• Title/Summary/Keyword: Stacking fault energy

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Strain-rate Effect on Tensile Properties of High-nitrogen Austenitic Stainless Steel (고질소 오스테나이트계 스테인리스강의 인장물성에 미치는 변형속도의 영향)

  • S. H. Lee;D. W. Kim;Y. G. Kim;J.-H. Kang
    • Transactions of Materials Processing
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    • v.33 no.5
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    • pp.322-329
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    • 2024
  • Because a high strain rate suppresses cross slip and delays dynamic recovery in the alloys with a face-centered cubic (FCC) structure, it is generally accepted that the influence of strain rate on strain hardening rate and tensile strength is greater than that on the yield strength of FCC alloys. The present study examined the tensile behavior of an austenitic stainless steel exhibiting an FCC structure, and revealed that the increment in yield strength was greater than that in tensile strength as the strain rate increased from 5.21×10-5s-1 to 4.17×10-1s-1. This indicated that the strain hardening rate was reduced by increasing the strain rate, which was inconsistent with the conventional explanation. Adiabatic heating was detected at high strain rates from 5.21×10-5s-1, and the resulting temperature increase could elevate stacking fault energy. The tendency for sip planarity was investigated by applying the Ludwigson model to the tensile curves, which suggested that higher stacking fault energy due to adiabatic heating could accelerate cross slip and dynamic recovery, thereby reducing the strain hardening rate.

The Effect of Vandium on the microstructure and Elevated Temperature Sliding Wear Resistance of Fe-20Cr-1.7C-1Si-xV Hardfacing Alloy (Fe-20Cr-1.7C-1Si-xV 경면처리 합금의 미세조직과 고온 Sliding 마모저항성에 미치는 Vanadium의 영향)

  • Kim, Jun-Gi;Kim, Geun-Mo;Lee, Deok-Hyeon;Jang, Se-Gi;Gang, Seong-Gun;Kim, Seon-Jin
    • Korean Journal of Materials Research
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    • v.8 no.10
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    • pp.969-974
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    • 1998
  • The effect of vanadium, which is known to decrease the stacking fault energy of Fe-base alloys, on the microstructure and elevated temperature sliding wear resistance of Fe-20Cr- 1.7C- 1Si alloy was investigated. The maximum amount of vanadium maintaining the austenitic matrix seems to be about 3wt.% in Fe-20Cr- 1.7C-1Si-xV (x = 0, 1, 3, 6. lOwt.%) alloys and the austenitic alloys showed better wear resistance than ferritic alloys. It was considered to be due to the low stacking fault energy and $\gamma->\alpha$ strain-induced phase transformation at rmm temperature. It was shown from elevated temperature sliding tests up to .$225^{\circ}C$ that the addition of vanadium increases the temperature, at which the transition from oxidative wear to adhesive wear occur, and the amount of d formed at $225^{\circ}C$. Thus, it was considered that the addition of vanadium improves the elevated temperature sliding wear resistance of Fe-20Cr- 1.7C - 1Si by reducing the increasing rate of stacking fault energy with temperature and by increasing Ma temperature.

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Nano-Scale Surface Observation of Cyclically Deformed Copper and Cu-Al Single Crystals (반복변형된 동 및 동알루미늄 단결정 표면형상의 나노-스케일 관찰)

  • ;;Hitoshii ISHII
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1999.06a
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    • pp.67-72
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    • 1999
  • Scanning probe Microscope(SPM) such as Scanning Tunneling Microscope(STM) and Atomic Force Microscope(AFM) was shown to be the powerful tool for nano-scale characterization of material surfaces Using this technique, surface morphology of the cyclically deformed Cu or Cu-Al single crystal was observed. The surface became proportionately rough as the number of cycles increased, but after some number of cycles no further change was observed. Slip steps with the heights of 100 to 200 nm and the widths of 1000 to 2000 nm were prevailing at the stage. The slipped distance of one slip system at the surface was not uniform. and formation of the extrusions or intrusions was assumed to occur such place. By comparing the morphological change caused by crystallographic orientation, strain amplitude, number of cycles or stacking fault energy, some interesting results which help to clarify the basic mechanism of fatigue damage were obtained. Furthermore, applicability of the scanning tunneling microscopy to fatigue damage is discussed.

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A High-Resolution Transmission Electron Microscopy Study on the Lattice Defects Formed in the High Energy P Ion Implanted Silicon (고에너지 P이온 주입한 실리콘에 형성된 격자 결함에 관한 고분해능 투과전자현미경 연구)

  • 장기완;이정용;조남훈;노재상
    • Journal of the Korean Ceramic Society
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    • v.32 no.12
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    • pp.1377-1382
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    • 1995
  • A high-resolution transmission electron microscopy study on the lattice defects formed in the high energy P ion implanted silicon was carried out on an atomic level. Results show that Lomer dislocations, 60$^{\circ}$perfect dislocations, 60$^{\circ}$ dislocation dipole and extrinsic stacking fault formed in the near Rp of as-implanted specimen. In the annelaed specimens, interstitial Frank loops, 60$^{\circ}$perfect disolations, 60$^{\circ}$dislocation dipoles, stacking faults, precipitates, perfect dislocation loops and <112> rodlike defects existed exclusively near in the Rp with various annealing temperature and time. From these results, it is concluded that extended secondary defects as well as the point defect clusters could be formed without annealing. Even at low temperature annealing such as 55$0^{\circ}C$, small interstitial Frank loops could be formed and precipitates were also formed by $700^{\circ}C$ annealing. The defect band annealed at 100$0^{\circ}C$ for 1 hr could be divided into two regions depending on the distribution of the secondary defects.

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Atomic structures and Energies of Planar defects in w-GaN (GaN 평면결함의 구조와 형성에너지에 관한 연구)

  • Moon, Won-Ha;Choi, Chang-Hwan
    • Proceedings of the IEEK Conference
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    • 2006.06a
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    • pp.567-568
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    • 2006
  • We investigate the structures and the formation energy of inversion domain boundaries (IDBs) using the Tersoff empirical potential. Four kinds of IDBs ( A and B types for IDB* and Holt ) are considered. The IDBs with A type are energetically favorable compared to B type with the structural instability. The IDB* is also more stable than the Holt type in spite of fourfold and eightfold rings of bonds. We calculate the atomic configurations of the Holt IDBs induced by the interactions of the IDB* with the stacking faults $I_1$ and $I_2$. The stacking fault $I_2$ interacted with $I_1$ on the IDB induces the structural transformation from IDB* to Holt type.

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Effect of Mn-Addition on the Sliding Wear Resistance and the Cavitation Erosion Resistance of Fe-base Hardfacing Alloy (Mn 첨가가 경면처리용 Fe계 신합금의 캐비테이션 에로젼과 슬라이딩 마모저항성에 미치는 영향)

  • Kim, Yoon-Kap;Oh, Young-Min;Kim, Seon-Jin
    • Korean Journal of Materials Research
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    • v.12 no.7
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    • pp.550-554
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    • 2002
  • The effect of Mn on cavitation erosion resistance and the sliding wear resistance of Fe-base hardfacing NewAlloy was investigated. Mn is known to decrease stacking fault energy and enhance the formation of $\varepsilon$-martensite. Cavitation erosion resistance for 50 hours and sliding wear resistance for 100 cycles were evaluated by weight loss. Fe-base hardfacing NewAlloy showed more excellent cavitation erosion resistance than Mn-added NewAlloys. $\Upsilon-\alpha$' phase transformation that can enhance erosion resistance by matrix hardening occurred in every specimens. But, only in Mn free Fe-base hardfacing NewAlloy, the hardened matrix could repress the propagation of cracks that was initialed at the matrix-carbides interfaces more effectively than Mn-added NewAlloy The Mn free Fe-base hardfacing NewAlloy showed better sliding wear resistance than Mn-added alloys. Mn-addition up to 5wt.% couldn't increase the sliding wear and cavitation erosion resistance of Fe-base hardfacing alloy because it didn't make $\Upsilon\to\varepsilon$ martensite phase transformation. Therefore, it is considered that the cavitation erosion and the sliding wear resistance can be improved due to $\Upsilon\to\varepsilon$ martensite phase transformation when Mn is added more than 5wt.% in Fe-base hardfacing alloys.

The development of deformation microstructures and textures in high Mn steels (고Mn강의 소성에 따른 미세조직및 Texture 변화에 관한연구)

  • Kim, Taek-Nam;Kim, Jong-Ok
    • The Journal of Natural Sciences
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    • v.7
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    • pp.83-90
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    • 1995
  • The microstructural and textural development during rolling is compared in two Hadifield's steels (high Mn steel), one having low carbon content (0.65 wt.%) and the other high carbon (1.35 wt.%).In low carbon Hadfield's steel (LCHS) mixed microstructures are formed which contain intrinsic stacking faults, deformation twins, and brass type shear bands. The deformation twins are thought to be formed by the stacking of intrinsic stacking faults. The similar development to 70-30 brass texture is observed in early deformation. However the abnormal texture is developed after 40 % deformation, which is thought to be due to the martensite phase transformation. In high carbon Hadfield's steel (HCHS) mixed substructures of dislocation tangles, deformation twins, and shear bands (both copper and brass type) are found to develop. The texture development is similar to that of 70-30 brass. This is consistant with no carbon segregation and no martensitic phase transformation in HCHS. In spite of the difference of substructure and texture development during rolling in two steels, the difference in stacking fault energy is measured to be small ($2 mJm^-2$). The carbon segregation is only occurred in LCHS. Thus it is thought that the carbon segregation influence the microstructure and texture development during rolling. This is related with martensite phase transformation in LCHS.

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Structural characterization of nonpolar GaN using high-resolution transmission electron microscopy (HRTEM을 이용한 비극성 GaN의 구조적 특성 분석)

  • Kong, Bo-Hyun;Kim, Dong-Chan;Kim, Young-Yi;Ahn, Cheol-Hyoun;Han, Won-Suk;Choi, Mi-Kyung;Bae, Young-Sook;Woo, Chang-Ho;Cho, Hyung-Koun;Moon, Jin-Young;Lee, Ho-Seong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.23-23
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    • 2009
  • GaN-based nitride semiconductors have attracted considerable attention in high-brightness light-emitting-diodes (LEDs) and laser diodes (LDs) covering from green to ultraviolet spectral range. LED and LD heterostructures are usually grown on (0001)-$Al_2O_3$. The large lattice mismatch between $Al_2O_3$ substrates and the GaN layers leads to a high density of defects(dislocations and stacking faults). Moreover, Ga and N atoms are arranged along the polar [0001] crystallographic direction, which leads to spontaneous polarization. In addition, in the InGaN/GaN MQWs heterostructures, stress applied along the same axis can also give rise to piezoelectric polarization. The total polarization, which is the sum of spontaneous and piezoelectric polarizations, is aligned along the [0001] direction of the wurtzite heterostructures. The change in the total polarization across the heterolayers results in high interface charge densities and spatial separation of the electron and hole wave functions, redshifting the photoluminescence peak and decreasing the peak intensity. The effect of polarization charges in the GaN-based heterostructures can be eliminated by growing along the non-polar [$11\bar{2}0$] (a-axis) or [$1\bar{1}00$] (m-axis) orientation instead of thecommonly used polar [0001] (c-axis). For non-polar GaN growth on non-polar substrates, the GaN films have high density of planar defects (basal stacking fault BSFs, prismatic stacking fault PSFs), because the SFs are formed on the basal plane (c-plane) due to their low formation energy. A significant reduction in defect density was recently achieved by applying blocking layer such as SiN, AlN, and AlGaN in non-polar GaN. In this work, we were performed systematic studies of the defects in the nonpolar GaN by conventional and high-resolution transmission electron microscopy.

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Evaluation of Microscopic Degradation of Copper and Copper Alloy by Electrical Resistivity Measurement (전기비저항 측정에 의한 구리와 구리합금의 미시적 열화평가)

  • Kim, Chung-Seok;Nahm, Seung-Hoon;Hyun, Chang-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.5
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    • pp.444-450
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    • 2010
  • In the present study, the microscopic degradation of copper and copper alloy subjected to cyclic deformation has been evaluated by the electrical resistivity measurement using the DC four terminal potential method. The copper (Cu) and copper alloy (Cu-35Zn), whose stacking fault energy is much different each other, were cyclically deformed to investigate the response of the electrical resistivity to different dislocation substructures. Dislocation cell substructure was developed in the Cu, while the planar array of dislocation structure was developed in the Cu-35Zn alloy increasing dislocation density with fatigue cycles. The electrical resistivity increased rapidly in the initial stage of fatigue deformation in both materials. Moreover, after the fatigue test it increased by about 7 % for the Cu and 6.5 % for the Cu-35Zn alloy, respectively. From these consistent results, it may be concluded that the dislocation cell structure responds to the electrical resistivity more sensitively than the planar array dislocation structure evolved during cyclic fatigue.

Sliding wear of Inconel 600 and 690 in room temperature air (상온 대기 중에서 인코넬 600과 690의 슬라이딩 마모)

  • 홍동석;김경국;김준기;김선진
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.11a
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    • pp.91-91
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    • 2003
  • Sliding wear behaviors of Inconel 600 and 690 were investigated at room temperature in air. In the present study, Archard's equation which has low reliability was modified. In the prediction of wear volume by Archard's equation, the reliabilities of Inconel 600 and 690 were about from 26.3% to 45.7% and from 69. l% to 88.6%, respectively, The sliding wear behaviors of Inconel 600 and 690 turned out to be influenced by their stacking fault energy, and the fact was confirmed by using TEM and micro-hardness test Based on experimental results, the wear coefficient was modified as a function of the sliding distance. The calculation with the modified wear equation showed that the reliability of Inconel 600 tested with 409 ferritic stainless steel increased from 45.7% to 93.4%.

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