• 대한기계학회논문집A
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• 제26권11호
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• pp.2322-2327
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• 2002

The corrosion degradation characteristics of the 12Cr alloy steel, which is widely used in fossil power plants as a turbine blade material, are evaluated nondestructively by use of the backward radiated Rayleigh surface wave. In order to evaluate corrosion degradation characteristics, we constructed automated system for the backward radiation, and the frequency dependency of the Rayleigh surface wave is investigated indirectly by measuring the angular dependency of the backward radiation of the incident ultrasonic wave in the specimens. The velocity of the surface wave decrease as the increase of the aging time in the backward radiation profile, which seems to result from the increase of the effective degrading layer thickness. And, amplitude of the surface wave increase as the aging time, which seems to result from the increase of the intergranular corrosion. The result observed in this study demonstrates high potential of the backward radiated ultrasound as a tool for the nondestructive evaluation of the corrosion degradation characteristics of the aged materials.

• 한국표면공학회지
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• 제47권1호
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• pp.1-6
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• 2014

The copper deposit on steel plate was prepared by pyrophosphate copper plating solution made with variation of inorganic additive. $NH_4OH$ and $NH_4NO_3$ were used as inorganic additives. The copper layer characteristics - tensile strength, crystallite size and crystal orientation - were evaluated by X-ray diffraction and Universal Test Machine. The presence of ammonium nitrate results in reduction of average roughness value from $0.08{\mu}m$ to $0.03{\mu}m$. In pyrophosphate copper plating solution without Inorganic additive, tensile strength of electrodeposit copper foil was reduced from 600 MPa to 180 MPa after 7 days aging. However, when adding ammonium nitrate, there was almost no change of tensile strength, intensity of crystal orientation - (111), (200) and (220) - and crystallite size (2~30 nm).

• 대한기계학회논문집A
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• 제39권5호
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• pp.543-547
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• 2015

고강도 철근을 생산하기 위해서는 템프코어(Tempcore)라고 불리는 냉각 공정이 적용되고 있는데, 템프코어를 이용하면 합금원소를 첨가하지 않고 Mild steel 로부터 강도 및 용접성이 우수한 철근을 생산 할 수 있다. 하지만 현장 설비를 이용하여 다양한 냉각 조건과 화학성분 변경의 영향을 평가하기에는 한계가 있다. 따라서, 본 연구에서는 템프코어 공정을 모사하기 위한 장치를 개발하였으며, 이를 이용하여 경화된 표층부, 중간영역, 연한 내부 조직으로 이루어진 템프코어 조직을 구현하였다. 실험장치는 현장 설비와 동일한 Cooler 1 기가 장착되었고, 12~13 bar 의 압력과 최대 $50m^3/h$의 유량을 공급하는 펌프라인으로 구성되어 있다. 항복강도를 기준으로 400 MPa 이상을 요구하는 강종인 SD400 모사 결과 경화층 면적비 및 냉각 깊이 별 경도가 제품과 잘 일치함을 알 수 있었다.

• Corrosion Science and Technology
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• 제3권4호
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• pp.140-147
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• 2004

High temperature oxidation of Fe-19Cr and Fe-19Cr-0.2Ti alloys is studied at 1173-1373 K in 16.5 kPa $O_2$ - balances $N_2$ atmosphere aimed at clarifying the effect of titanium addition. Oxidation rate of Fe-19Cr alloy was accelerated with titanium. For both alloys chromium rich $(Fe,\;Cr)_2O_3$ was formed as a major oxidation product. On Fe-19Cr-0.2Ti alloy, a thin layer composed of spinel type oxide and titanium oxide was also formed and an internal oxidation of titanium was observed. Titanium was concentrated at the oxide surface and internal oxidation zone but a small amount of titanium was also found in the intermediate corundum type $(Fe,\;Cr)_2O_3$ layer. Crystals of corundum type $(Fe,\;Cr)_2O_3$ formed on Fe-19Cr alloy are coarse but that formed on Fe-19Cr -0.2Ti alloys were fine and columnar. Reason for the difference in oxidation kinetics and crystal structure will be discussed relating to the distribution of aliovalent titanium in corundum type $(Fe,\;Cr)_2O_3$ oxide layer.

• Journal of Welding and Joining
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• 제34권1호
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• pp.75-81
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• 2016

This study applied laser surface melting process using CW(Continuous wave) Yb:YAG laser and cold-work die steel SM45C and investigated microstructure and hardness. Laser beam speed, power and beam interval are fixed at 70 mm/sec, 2.8 kW and $800{\mu}m$ respectively. Depth of Hardening layer(Melting zone) was a minimum of 0.8 mm and a maximum of 1.0 mm that exceeds the limit of minimum depth 0.5 mm applying trimming die. In all weld zone, macrostructure was dendrite structure. At the dendrite boundary, Mn, Al, S and O was segregated and MnS and Al oxide existed. However, this inclusion didn't observe in the heat-affected zone (HAZ). As a result of interpreting phase transformation of binary diagram, MnS crystallizes from liquid. Also, it estimated that Al oxide forms by reacting with oxygen in the atmosphere. The hardness of the melting zone was from 650 Hv to 660 Hv regardless of the location that higher 60 Hv than the hardness of the HAZ that had maximum 600 Hv. In comparison with the size of microstructure using electron backscatter diffraction(EBSD), the size of microstructure in the melting zone was smaller than HAZ. Because it estimated that cooling rate of laser surface melting process is faster than water quenching.

• 비파괴검사학회지
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• 제26권1호
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• pp.7-11
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• 2006

기계부품의 세라믹 코팅 층은 사용 중 그 표면특성이 변하므로 잔류수명 예측과 신뢰성 확보를 위해 비파괴적으로 세라믹 코팅 층의 특성을 평가하는 것은 매우 중요하다. 이를 위해 본 인구는 AISI 1045 강과 오스테나이트 스테인리스 304 강 모재위에 매우 얇은 TiN 세라믹 층을 코팅한 시편에 내하여 누설 레일리(Rayleigh) 표면파를 이용한 TiN 코팅부재의 특성평가를 시도하였다. 후방복사 측정기법으로 코팅 층 내의 표면파의 전파특성이 평가되었고 표면 거칠기, 코팅 층 두께, 마모조긴 둥이 다양한 시편들에 대해 후방복사 프로파일이 측정되었다. 후방복사 프로파일의 정점각과 크기는 시편의 조건들에 따라 민감하게 변하였고, 정점각의 증가는 코팅 층 접합 강도의 저하로 설명되었다. 결과들은 후방복사 기법을 이용한 표면파의 분산성 평가가 코팅 층의 특성 평가에 매우 유용함을 보여주었다.

• 한국기계가공학회지
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• 제17권4호
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• pp.76-82
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• 2018

3D formed Electrical Discharge Machining (EDM) and hole EDM were conducted for die and mold manufacturing with electrodes which were made by mechanical machining and wire EDM. It is difficult to machine the hardened material after heat treatment and quenching with traditional machining. The only method of machining hardened material is die-sinking EDM. In this research, hole EDM was conducted for heat-treated cold-worked tool steel (SKD11) for use as a die material. The EDM surfaces were analyzed by pulse-on time and peak current of EDM current, according to the machining conditions of EDM. The EDM surface profiles were affected by the peak current. The contribution of each factor is peak current (91.63%) and pulse-on time (0.93%). The best surface roughness was obtained with a $130{\mu}s$ pulse-on time and a 14.2 A peak current. With uniform EDM processing, the surface deteriorated with increasing pulse-on time and peak current. The thickness of the solidified layer induced by EDM was increased as the peak current, crater shapes, and erupted shapes of EDM surfaces were increased. Therefore, microcracking gaps induced by surface tension were increased.

• 한국표면공학회지
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• 제31권6호
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• pp.379-388
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• 1998

The iron-zinc interfacial reaction and corrosin properties in galvanizing bath containning Ni have been intestigated. The substrate steel plates were galvanized in Zn or Zn-0.018Al baths with various Ni contents. The corrosion resistance of galvanized specimens was also evaluated by $60^{\circ}$bending test for galvannealing speaaimens. The corrosion resistance was improved with Ni addition in pure Zn bath, while deteriorated with Ni addition in Zn-0.18Al bath. The anti-powdering property, on thhe otherhand, was improved with Ni addition in Zn-0.18Al bath, while deteriorated with Ni addition in pure Zn. It was found that the anti-powdering property was improved with increasing $\xi$ phase ratio in reaction layer.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2002년도 춘계학술대회 논문집
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• pp.844-847
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• 2002

This paper is to investigate the wear behavior of submerged-arc clad materials by the wear test with a ball-on-disk type wear testing machine in air. The specimens were clad with Stoody105 alloy wire on a carbon steel (SM45C) substrate by submerged-arc cladding process under different welding parameters. The wear behavior of the cladding through ball-en-disk test has been studied under the wear load from 5N to 16N and sliding speed from 8cm/s to 35cm/s. The weight of the specimen loss was measured. Scanning electron micrographs of the worn surface show a layer of oxide film formed on the worn surface. Oxidation wear mechanism controls the wear process. The spalling of the oxide is caused by the repeated rubbing fatigue mechanism.

• 한국정밀공학회지
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• 제20권1호
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• pp.179-186
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• 2003

This paper is to investigate the wear behavior of submerged-arc claddings by the wear test with a ball-on-disk type wear testing machine in air. The specimens were clad with Stoody105 alloy wire on a medium carbon steel (SM45C) substrate by submerged-arc cladding process under different welding parameters. The wear behavior of the cladding through ball-on-disk test has been studied under the wear load from 5 to 16 N and the sliding speed from 8 to 35 cm/s. The weight loss of the specimen was measured. Scanning electron micrographs of the worn surface show a layer of oxide film formed on the worn surface. Oxidation wear mechanism controls the wear process. The spatting of the oxide is caused by the repeated rubbing fatigue mechanism.