• 한국세라믹학회지
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• 제11권2호
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• pp.3-10
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• 1974

For the manufacture of the silver-yellow glass, silver nitrate was used as a colorant in the base glass of $K_2O$-CaO-$SiO_2$ system. The latter in which the optimum condition was revealed showing beautiful yellow color had been selected among others after the preparatory studies to choose base glass. Other base glass systems considered were $Na_2O$-CaO-$SiO_2$, $R_2O$-PbO-$SiO_2$ and $R_2O$-PbO-BaO-$SiO_2$. The color developed on the specimen in various conditions was examined, using spectorphotometer, in term of the changes in absorbance with wavelength in the visible range. Experimental variables were the amount of the colorant and the additives, reheating temperature and time. The additives such as ZnO, BaO, $B_2O_3$ and $As_2O_3$ were added to increase the coloring action. It was observed that as the amount of silver increased in the base glass the absorbance around $410{\mu}m$ showed the increasing tendency, but the width of absorption curve was wider. Hence, the optimum amount of silver appeared to be 0.11~0.12%. It was found that ZnO was effective additive when present about 0.1%, while $As_2O_3$ ineffective rather retarding the coloration. Borax and $BaCO_3$ were proved effective when contained separately, but appeared ineffective when coexisted. Proper reheating temperature and time was ranged 550~$580^{\circ}C$ and 50~60 minutes. The higher the reheating temperature and the longer the reheating time, the absorbance was increased, while the width of absorption curve was wider. The colored glass prepared in the present experimental condition was found to have good water-resistance for the decorative purpose.

• Tribology and Lubricants
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• 제33권2호
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• pp.59-64
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• 2017

This study investigates friction and wear characteristics of anodized aluminum (Al) alloy 6061 by using a reciprocating tribotester. The diameter and height of the specimen are 30 mm and 10 mm, respectively. The surface roughness of the mirrored-surface is approximately $0.01{\sim}0.02{\mu}m$, and it is used throughout the current study. As a result of anodizing, the depth and diameter of the nanopore are approximately $25{\mu}m$ and 30-40 nm, respectively. The testing conditions are as follows: loads of 1, 3, and 5 N; a frequency of 1 Hz; a stoke of 3 mm; and a duration of 1800 s. We use deionized water with a volume of approximately $25{\mu}l$, as the lubricant. Micro Vickers hardness measurements show that mirrored-surface specimens had lower hardness values than anodized specimens. Further, their coefficients of friction are lower than those of the anodized samples, and the width of their wear track increases with load, as expected. The anodized specimens' coefficients of friction increase with stable frictional behavior and exhibit insignificant load dependence. Further, we observe that the width of the wear track is less than that of the mirrored-surface specimens, and micro cracks are present near it. Moreover, the anodizing process increases the hardness of the samples, improving their wear resistance. These results indicate that nanoporous structures are not effective in lowering friction under the water-lubricated condition.

• 한국건설순환자원학회논문집
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• 제9권3호
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• pp.375-382
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• 2021

자기치유 콘크리트는 직접적인 보수보강 없이도 스스로 구조물의 균열을 치유하여 효율적으로 콘크리트 구조물의 수명연장이 가능하다는 측면에서 각광받고 있다. 현재 자기치유 콘크리트는 전 세계적으로 활발히 연구가 진행되고 있는 분야이지만 대부분의 연구는 치유 성능의 향상에 초점을 맞추고 있기 때문에 객관적으로 치유성능을 평가하는 방법은 부족한 실정이다. 자기치유 콘크리트의 성능평가에 활용하기 위해 기체확산실험 방법이 개발된 바가 있지만, 시편의 포화도 및 실험시의 온습도 등과 같은 환경조건의 통제가 필요하다는 단점이 있다. 따라서 본 연구에서는 기체 확산 실험시에 필요한 환경조건을 대폭 완화하여 적용성을 향상시키고자 하였다. 아울러 실험시간을 단축시키고자 사전 안정화 과정을 도입하였고, 약 20분이내의 실험시간에서 3%이내의 오차 수준으로 균열폭의 추정이 가능하였다.

• 열처리공학회지
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• 제17권4호
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• pp.223-229
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• 2004

The effects of the cooling and annealing conditions on the microstructures and corrosion properties were investigated for the Cu-contained Zr-Nb alloy (Zr-1.1Nb-0.07Cu). After annealing at $1050^{\circ}C$ for 15 min, the specimens were cooled by three methods of water quenching, air cooling, and furnace cooling. Widmanstatten structures were developed in both air- and furnace-cooled specimens, and the Widmanstatten plate width of the furnace-cooled specimens was wider than that of the air-cooled ones. The weight gain in the furnace-cooling case was higher than that in the air-cooling case. This could be the reason why the diffusion time was more enough during the furnace cooling than the air cooling. The oxide of the furnace-cooled specimen was nonunformly formed just beneath the Widmanstatten plate boundaries, where ${\beta}_{Zr}$ phases were exised concentrately. Compared with the $640^{\circ}C$ annealing after the water quenching, the $570^{\circ}C$ annealing could make the ${\beta}_{Nb}$ phases and a concomitant reduction of the Nb in the matrix, and then it could improve the corrosion resistance with the increase of the annealing time. It would be concluded that the corrosion resistance of the Zr-1.1Nb-0.07Cu was good when the Nb concentration in the matrix was reached at an equilibrium level and then the ${\beta}_{Nb}$ phase was formed.

• 한국건축시공학회지
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• 제12권4호
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• pp.377-385
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• 2012

In this study, the Impact resistance of steel fiber and organic fiber reinforced concrete and mortar was evaluated and the improvement in toughness resulting from an increase in compressive strength and mixing fiber for impact resistance on performance was examined. The types of fiber were steel fiber, PP and PVA, and these were mixed in at 0.1, 0.5 and 1.0 vol.%, respectively. Impact resistance is evaluated with an apparatus for testing impact resistance performance by high-speed projectile crash by gas-pressure. For the experimental conditions, Specimen size was $100{\times}100{\times}20$, 30mm ($width{\times}height{\times}thickness$). Projectile diameter was 7 and 10 mm and impact speed is 350m/s. After impact test, destruction grade, penetration depth, spalling thickness and crater area were evaluated. Through this evaluation, it was found that as compressive strength is increased, penetration is suppressed. In addition, as the mixing ratio of fiber is increased, the spalling thickness and crater area are suppressed. Organic fibers have lower density than the steel fiber, and population number per unit area is bigger. As a result, the improvement of impact resistance is more significant thanks to dispersion and degraded attachment performance.

• 대한기계학회논문집A
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• 제25권7호
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• pp.1064-1072
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• 2001

It is very important to evaluate material degradation like temper and carbide embrittlements to secure the reliable and efficient operational conditions and to prevent brittle failure in service. The extent of material deterioration can be accurately evaluated by mechanical test such as impact test or creep test. But it is almost impossible to sample a large specimen from in-service plants. Thus, the material degradation evaluation by a non-destructive method is earnestly required. Recently the non-destructive test technique which uses the grain boundary etching characteristics owing to the variation of material structures has been proposed. However the program for material degradation evaluation using the grain boundary etching method(GEM) in Windows 98 domain doesnt be developed now. The aims of this paper are to develop the program and to complete the new master curve equations for the evaluation of material degradation on in-serviced high temperature components.

• 한국구조물진단유지관리공학회 논문집
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• 제16권5호
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• pp.121-128
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• 2012

이 논문에서는 대표적 수치해석에의 균열처리 방법으로 손상모델 기반의 분산균열모델을 체택하여 구조내력을 산정하였다. 또한 전력구 구조물의 실구조 모델링을 위해 3차원 해석방법을 택하였으며 3차원 콘크리트 구성모델로는 현재 3차원 모델중 콘크리트의 다축압축, 인장균열을 효과적으로 모사하는 미소면 모델(Microplane model)을 재료모델로 사용하여 비선형 유한요소해석을 수행하였다. SFRC의 인장연화곡선을 얻기 위해 역해석법을 사용하였으며, 역해석으로 구한 인장연화곡선이 실험결과와 아주 잘 일치함을 보였다. 하중-균열폭 관계를 입력값으로 사용한 역해석 결과와 하중-CMOD 관계를 사용한 역해석 결과는 서로 잘 일치하는 경향을 나타냈다. 이 논문에서는 실험으로부터 측정된 균열폭 데이터와 수치해석시의 손상지수와의 관계를 도출하여으며, 이와 같은 결과는 향후 균열탐사를 통한 구조물의 잔존 구조내력 산정에 적용할 수 있으리라 판단된다.

• 한국자동차공학회논문집
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• 제24권4호
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• pp.425-431
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• 2016

The usage of Friction Stir Welding(FSW) technology has been increasing in order to reduce the weight in automobile industries. Previous studies that investigated on the FSW have focused on the aluminum alloy. In this study, Al6061-T6 alloy plates having 5 mm of thickness were welded under nine different conditions from three tool rotation speeds: 900, 1000 and 1100 rpm, and three feed rates: 270, 300 and 330 mm/min. Specimen size of Micro Shear Punch(MSP) test was $10{\times}10{\times}0.5mm$. The mechanical properties were evaluated by MSP test and Analysis of Variance (ANOVA). The specimens were classified by advancing side(AS), retreating side(RS), and center(C) of width of tool shoulder. The optimal welding condition of FSW based on micro strengh was obtained when the tool rotation speed was 1100 rpm and the feed rate was 300 mm/min. The maximum load measured AS, RS, and C in the weldment was measured 554.7 N, 642.9 N, and 579.2 N, respectively.

• 한국구조물진단유지관리공학회 논문집
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• 제19권4호
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• pp.75-82
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• 2015

이 논문에서는 철근으로 보강한 고인성 섬유복합체(ECC) 기둥의 반복이력거동을 연구하였다. ECC를 제조하기 위하여 1종 보통 포틀랜드 시멘트(OPC)를 기본 결합재로 하고, 플라이애시를 다량 치환하여 결합재와 충전재로 사용하는 배합을 적용하였다. 철근 보강한 ECC 기둥의 반복이력거동을 평가하기 위하여 일반 철근콘크리트 기둥 실험체를 제작하여 실험을 수행하였다. 반복하중에 의한 실험의 결과, 일반 철근콘크리트 기둥에 비하여 철근 보강한 ECC 기둥은 높은 연성비와 함께 안정적인 이력거동을 나타내었고, 우수한 휨 균열 제어 특성을 나타내었다. 또한 횡방향 하중에 대한 기둥의 내력 증진효과와 함께 에너지 소산능력의 향상을 나타내었다.

• 한국광물학회지
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• 제17권4호
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• pp.327-338
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• 2004

Na-장석(Amelia albite)의 $1100^{\circ}C$ 등온가열에 대한 XRD 분석결과는 Si-Al의 재배열에 의한 급격한 구조변화를 보여주며 4일 이상의 가열에 의해 저온형에서 고온형으로의 상전이를 보였다. TEM의 제한시야전자회절(SAED)법을 이용하여 구조변화 인지를 시도한 결과, 변화의 양상은 보이나 측정 오차에 의해 Si-Al 배열상태의 정량화가 어려웠다. 수렴성빔전자회절(CBED)법을 이용한 연구결과, 관찰을 위한 최적 실험조건은 냉각 시료지지대의 사용과 120 kV의 가속전압, 37 $\mu\textrm{m}$크기의 C3 조리개, 25 nm의 빔 크기로 나타났다. 알바이트의 구조변화에 따라 HOLZ 선이 두드러진 변화를 보인 방향은 [418] 방향에서 약 $-1.2^{\circ}$ 회전한 방향으로 파악되었으며, 이 방향에서는 저온형과 고온형 알바이트에서 두 HOLZ선의 폭이 서로 반대로 나타나 Si-Al 배열상태의 뚜fut한 구별이 가능하였다.