• Title/Summary/Keyword: Specimen type

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Properties of Wollastonite-Reinforced Glass-Ceramics Made from Waste Automobile Glass and Waste Shell

  • Yun, Yeon-Hum;Yoon, Chung-Han;Kim, Chi-Kyun;Hwang, Kyu-Seog
    • Resources Recycling
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    • v.13 no.1
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    • pp.54-58
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    • 2004
  • Wollastonite-type glass ceramics were prepared by milling and firing at various temperatures using an automobile waste glass and waste shell as starting materials. Powder mixture ground by disk-type ball mill for 3 hours was pressed into a disk. The pressed specimen was fired at $850^{\circ}C$,$950^{\circ}C$ and $1050^{\circ}C$ for 1 hour in air. From FE-SEM observation, with an increase of the firing temperature from $850^{\circ}C$ to $1050^{\circ}C$, whisker-type phase was grown to about 10 $\mu\textrm{m}$ in length. Specimen fired at $1050^{\circ}C$ showed the formation of well-crystallized whisker-type wollastonite grains and the highest compressive strength.

Transmission Electron Microscopy Specimen Preparation of Delicate Materials Using Tripod Polisher

  • Cha, Hyun-Woo;Kang, Min-Chul;Shin, Keesam;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.46 no.2
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    • pp.110-115
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    • 2016
  • Transmission electron microscopy (TEM) is a powerful tool for analyzing a broad range of materials and provides localized information about the microstructure. However, the analysis results are strongly influenced by the quality of the thin foil specimen. Sample preparation for TEM analysis requires considerable skill, especially when the area of interest is small or the material of interest is difficult to thin because of its high hardness and its mechanical instability when thinned. This article selectively reviews recent advances in TEM sample preparation techniques using a tripod polisher. In particular, it introduces two typical types (fl at type and wedge type) of TEM sample preparation and the benefits and drawbacks of each method; finally, a method of making better samples for TEM analysis is suggested.

VISUALIZATION OF INTERNAL DEFECTS IN PLATE-TYPE NUCLEAR FUEL BY USING NONCONTACT OPTICAL INTERFEROMETRY

  • Park, Seung-Kyu;Park, Nak-Gyu;Baik, Sung-Hoon;Kang, Young-June
    • Nuclear Engineering and Technology
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    • v.45 no.3
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    • pp.361-366
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    • 2013
  • An imaging technique to visualize the internal defects in a plate-type nuclear fuel specimen was developed by using an active optical interferometer for a nondestructive quality inspection. A periodic thermal wave having a sinusoidal intensity pattern induced a periodical strain variation for the specimen. The varying strain image was acquired using an optical laser interferometer. The strain distribution over the internal defects will be distorted in an acquired strain image because a part of the thermal wave will be reflected from these defects during propagation. In this paper, internal defects were efficiently visualized by sequentially accumulating the extracted defect components. The experimental results confirmed that the developed visualization system can be a valuable tool to detect the internal defects in plate-type nuclear fuel.

Analysis of airborne sound insulation performance by the experiment using small size specimen (축소시편 실험을 통한 공기전달음 차단성능 분석)

  • Kim, Hang;Park, Hyeon Ku;Goo, Hee Mo;Kim, Sun-Woo
    • KIEAE Journal
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    • v.14 no.1
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    • pp.83-89
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    • 2014
  • The residents' demand for the comfortable life is promoting development of wall and window which has high sound insulation performance. To develop wall system, various aspects should be considered on the environment, material, construction and structure. Especially focusing on the acoustical view, the economical solution is one of the most critical point. Recently the interest on the partition wall is being increased, because it is useful for the Rahmen type apartment which is considered as an alternative to reduce floor impact sound. This study examines simplified measurement method of airborne sound insulation applied small size specimen, in order to save money to be used for the standard specimen then to promote the development process. The results showed that the simplified method could be effective for the wall system the sound insulation performance upto Rw 50 dB, and for the judgement of rank order of sound insulation performance of the similar wall type while developing.

Overload Analysis and Fatigue Life Prediction Using an Effective J-Integral of Spot Welded Specimens (점용접시편의 과부하해석 및 유효 J-적분에 의한 피로수명예측)

  • Lee, Hyeong-Il;Choe, Jin-Yong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.3 s.174
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    • pp.567-580
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    • 2000
  • This paper proposes an integrated approach, which is independent of specimen geometry and loading type, for predicting the fatigue life of spot welded specimens. We first establish finite element models reflecting the actual specimen behaviors observed on the experimental load-deflection curves of 4 types of single spot welded specimens. Using finite element models elaborately established, we then evaluate fracture parameter J-integral to describe the effects of specimen geometry and loading type on the fatigue life in a comprehensive manner. It is confirmed, however, that J-integral concept alone is insufficient to clearly explain the generalized relationship between load and fatigue life of spot welded specimens. On this ground, we introduce another effective parameter $J_e$ composed of $J_I$, $J_{II}$, $J_{III}$, which has been demonstrated here to more sharply define the relationship between load and fatigue life of 4 types of spot welded specimens. The crack surface displacement method is adopted for decomposition of J, and the mechanism of the mixed mode fracture is also discussed in detail as a motivation of using $J_e$.

Evaluation of the Residual Stress with Respect to Supporting Type of Multi-layer Thin Film for the Metallization of Pressure Sensor (압력센서의 배선을 위한 다층 박막의 지지조건 변화에 따른 잔류응력 평가)

  • Shim, Jae-Joon;Han, Geun-Jo;Han, Dong-Seup
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.5
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    • pp.532-538
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    • 2004
  • MEMS technology applying to the sensors and micro-electro devices is complete system. These microsystems are made by variable processes. Especially, the mentallization process has very important functions to transfer the power operating the sensor and signal induced from sensor part. But in the structures of MEMS the local stress concentration and deformation are often yielded by an irregular geometrical shape and different constraint. Therefore, this paper studies the effect of supporting type and thickness ratio about thin film of the substrate on the residual stress variation when the thermal loads is applied to the multi-layer thin film fabricated by metallization process. Specimens were made from several materials such as Al, Au and Cu. Then, uniform thermal load was applied, repeatedly. The residual stress was measured by FE Analysis and nano-indentation method using AFM. Generally, the specimen made of Al induced the larger residual stress than that of made of other materials. Specimen made of Cu and Au having the low thermal expansion coefficient induces the minimum residual stress. Similarly, the lowest indentation length was measured by nano-indentation method in the Si/Au/Cu specimen. Particularly, clusters are created in the specimen made of Cu by thermal load and the indentation length became increasingly large by cluster formation.

Precision Analysis of Workpieces made with Dental 3D Printing Technology (치과용 3D 프린팅 기술로 제작된 가공물의 정밀성 분석)

  • Choi, Sung-min
    • Journal of Technologic Dentistry
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    • v.40 no.4
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    • pp.231-237
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    • 2018
  • Purpose: The development of the dental technology industry has digitized the dental process. Definition of Digitalization of Dental Implantation Digitalization is the process of model making and prosthodontic processing using 3D CAD and CAM. Currently, it is becoming popular due to the spread of various devices. However, precision evaluation at this stage is an important factor in precision-based dental procedures. Therefore, in this study, we want to analyze the precision of the processed body made with digital dental machine. Methods: The accuracy of digital dental pore devices was evaluated. Specimens were fabricated with 5 types of 3D printers. The external shape was measured with the prepared specimen. The surface roughness was measured. Results: As a result, precision was excellent in order of EP2 specimen, EP1 specimen, and EA2 specimen. The precision of EP3 specimen and EA1 specimen is not excellent. And the precision of the specimen processed with polymer 3D printer is excellent. The accuracy of LCPS type polymer 3D printers is considered to be excellent. Conclusion : 1. Observation of the shape The 3D printer for LCPS system and the 3D printer for SLM $40{\mu}m$ system were found to be precisely processed. 2. Surface roughness results The LCPS system polymer 3D printer has been shown to have a precise surface.

Variation of Impact Characteristics of ISB Panels with a Pyramidal Inner Structure According to Joining Technologies (피라미드형 내부구조체를 가진 ISB 판넬의 접합형태에 따른 충격 특성 변화)

  • Ahn, Dong-Gyu;Moon, Gyung-Jae;Jung, Chang-Gyun;Yang, Dong-Yol
    • Journal of the Korean Society for Precision Engineering
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    • v.24 no.9
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    • pp.110-118
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    • 2007
  • ISB (Inner structured and bonded) panel with a pyramidal inner structure is actively developing to reduce the weight and to improve the crashworthiness of the material. The objective of this paper is to investigate into the variation of impact characteristics of ISB panels with a pyramidal inner structure according to joining types between skin sheets and inner structures. Several drop impact tests have been performed. In order to examine the impact characteristics at a drawing condition, drawing type of experimental set-up has been proposed. From the results of the experiments, the influence of joining types between skin sheets and the inner structures on the characteristics of the deformation, the energy absorption and the failure has been quantitatively examined. In addition, it has been shown that maximum load decreased and the maximum displacement increases as the joining type changes from the bonding to the welding. The results of the observation of the specimen have been shown that major wrinkles form in the minor crimping direction irrespective of the joining types. Through the comparison of the experimental results for bonding and welding specimens, it has been shown that the absorption energy of the bonded specimen is nearly 1.3-1.5 times of the welded specimen at the same displacement.

A New Measurement Method of Dielectric Constants Applied the Principles of Cross Capacitance (Cross Capacitance 원리를 작용한 새로운 유전상수 측정방법 제안)

  • Kim, Han-Jun;Lee, Rae-Duk;Kang, Jeon-Hong;Yu, Kwang-Min;Han, Sang-Ok
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07b
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    • pp.1084-1087
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    • 2002
  • The guard-ring type 3-terminal parallel plate electrodes proposed by ASTM D 150-81 and IEC 250 have been widely used for measurement of dielectric constants of solid dielectrics. However the method using this electrodes causes many uncertainty associated with the measurement errors of the diameter of the guarded electrode. the gap between guarded and guard-ring electrode. the distance of two active electrodes(the thickness of specimen), the roughness and contamination of surface of electrode and specimen. close adherence grade of electrode and specimen. In this paper. a new electrode system of cross capacitance type based on Thompson-Lampard theorem is designed and is employed for the measurement of dielectric constant. The results of simulation of guard-ring electrode and cross capacitance electrode using FEM program show that distance measurement between two electrodes in guard-ring electrode produces large uncertainty. on the other hand this effect in cross capacitance electrode is negligible. Furthermore. the air gap effects in the cross capacitance electrode is 5.6 times less sensitive than that in guard-ring electrode by assuming air gap of $50{\mu}m$.

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A Study on the Predicting Transverse Residual Stress at the ultra thick FCA butt weldment of hatch coaming in a Large Container Ship (대형 컨테이너선의 해치 코밍 FCA 맞대기 용접부의 횡 방향 잔류응력 예측에 관한 연구)

  • Shin, Sang-Beom;Lee, Dong-Ju;Park, Dong-Hwan
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.102-102
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    • 2009
  • The purpose of this study is to establish the predictive equation of transversal residual stress at the thick weldment of large container ship. In order to do it, the variables used for this study were restraint degree, yield strength of base material, thickness of weldment and welding heat input. Here, the level of restraint degree at the thick weldment of container ship having the various welding sequence was calculated using FEA. From the result, the h-type specimen was designed to simulate the level of restraint degree at the actual weldment of containership. With H-type test specimen designed, the effect of the variables on the distribution of transversal residual stress at the weldment in a container ship was evaluated using the comprehensive FEA. Based on the results, the predictive equations of mean value and the distribution of transverse residual stress in each location of residual stress were established using dimensional analysis and multiple-regression method. The validation of predictive equations was verified by comparing with measured results by XRD in the actual weldment of the ship.

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