• Progress in Superconductivity
• /
• 제1권1호
• /
• pp.51-55
• /
• 1999

A Ni/Ag/Stainless steel 310S(SS310S) multi-layer sheet has been fabricated by a combination of vacuum brazing, cold rolling and texture annealing processes. After heat-treating the thin Ni/Ag/SS310S multi-layer sheet at $900^{\circ}C$ for 2h, development of (100)<001>cube texture on Ni surface was revealed by (111) pole figure. Quantitative chemical analysis was made by EPMA for the cross-section of the Ni/Ag/SS310S multi-layer sheet. EPMA results showed that Ag diffusion into the Ni layer, which may suppress the cube texture development, was negligible. A small amount of Cr atoms were detected in the Ni layer. It showed that Ag can be used as a chemical barrier of alloying element atoms in Ni layer for the Ni/Ag/SS310S multi-layer sheet and a strong cube texture was developed for the Ni layer in the Ni/Ag/SS310S multi-layer sheet.

• 소성∙가공
• /
• 제29권6호
• /
• pp.323-330
• /
• 2020

The surface region of a sheet metal may have different characteristics from the inner region because the surface region is less restricted than the interior. In addition, the grains on the free surface are less hardened because of surface adsorption of the dislocations, rather than piling up. In the case of bulk or thick sheet metals, this effect is negligible because the fraction of the surface region is much smaller than that of the inner region. However, this surface effect is important in the case of ultra-thin sheet metals. In order to evaluate the surface effect, tensile and bending tests were performed for the SS304 stainless steel with a thickness of 0.39 mm. The bending force predicted using the tensile behavior is higher than the measurement because of the surface effect. To account for the surface effect, the surface layer model was developed by dividing the sheet section into surface and inner layers. The mechanical behaviors of the two regions were calibrated using the tensile and bending properties. The surface layer model reproduced the bending behavior of the ultra-thin sheet metal.

• Composites Research
• /
• 제22권4호
• /
• pp.33-40
• /
• 2009

유리섬유/에폭시 복합재료로 피막한 판유리의 표변파괴거동에 대한 섬유방향효과를 미소강구 충격실험을 통해 연구했다. 본 연구에서는 단순소다유리판(soda-lime glass plates), 일방향 유리섬유/에폭시박막 (glass/epoxy lamina ply)을 1층 및 2층 접착, 직교형 유리섬유/에폭시 박막 (2층)을 접착한 4종류의 시편을 사용하였다. 유리판 배면에 스트레인게이지를 부착하여 충격중의 최대 응력과 흡수파괴에너지를 측정하였다. 피막없는 판유리의 경우 충격속도 증가에 따라 링균열, 콘균열, 레이디얼 균열이 충격표면부에서 발생하였다. 복합재료 박막으로 피막한 결과, 소다유리판의 균열은 현저히 감소하였으며 섬유층과 판유리사이의 박리 및 소성변형영역의 방향은 섬유방향으로 진행했다. 최대응력과 흡수파괴에너지를 이용하여 구한 충격 표면파괴지수는 표면저항의 효과적인 평가지수로서 사용될 수 있었다.

• 한국표면공학회:학술대회논문집
• /
• 한국표면공학회 2015년도 추계학술대회 논문집
• /
• pp.289-290
• /
• 2015

In this experiment, nitriding treatment has been performed at $400^{\circ}C$ with various $N_2$ content and with changing processing time on AISI 420 martensitic stainless steel to investigate the expanded martensite layer (${\alpha}^{\prime}_N$ layer) formation behavior. Nitriding was implemented with changing $N_2$ content from 10% to 25% for 15 hrs and processing time was changed from 4hr to 15hr at 25% $N_2$ content. After treatment, the behavior of the ${\alpha}^{\prime}_N$ layer was investigated by optical microscopy, X-ray diffraction, and micro-hardness testing. Potentiodynamic polarization test was also used to evaluate the corrosion resistance of the samples. It was found that the surface hardness and ${\alpha}^{\prime}_N$ layer thickness increases with increasing $N_2$ percentage and processing time. Although their corrosion behaviors are worse than the bare sample.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2006년도 춘계학술대회 논문집
• /
• pp.308-313
• /
• 2006

The effect of coating time on surface properties of the TiN-coated high speed steel(SKH51) by arc ion plating is and presented in this paper. Surface roughness, micro-hardness, coated thickness, atomic distribution of TiN and adhesion strength are measured for various coating times. It has been shown that the coating time has a deep influence more than 60 minites on the micro-hardness, coated thickness, atomic distribution of Ti and adhesion strength of the SKH51 steels, but that the coating time has little influence on the surface roughness.

• 한국군사과학기술학회지
• /
• 제13권2호
• /
• pp.275-282
• /
• 2010

The improved properties of surface layer can be achieved by so-called "new salt bath nitriding(NSBN)", which has been developed by a domestic company. This process based upon modified traditional salt bath nitriding process, increased hardenability with minimum toughness deterioration. This process also offers not only less white layer surfaces but also more eco-friendly one. That is, NSBN is the new eco-friendly surface treatment technology removing harmful $CN^-$ and toxic gas. According to the research of applying NSBN to Cr-Mo-V steel which has been used in defense industry, showed the improved result of wear resistance and surface hardening than non-coated condition. In further, we expect NSBN to curtail expenses and productivity improvement applied to the various defense industry parts.

• 한국표면공학회:학술대회논문집
• /
• 한국표면공학회 2013년도 춘계학술대회 논문집
• /
• pp.109-110
• /
• 2013

Medium carbon steel was aluminized by hot dipping into molten Al or Al-1%Si baths. After hot-dipping in these baths, a thin Al-rich topcoat and a thick alloy layer rich in $Al_5Fe_2$ formed on the surface. A small a mount of FeAl and $Al_3Fe$ was incorporated in the alloy layer. Silicon from the Al-1%Si bath was uniformly distributed throughout the entire coating. The hot dipping increased the microhardness of the steel by about 8 times. Heating at $700-1000^{\circ}C$ however decreased the microhardness through interdiffusion between the coating and the substrate. The oxidation at $700-1000^{\circ}C$ in air formed a thin protective ${\alpha}-Al_2O_3$ layer, which provided good oxidation resistance. Silicon was oxidized to amorphous silica, exhibiting a glassy oxide surface.

• 한국진공학회지
• /
• 제7권1호
• /
• pp.59-65
• /
• 1998

13.56MHz를 사용하는 r.f.PACVD(Plasma assisted chemical vapor deposition)방법 으로 다층 다이아몬드상 카본(DLC)필름을 Si wafer기판 위에 합성하였다. 다층 DLC필름은 2.5$\mu$m두께의 순수한 DLC필름과 0.2$\mu$m두께의 Si이 함유된 Si-DLC필름으로 구성되었으 며, ball on disk type의 tribometer를 이용하여 대기 중에서 다층 DLC필름의 마모거동을 고 찰하였다. 표면층으로 합성된 Si-DLC필름내의 Si함량이 증가함에 따라 다층 DLC필름과 AISI52100 steel ball 사이에 0.1 이하의 낮은 마찰계수를 유지하는 기간이 증가하였다. 44,000cycle과 158,400cycle의 마모실험 후 측정된 다층 DLC필름의 마모율은 각각 $2.5\times10^{-8}\sim1.8\times10^{-7}\textrm{mm}^3$/rev.과 $7.1\times10^{-9}\sim1.8\times10^{-8}\textrm{mm}^3$/rev.로 나타났다. 158,400cycle의 마모실험 후 측정된 마모율은 내마모 특성이 우수한 DLC필름보다도 2배 정도 우수한 것으로 나타났 다. 마모시험에 의해 형성된 debris의 조성을 분석한 결과, 이런 낮은 마찰계수와 우수한 내 마모 특성은 steel ball의 wear 표면을 덮고 있는 Si oxide debris층의 형성에 따른 결과로 판단되었다. 또한, 이러한 steel ball의 wear scar표면에 형성된 debris층을 제거하여도, 새로 운 Si oxide debris층이 wear scar표면에 다시 생성되어 낮은 마찰계수를 유지하고 있었다.

• 한국재료학회지
• /
• 제2권6호
• /
• pp.436-442
• /
• 1992

레이저빔에 의한 철강재의 Ti 표면합금화에 미치는 C함량의 영향을 관찰하였다. 철강재상에 Ti 코팅 후 레이저빔 조사시 질소를 취입가스로 사용하면 부분적으로 TiN과 F$e_2$Ti가 형성된다. 저탄소강의 경우 Ti함량의 증가에 따라 임계냉각 속도의 증가로 마르텐사이트화가 억제된다. 고탄소강의 경우 Ti의 함량이 1.5%정도 임에도 훼라이트 조직이 형성되지 않고 마르텐사이트 조직이 형성되어 경화된다. 그리고 고탄소강의 Ti 표면합금층 형성에 부분적인 TiC의 석출이 있어 더욱 경도를 증가시키는 것으로 생각된다.

• 열처리공학회지
• /
• 제35권5호
• /
• pp.246-254
• /
• 2022

The high-temperature oxidation behavior of Cr-Mo steel AISI 4115 in air at different temperatures (600, 850, 950℃) for 120 min was studied by mass gain analysis, phase analysis (optical microscopy, electron probe micro-analysis, x-ray diffraction) and hardness measurement of each iron oxide-phase. The oxidation scales that formed on oxidation process consisted outer layer (Hematite), middle layer (Magnetite) and the inner layer (Chromite). In the case of 850 and 950℃, the oxidation mass gain per unit area of AISI 4115 steel increased according to the logarithmic rate as atmospheric pressure increased. Especially, It has been observed that with an increase in the atmospheric pressure at 600℃, the oxidation mass gain per unit area changed from a linear to logarithmic relationship.