• Title/Summary/Keyword: Specimen Preparation

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침적법에 의한 수산화아파타이트 코팅 금속재의 기초적 연구 (Hydroxyapatite Coating on Ti Plate by a Dipping Method)

  • 이준희;김석영;김영곤;이인섭
    • 대한의용생체공학회:의공학회지
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    • 제18권3호
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    • pp.217-222
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    • 1997
  • Hydroxyapatite(HA)-coated metal composites were made by the dipping method. The specimen substrates were Ti plates with a thickness of 2 mm. The HA coating was carried out in HA-sol for 1 min by the dipping method. The concentration of HA-sol for the coating ranged from 3.28 to 9.99 wt%. Excellent coating was observed on Ti substrate dipped once in 9.99 wt% sol. Preparation of Ti plates by sandblasting provided the better environment for coating HA on Ti surface than non-treated surface. As the concentration of sol increased, the weight change and the coating thickness increased. Above 7 wt% sol, they increased sharply.

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진공증착법으로 제조한 PVDF 박막의 열자격전류에 관한 연구 (A Study on the Thermally Stimulated Current of PVDF Thin Film Prepared by Physical Vapor Deposition Method)

  • 이선우;박수홍;김형권;임응춘;김수정;육재호;이덕출
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1998년도 추계학술대회 논문집 학회본부 C
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    • pp.755-757
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    • 1998
  • The thermally stimulated current (TSC) of PVDF thin film prepared by physical vapor deposition method was investigated. PVDF shows three TSC peaks designated $P_1$, $P_2$ and $P_3$ in ascending order of temperature. The $P_1$ peak is associated with water in the PVDF specimen. $P_2$ and $P_3$ Peaks are specific peaks of $\alpha$ and $\beta$ type PVDF, respectively. The peak temperature was shifted to higher temperature, and peak intensity was decreased with increasing substrate temperature under thin film preparation.

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전자차폐(電磁遮蔽)를 위한 크롬 및 알루미늄 스퍼터링의 효과 (Effects of Cr and Al Sputtered sheet for the Electromagnetic Shielding)

  • 김동진
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 추계학술대회논문집A
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    • pp.73-79
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    • 2001
  • In this paper, shielding effectiveness(SE) of the shielding material of electromagnetic(EM) waves was investigated with actual experiments. The materials used in this study were made up of sputtering, film and powder of conductive materials - Cr, Al, Ag and Cu etc. Also, the polyester film was used as a base material. The experiment was carried out by using a shielding evaluator(Shielding box) TR17302 with an ADVANTEST spectrum analyzer, model R3361C. It was found from the experimental results that silver, copper, aluminum and chromium were good candidates as a shielding material against the EM waves with increasing the SE as the composite was laminated. The characteristics of the SE against the EM waves depended on a mode of preparation of specimen. The effects of density of particles on the SE were studied when the sputtering. The SE strongly depended on the electric resistance by density of sputtering and painting particles. SE increased as the density of particles was increasing.

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공극수 추출방법에 따른 시멘트 페이스트의 수화도와 공극 특성 분석 (Evaluation of different methods to remove pore water in an early age cement paste for the degree of hydration measurement and pore structure analysis.)

  • 안유리;로양;김백중;이종구;강경인
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2012년도 춘계 학술논문 발표대회
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    • pp.245-246
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    • 2012
  • The analysis of microstructure is essential to understand the material behavior such as shrinkage, strength, and permeability. In this study, three different easy-to-apply specimen preparation methods for the mercury intrusion analysis were chosen, and their effectiveness in removing pore water and thus impeding further hydration was evaluated. As a result, it was found that the direct freeze-drying was the most effective among the three methods.

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A Brief Overview of Atom Probe Tomography Research

  • Gault, Baptiste
    • Applied Microscopy
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    • 제46권3호
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    • pp.117-126
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    • 2016
  • Atom probe tomography (APT) has been fast rising in prominence over the past decade as a key tool for nanoscale analytical characterization of a range of materials systems. APT provides three-dimensional mapping of the atom distribution in a small volume of solid material. The technique has evolved, with the incorporation of laser pulsing capabilities, and, combined with progress in specimen preparation, APT is now able to analyse a very range of materials, beyond metals and alloys that used to be its core applications. The present article aims to provide an overview of the technique, providing a brief historical perspective, discussing recent progress leading to the state-of-the-art, some perspectives on its evolution, with targeted examples of applications.

Surface Integrity and Tribological Properties of Machined Surfaces

  • Kim, Dae-Eun;Hwang, Dong-Hwan
    • Tribology and Lubricants
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    • 제11권5호
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    • pp.31-39
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    • 1995
  • The surface integrity of a machined surface is an important factor that dictates several performance characteristics of a metal part. In this paper, the surface integrity aspects are presented specifically with respect to the tribological properties of steel. Test specimens were prepared under varying conditions to induce different levels of surface deformation and hardness. Sliding and rolling experiments were performed to assess the friction and wear characteristics of these specimens using a pinon-disk type tribotester and a plate-on-ball type set-up. It is reaffirmed that heat treated steels possess superior sliding and rolling fatigue resistance than raw steel. However, for the case of raw steels machined under varying conditions, the harder specimen resulted in higher wear. This result is attributed to the presence of surface cracks that were induced during machining. The results of such findings will aid in the optimization of surface preparation process for tribological applications of steel.

Study on The Preparation and Mechanical Properties of Fiberglass Reinforced Wood-Based Composite

  • Zhang, Yang;Ma, Yan
    • Journal of the Korean Wood Science and Technology
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    • 제44권4호
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    • pp.505-514
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    • 2016
  • To study mechanical properties of fiberglass reinforced wood-based composite (FRWC), fiberglass with a diameter of $20{\mu}m$ was selected to prepare test specimens. Mechanical properties of fiberglass reinforced wood-based composite were determined by three-point-bending test while its microstructure was characterizes by scanning electron microscopy (SEM). The results showed that mechanical properties of fiberglass reinforced wood-based composite were superior to that of the wood fiberboard based on the contrasting mechanical curves and the analysis of fracture mechanism. It is believed that the material design with this "sandwich" structure brings a unique buffering capacity of fiberglass into play in the composites. So the specimen did not produce a sudden fracture failure at high level of applied loads because it had a bearing ability. The SEM analysis showed that the working strength of PVAc adhesive was high; under a bearing force, it could properly transfer a load. In addition, glass fiber mesh and wood fiber board combined well.

Preparation of TZM Alloys Having Elongated Coarse-grain Structure with High Aspect Ratio and their Mechanical Properties

  • Toyosima, Gouhei;Nagae, Masahiro;Yoshio, Tetsuo;Takada, Jun;Hiraoka, Yutaka;Takida, Tomohiro
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1163-1164
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    • 2006
  • TZM alloy having elongated coarse-grain structure was developed by three-step internal nitriding treatment at 1423 to 1873 K in $N_2$ and subsequent recrystallization treatment at 2173 K in vacuum. Some specimens were subjected to re-nitriding treatment at 1873 K for 16 h. After the recrystallization treatment, aspect ratio (L/W) of grains for rolling direction was about 50 at the maximum. Yield stress obtained at 1773 K after re-nitriding treatment was about 6 times as large as that of recrystallized specimen. Re-nitriding was very effective in the improvement in strength of TZM alloy having elongated coarse-grain structure.

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RTM 공정에 의해 생산된 GFRP 보강근의 콘크리트 부착특성에 관한 실험연구 (An Experimental Study on the Bond Characteristics of GFRP Rebar to Concrete Produced by RTM (Resin Transfer Molding) Process)

  • 박지선;유영찬;박영환;유영준;김형열;김긍환
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2005년도 봄학술 발표회 논문집(II)
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    • pp.297-300
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    • 2005
  • The bond characteristics of GFRP(glass fiber reinforced polymer) rods with various surface deformation produced by RTM(resin transfer molding) process were analyzes experimentally. Two types of GFRP rods with different surface deformation manufactured by RTM process in domestic area and two types of GFRP rebars imported were considered in this study. All testing procedures including specimens preparation, set-up of test equipments and measuring devices were made according to the CSA S806-02 recommendations. From the test results, it was found that deformed-type GFRP rod manufactured by RTM process showed the highest bond strength among test specimen. But, wave-type GFRP rod made by RTM process show the lowest value due to the splitting failure of concrete caused by the wedge action of waved surfaces on GFRP rods.

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저급점토를 이용한 다공성 세라믹스 제조 (Preparation for Porous Ceramics Using Low Grade Clay)

  • 한상목;신대용;강상규
    • 한국세라믹학회지
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    • 제35권6호
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    • pp.575-582
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    • 1998
  • Sutiability of Jungsan clay shale dolomite sludge Anyang feldspar and alumina as raw materials for light-weight porous ceramics was examined. In order to find optimum manufacturing conditions compositions heating temperatuers and heating times were varied and their effects on physical properties were measured and bloating mechanism was investigated. Jungsan clay seems suitable as raw material to make the light-weight constructional materials with 5wt% of ANyang feldspar and alumina added in calcined clay (800$^{\circ}C$) having bulk density of 0.45g/cm3 water absorption of 1.34% and compressive strength of 85kg/cm2 rapid-heated at 1200$^{\circ}C$ for 30min. It is suggested that bloating mechanism depends on the difference of tem-peratures between the inside and outside in specimen the remained gases in interstices can bloat by the li-quid phase of surface with high viscosity and gas pressure at elevated temperature.

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