• Title/Summary/Keyword: Speed sintering

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Machinability Evaluation of Endmill Tool through Development of Ultra-fine Grain Grade Cemented Tungsten Carbide Material (초미립 초경소재 개발을 통한 엔드밀 공구의 성능 평가)

  • 김홍규;서정태;권동현;김정석;강명창
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.865-869
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    • 1997
  • In recent years, there has been increasing demand of ultra-fine grain graded cemented tungsten carbide material with high hardness and toughness which is used as high speed cutting tool for development in semiconductor, electronics and die/mold industry, which bring into limelight high-precision, high-efficient machining of sculptured surfaces. This paper deals with the performance of variation in the ultra-fine grain graded cemented tungsten carbide material such as grain size, hardness and density varied according to the volume of added elements, Co or TaC, and he changing of mixing, sintering process. Also, the performance of developing material with uniformed grain size of 0.5${\mu}{\textrm}{m}$ is compared with other domestics' & foreign companies' with analyzing and cutting performance testing.

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Compaction of Ultra-fine WC Powder by High-Speed Centrifugal Compaction Process

  • Suzuki, Hiroyuki Y.;Kadono, Yuichi;Kuroki, Hidenori
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.24-25
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    • 2006
  • High-Speed Centrifugal Compaction Process is one of slip-using compacting method originally developed for processing of oxide ceramics. In this study, we apply the HCP to ultra-fine (0.1 micron) WC powder. Organic liquid of heptane was chosen as dispersing media to avoid possible oxidation of WC. The mixing apparatus was a key to obtain dense compacts. Only the slips mixed by high energy planetary ball mill were packed up to 55% by the HCP, and sintered to almost full density at 1673 K without any sintering aids. This sintered compact marked Vickers hardness of Hv 2750 at maximum.

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Aeroelastic tailoring using crenellated skins-modelling and experiment

  • Francois, Guillaume;Cooper, Jonathan E.;Weaver, Paul M.
    • Advances in aircraft and spacecraft science
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    • v.4 no.2
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    • pp.93-124
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    • 2017
  • Aeroelastic performance controls wing shape in flight and its behaviour under manoeuvre and gust loads. Controlling the wing‟s aeroelastic performance can therefore offer weight and fuel savings. In this paper, the rib orientation and the crenellated skin concept are used to control wing deformation under aerodynamic load. The impact of varying the rib/crenellation orientation, the crenellation width and thickness on the tip twist, tip displacement, natural frequencies, flutter speed and gust response are investigated. Various wind-off and wind-on loads are considered through Finite Element modelling and experiments, using wings manufactured through polyamide laser sintering. It is shown that it is possible to influence the aeroelastic behaviour using the rib and crenellation orientation, e.g., flutter speed increased by up to 14.2% and gust loads alleviated by up to 6.4%. A reasonable comparison between numerical and experimental results was found.

Effects of Pre-Sintering Surface Treatment and Liner Application on the Shear Bond Strength of Zirconia and Pressable Ceramic (소결 전 지르코니아 표면처리와 라이너 사용에 따른 지르코니아와 열가압성형도재의 전단결합강도)

  • Lee, Gwang-Young;Cho, Mi-Hyang;Choi, Sung-Min
    • Journal of Technologic Dentistry
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    • v.37 no.3
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    • pp.121-127
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    • 2015
  • Purpose: This study was intended to investigate the effect of applying liner for chemical bonding and physical surface roughness created on zirconia by using a sandpaper before sintering on the bond strength between the two materials. Methods: Zirconia blocks were cut using a low-speed cutter. Plate-shaped specimen($6mm{\times}6mm{\times}3mm$) was fabricated by sintering after giving surface roughness according to four kinds of sandpapers. Depending on whether or not to use liner, 60 specimens were divided into two groups ZN(non-liner), ZL(liner), and the two groups were subdivided into four groups respectively in accordance with sandpaper used, totaling eight groups (n=10). The surface roughness (Ra) values and shapes before sintering were observed, and shear bond strength after pressing ceramic plasticity was measured with a universal testing machine. For a test of the significance, a one-way ANOVA was performed, and Tukey's multiple comparison test was conducted. Results: The observation of the surface roughness was SB04($2.22{\pm}1.16{\mu}m$), SB08($2.98{\pm}0.33{\mu}m$), SB12($2.44{\pm}1.32{\mu}m$), SB20($2.34{\pm}0.59{\mu}m$) and SA04($2.34{\pm}0.67{\mu}m$), SA08($1.28{\pm}0.90{\mu}m$), SA12($2.03{\pm}1.60{\mu}m$), SA20($2.19{\pm}1.73{\mu}m$). In the case of ZN Group, the shear bond strength was ZN04($23.26{\pm}3.83MPa$), ZN08($21.76{\pm}2.33MPa$), ZN12($20.49{\pm}3.01MPa$), ZN20($24.98{\pm}4.22MPa$)(p<0.05). As for ZL Group, the shear bond strength was ZL04($25.09{\pm}5.67MPa$), ZL08($22.98{\pm}2.26MPa$), ZL12($21.54{\pm}5.70MPa$), ZL20($23.98{\pm}3.23MPa$)(p<0.05). Conclusion: The research results showed that the bond strength of Zirconia core and Pressing ceramic was further improved by physical surface treatment before sintering, rather than by chemical bonding through liner surface treatment.

SrAl2Si2O8 ceramic matrices for 90Sr immobilization obtained via spark plasma sintering-reactive synthesis

  • Papynov, E.K.;Belov, A.A.;Shichalin, O.O.;Buravlev, I. Yu;Azon, S.A.;Golub, A.V.;Gerasimenko, A.V.;Parotkina, Yu. А.;Zavjalov, A.P.;Tananaev, I.G.;Sergienko, V.I.
    • Nuclear Engineering and Technology
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    • v.53 no.7
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    • pp.2289-2294
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    • 2021
  • In the present study, an original spark plasma sintering-reactive synthesis (SPS-RS) method for minerallike ceramic materials based on SrAl2Si2O8 feldspar-like skeleton structure was used for the first time, promising solid-state matrices for reliable immobilization of high-energy 90Sr. The method is based on the "in-situ" reaction of a mixture of SrO, Al2O3 and SiO2 oxides when heated by a unipolar pulsed current under compacting pressure. The phase and elemental composition structure were studied. The dynamics of the consolidation of the reaction mixture of oxides was studied in the range of 900-1200 ℃. The study found the temperature of the high-speed (minutes) SPS-RS formation of single-phase SrAl2Si2O8 composition ceramic in the absence of intermediate reaction products with a relative density of up to 99.2% and compressive strength up to 145 MPa and a strontium leaching rate of 10-4g/cm2·day.

A Study on the Industrial Type SFF System using SLS Proecss (SLS 공정을 이용한 산업용 임의형상 제작시스템에 관한 연구)

  • 김동수;임현의;김성종
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1299-1302
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    • 2004
  • A real object duplication system (RODS), including three dimensional (3D) scanner and solid freeform fabrication system (SFFS), is a device to make three-dimensional objects directly from the drawing or photo data. A Selective Multi-Laser Sintering (SMLS) process designed in this paper is by which computer images received using 3D scanner are built up from polymer powder on building room of large size using dual laser at industrial type SFF system. Using the process can rapidly produce real object duplication components of industrial type such as cylinder, engine block, chassis of automobile, etc. In this paper, the industrial type SFF system using SMLS process is manufactured and the system is satisfied with high precision and high speed processing technique. To research characteristics of each part for theindustrial type SFF system, a structure and thermal analysis and test of each part is carried out. Also, to achievement of high performance for industrial type SFF system, design and fabrication for the structure, heater, nitrogen supply, laser and control part are carried out.

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A Study on the Grinding Characteristics of AlNs Produced by Different Sintering Techniques (소결방법에 따른 질화알루미늄의 연삭 가공 특성에 관한 연구)

  • Cho, Jun-Hyun;Lee, Sang-Min;Moon, Dong-Ju;Lee, Jong-Chan;Jung, Jae-Keuk;Huh, Chan
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.13 no.2
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    • pp.94-99
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    • 2014
  • In this study, using AlN materials produced by two different sintering techniques, grinding experiments were performed under various grinding conditions, including different table speeds and cut depths. In order to measure the grinding force, a tool dynamometer was used. Surface roughness measurements and a digital microscope were also was used. The grinding forces were higher at a higher table speed and a higher cut depth. The experimental results show that the grinding characteristics of the two workpieces are similar.

Electrical Properties of Multilayer Chip Varistors in the Response Surface Analysis (반응표면분석법에 의한 적층 칩 바리스터의 전기적 특성)

  • Yoon, Jung-Rag;Jeong, Tae-Seok;Choi, Keun-Mook;Lee, Seok-Weon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.6
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    • pp.496-501
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    • 2007
  • In order to enhance sintering characteristics on the $ZnO-Pr_6O_{11}$ based multilayer chip varistors (MLVs), a response surface analysis using central composite design method were carried out. As a result, varistor voltage($V_{1mA}$), nonlinear coefficient ($\alpha$), leakage current ($I_L$) and capacitance (C) were considered to be mainly affected by sintered temperature and holding time. MLVs sintered at $1200^{\circ}C$ and above $1200^{\circ}C$ revealed poor electrical characteristics, possibly due to the reaction between electrode materials(Pd) and $ZnO-Pr_6O_{11}$ based ceramics. On the sintering temperature range $1150{\sim}1175^{\circ}C$, nonlinear coefficient ($\alpha$) and leakage current ($I_L$) were shown to be $60{\sim}69$ and below $0.3{\mu}A$, respectively. In particular, MLVs sintered at $1175^{\circ}C$, 1.5 hr and $2^{\circ}C/hr$ (cooling speed) showed stable ESD(Electrical Static Discharge) characteristics under the condition of 10 times at 8 Kv with deviation varistor voltage, and deviation nonlinear coefficient were 0.3% and 0.33% (at positive), 0.55% (at negative), respectively.

Measurement of the intrinsic speed of sound in a hot melt ceramic slurry for 3D rapid prototyping with inkjet technology (3차원 잉크젯 쾌속 조형법을 위한 세라믹 상변화 잉크의 음속측정)

  • Shin, Dong-Youn
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.4
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    • pp.892-898
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    • 2008
  • 3D rapid prototyping is the manufacturing technology to fabricate a prototype with the data stored in a computer, which differs from conventional casting technology in terms of an additive process. Various 3D rapid prototyping techniques such as stereolithograpy. fused deposition modeling. selective laser sintering, laminated object manufacturing have been developed but among them, 3D inkjet printing has a unique feature that materials could be jetted to directly form the body of a prototype, which could be a finished product functionally and structurally. However, this needs ink with a high solid content, which tends to increase the dynamic viscosity of ink. The increase of ink viscositytends to restrict the jettable range of ink and hence the jetting conditions should be optimized. The intrinsic speed of sound in a hot melt ink with ceramic nanoparticles dispersed is one of key components to determine the jettable range of ink. In this paper, the way to measure the intrinsic speed of sound in a hot melt ceramic ink is proposed and its influence on the jetting condition is discussed.

Metal Nano Powders as a New Getter Material (새로운 게터소재로서의 금속 나노 분말)

  • Kim, Won-Baek;Park, Je-Shin;Suh, Chang-Youl;Chang, Han-Kwon;Lee, Jae-Chun;Park, Mi-Young
    • Journal of Powder Materials
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    • v.14 no.1 s.60
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    • pp.56-62
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    • 2007
  • Getter property of nano-sized metallic powders was evaluated as a possible candidate for the future getter material. For the purpose, Ti powders of about 50 nm were prepared by electrical wire explosion. Commercial Ti powders of about 22 micrometer were tested as well for comparison. The room-temperature hydrogen-sorption speed of nano-sized Ti powders was $1.34\;L/sec{\cdot}cm^{2}$ which was more than 4 times higher than that of micron-sized ones. The value is comparable to or even higher than those of commercial products. Its sorption speed increases with activation temperature up to $500^{\circ}C$ above which it deteriorates due to low-temperature sintering effect of nano-sized particles.