 결정의 구조분석)

  • Song, Kyung;Kim, Youn-Joong;Kwon, Ki-Hyun;Kim, Jin-Gyu;Moon, Sun-Min;Cho, Nam-Hee
    • Applied Microscopy
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    • v.39 no.4
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    • pp.341-348
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    • 2009
  • The crystal structure of nano-crystalline, $BaTiO_3$, with the average particle size of 100 nm was investigated using electron diffraction techniques. We characterized the precession electron diffraction system and then carried out the structure determination using precession electron diffraction and conventional selected area electron diffraction. As a result, it was revealed that $BaTiO_3$ nano-crystalline exist as a mixture of tetragonal structure and cubic structure by precession electron diffraction technique. In addition, it could be turned out that $BaTiO_3$ nano-crystalline is a core-shell structure consisted of a tetragonal phased core and a cubic phased surface layer by theoretical calculation. The thickness of the cubic surface layer was approximately 8.5 nm and the lattice parameters of cubic and tetragonal phases were a=3.999${\AA}$ and a=3.999${\AA}$, c=4.022${\AA}$, respectively. Finally, it is expected that precession electron diffraction is more useful technique for structure determination of complicated nano-crystalline materials because of its higher spatial resolution and minimization of dynamical scattering effect.

Motion Analysis of a Very Large Floating Structure in Irregular Waves (불규칙파 중 초대형 부유식 해양 구조물에 대한 운동 해석)

  • 신현경;이호영;임춘규;신현수;박인규
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2000.04a
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    • pp.63-68
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    • 2000
  • A very large floating structure has rather small motion characteristics as to the whole body, while the motion at end part of such structure becomes largest due to the elastic motion of the structure. This paper presents on the theoretical result on the relative motion characteristics and green water phenomena of VLFS in waves This phenomena affect not only to strength of the structure but also the determination of depth of structure. To predict motion responses of structure in regular waves, the source-dipole distribution method and F.E.M is used By irregular wave results, the probability of occurrence of green water and response of the structure were calculated.

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Design Automatization of Space Truss Structure Using Optimizations Technique (최적화 기법을 이용한 3차원 트러스 구조물의 설계자동화)

  • 최은규;임기식;이병해
    • Proceedings of the Computational Structural Engineering Institute Conference
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    • 1993.10a
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    • pp.81-90
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    • 1993
  • The optimum design of a structure requires the determination of the economical member size and shape of the structure which satisfies the design condition and function. In this study, the process of design automatization of three-dimensional truss structure introduces the optimization technique tests its application in the design automatization, proposes its application method and applies the example structure of the parabolic antenna truss. Using the Formex Algebra of configuration function, the structure's mesh-generation is automatized. By using the program developed in this study, the input member array, member size and load condition designer can generate the input data file for the structure analysis and optimum design. This study is aimed at the development of a design automatization system that search for tile optimum value of a structure design by observing the structure's sensitivity from the modification of member array and member property.

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