• Title/Summary/Keyword: Stainless Steels

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Pitting Corrosion Behavuor of N2+ ion Implanted AISI 316L Stainless Steel Compacts (질소 이온주입된 AiSi 316L 스테인리스강 소결체의 공식거동)

  • 최한철
    • Journal of the Korean institute of surface engineering
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    • v.31 no.2
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    • pp.73-80
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    • 1998
  • The aim of this study is to develop sintered stainless steels (SSS) with good mechanical strength, wear resistance, and corrosion resistance by nitrogen ion implantation on the Culated SSS surface. Stainless steel compacts containg Cu (2-10 wt%) were prepared by electroless Cu-pating method which results in the increased3 homogenization in alloying powder. Nitrogen ion implantation was carried out by using N2 gas as the ion source. Nitrogen ions were embedded by an acceleratol of 130keV with doese $3.0\times10^{17}\;ions/\textrm{cm}^2$ on the SSS at $25^{\circ}C$ in$2\times10^{-6}$ torr vacuum. The nitrogen ion implanted SSS obtained from anodic ploarization curves revealed higher corrosion potential than that of nitrogen ion unimplante one. And nitrogen ion implanted 316LSSS had good resistance to pitting corrosion due to the synergistic effect of Mo and N, and the inhibition of $NH_4\;^+$<\TEX>, against $CI^-$<\TEX>.

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Corrosion Resistance of Stainless Steels Analyzed by Fractal Geometry

  • Kim, Eun-Ji;Park, Su-Jin;Heo, Jung-Ho;Shin, Heon-Cheol
    • Journal of Electrochemical Science and Technology
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    • v.1 no.2
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    • pp.112-116
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    • 2010
  • Fractal property of the passivated steel surface was investigated on the basis of scaling analysis with a special focus on its relationship with corrosion resistance. For this purpose, the surface of stainless steel was intentionally oxidized under a variety of passivation conditions and its scaling property was analyzed by a triangulation method. The morphology of the passivated steel surface was satisfactorily evaluated with fractal dimension. From the chronoamperometry and impedance measurement, it proved that lower fractal dimension leads to more enhanced corrosion resistance. The higher passivity of the steel surface with lower fractal dimension was discussed in terms of active area and structural imperfection.

Relationship between Creep Characteristic Values and Rupture time in STS304 Stainless Steels (스테인리스강의 크리프 특성치와 파단시간과의 관계)

  • KONG YU-SIK;KIM SEON-JIN;LEE BAE-SUB
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2004.11a
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    • pp.228-233
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    • 2004
  • The characteristics of the probability distribution for mechanical properties, e.g. tensile strength, reduction of area ana elongation, for STS304 stainless steel in elevated temperature were investigated from tensile test performed by constant cross head speea controls with 1mm/min, Recently, in order to clarify the strengthening mechanisms at high temperature, a new scheme to improve high temperature mechanical properties is desired. Therefore, the test ,technique development of high temperature creep behaviors for this material is very important. In this paper, the creep praperties and creep life prediction by Larson-Miller parameter method for STS304 stainless steel to be used for other high temperature components were presented at the elevated temperatures of 600, 650 and $700^{\circ}C$.

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CHARACTERISTICS OF PLATED GOLD LAYER ON ANSI 304 STAINLESS STEEL ACCORDING TO THE VARIATION OF PRETREATMENTS AND ELECTROLYSIS CONDITIONS

  • Lee, Dong-hun;Lee, Jae-Bong
    • Journal of the Korean institute of surface engineering
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    • v.32 no.3
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    • pp.224-234
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    • 1999
  • An attempt was made to characterize the relationship between pretreatment processes, electrolysis conditions and behaviors of the plated gold layer. In order to investigate the effect of pretreatment processes on plating, rest potential measurements of various pretreated stainless steels and a.c.-impedance spectroscopy tests were carried out in the strike plating solution. Characteristics of plated gold layers and adhesions between plated gold layers and stainless steel substrates were examined by scratching tests and micro-Vickers hardness tests. The result shows that the strike plating enhanced the adhesion of interface, the cathodic electro-activation pretreatment process improving both corrosion resistance and adhesion strength. The preferred orientations of plated gold layers were examined by the X-ray diffraction technique. As the current density increases, [111] preferred orientation of plated gold layers was found to become well developed.

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Classification of ultrasonic signals of thermally aged cast austenitic stainless steel (CASS) using machine learning (ML) models

  • Kim, Jin-Gyum;Jang, Changheui;Kang, Sung-Sik
    • Nuclear Engineering and Technology
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    • v.54 no.4
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    • pp.1167-1174
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    • 2022
  • Cast austenitic stainless steels (CASSs) are widely used as structural materials in the nuclear industry. The main drawback of CASSs is the reduction in fracture toughness due to long-term exposure to operating environment. Even though ultrasonic non-destructive testing has been conducted in major nuclear components and pipes, the detection of cracks is difficult due to the scattering and attenuation of ultrasonic waves by the coarse grains and the inhomogeneity of CASS materials. In this study, the ultrasonic signals measured in thermally aged CASS were discriminated for the first time with the simple ultrasonic technique (UT) and machine learning (ML) models. Several different ML models, specifically the K-nearest neighbors (KNN), Support Vector Machine (SVM), and Multi-Layer Perceptron (MLP) models, were used to classify the ultrasonic signals as thermal aging condition of CASS specimens. We identified that the ML models can predict the category of ultrasonic signals effectively according to the aging condition.

Mechanical performance of additively manufactured austenitic 316L stainless steel

  • Kim, Kyu-Tae
    • Nuclear Engineering and Technology
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    • v.54 no.1
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    • pp.244-254
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    • 2022
  • For tensile tests, Vickers hardness tests and microstructure tests, plate-type and box-type specimens of austenitic 316L stainless steels were produced by a conventional machining (CM) process as well as two additive manufacturing processes such as direct metal laser sintering (DMLS) and direct metal tooling (DMT). The specimens were irradiated up to a fast neutron fluence of 3.3 × 109 n/cm2 at a neutron irradiation facility. Mechanical performance of the unirradiated and irradiated specimens were investigated at room temperature and 300 ℃, respectively. The tensile strengths of the DMLS, DMT and CM 316L specimens are in descending order but the elongations are in reverse order, regardless of irradiation and temperature. The ratio of Vickers hardness to ultimate tensile strength was derived to be between 3.21 and 4.01. The additive manufacturing processes exhibit suitable mechanical performance, comparing the tensile strengths and elongations of the conventional machining process.

The Effect of Alloying Elements and Heat Treatment on the Pitting Corrosion of 440 A Martensitic Stainless Steels (440A 강의 공식부식에 미치는 첨가원소 및 열처리의 영향)

  • Kim, Moo-Gil;Jung, Byong-Ho;Lee, Byoung-Chan
    • Journal of the Korean Society for Heat Treatment
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    • v.22 no.2
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    • pp.67-74
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    • 2009
  • 440A martensitic stainless steels which were modified with reduced carbon content (${\sim}$0.5%) and addition of small amount of nickel, vanadium, tungsten and molybdenum were manufactured. Effects of alloying elements and heat treatment on the pitting corrosion in 3.5% NaCl were investigated through the electrochemical polarization tests. The lowest pitting potential, $E_p$, was obtained when austenitizing temperature was $1250^{\circ}C$ and this is because of the grain coarsening. When austenitized at $1050^{\circ}C$ and tempered at $350{\sim}750^{\circ}C$, the highest $E_p$ was obtained at $350^{\circ}C$, while the lowest at $450^{\circ}C$ and $550^{\circ}C$ regardless of alloying elements added. But $E_p$ was increased a little at the tempering temperature of $450^{\circ}C$ and $550^{\circ}C$ when 0.4 wt.% of tungsten was added. More pitting was observed at $450{\sim}550^{\circ}C$, and pitting was formed at regions where Cr concentration is low or grain boundaries are intersecting and showed irregular shape.

A Study on the Cracking Behavior in the Welds of Ni-Cr-Fe and Ni-Fe-Cr-Mo Alloys Part I : Solidification Cracking in the Fusion Zone (Ni-Cr-Fe 및 Ni-Fe-Cr-Mo계 합금의 용접부 균열특성에 관한 연구 Part I : 용착금속의 응고균열)

  • 김희봉;이창희
    • Journal of Welding and Joining
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    • v.15 no.4
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    • pp.78-89
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    • 1997
  • This study has evaluated the weld metal solidification cracking behavior of several Ni base superalloys (Incoloy 825, Inconel 718 and Inconel 600). Austenitic stainless steels(304, 310S) were also included for comparison. In addition, a possible mechanism of solidification cracking in the fusion zone was suggested based on the extensive microstructural examinations with SEM, EDAX, TEM, SADP and AEM. The solidification cracking resistance of Ni base superalloys was found to be far inferior to that of austenitic stainless steels. The solidification cracking of Incoloy 825 and Inconel 718 was believel to be closely related with the Laves-austenite (Ti rich in 825 and Nb rich in 718) and MC-austenite eutectic phases formed along the grain boundaries during solidification. Cracking in Inconel 600 was always found along the grain boundaries which were enriched with Ti and P. Further, solidifidcation cracking resistance was dependent not only upon the type of love melting phases but also on the amount of the phases along the solidification grain boundaries.

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Effect of Grain Size on Corrosion Resistance and High Temperature Oxidation Behavior of 22Cr-15Ni-5W Super Austenitic Stainless Steels (22Cr-15Ni-5W 슈퍼 오스테나이트계(系) 스테인리스강(鋼)의 고온산화(高溫酸化) 및 내식성(耐蝕性)에 미치는 결정립(結晶粒) 크기의 영향(影響))

  • Kim, H.J.;Lee, H.W.;Lee, J.M.;Kang, C.Y.
    • Journal of Power System Engineering
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    • v.10 no.3
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    • pp.51-57
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    • 2006
  • The effect of grain size on corrosion resistance and high temperature oxidation behavior was studied in 22Cr-15Ni-5W super austenitic stainless steels for desulfurization equipment as a heat power station. In the high temperature oxidation test, oxidation rate was increased as the temperature increased from $600^{\circ}C\;to\;800^{\circ}C$. In vapor, oxidation rate was faster than that in air. Because the vapor was inhibited nucleation of $Cr_2O_3$ film. And the high temperature oxidation resistance at $600^{\circ}C{\sim}800^{\circ}C$ was excellent from all specimens and specimen of the smallest grain size was the most excellent. Because increasing of diffusion course through the grain-boundary was promoted nucleation and growth of $Cr_2O_3$ film. In the test temperature at $600^{\circ}C{\sim}800^{\circ}C$, Cr rich round particle oxide was formed in air, whereas Fe rich needle type oxide was developed in vapor.

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A study on the influence of process parameters during laser welding of sheet steels (강판의 레이저 용접시 공정변수의 영향에 관한 연구)

  • Park, Young-Soo;Lee, Yoon-Sik;Kim, Hyung-Sik;Kim, Chan
    • Laser Solutions
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    • v.2 no.3
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    • pp.11-18
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    • 1999
  • This paper describes the weldability of carbon steel and stainless steel using 5㎾ $CO_2$ laser system with nearly multi-mode beam and a parabolic focusing mirror. In the laser welding of steels, major welding parameters are focal point, travel speed, beam power, shield gas and gap tolerance, etc.. Two kinds of gases(Ar, He) were used as a assist gas and supplied through the external nozzle. It is very important for optimum condition to remove plasma plume which absorbs laser beam and to obtain deep penetration and sound weld bead. Bead-on-plate welding tests were carried out for the experiments. Penetration data were obtained with various welding parameters and the effects of welding parameters were discussed. Butt welding tests were performed with various conditions. Only the optimum laser parameters assured good weld quality As a result of this study, We achieve the fundamental weldabilities using a high power $CO_2$ laser for carbon steel and stainless steel.

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