• 제목/요약/키워드: Specimen Preparation

검색결과 237건 처리시간 0.03초

공시체 크기가 변형강도를 이용한 소성변형 추정에 미치는 영향 (Specimen Size Effect in Estimation of Rut Resistance based on Deformation Strength)

  • 이문섭;최선주;도영수;김광우
    • 한국도로학회논문집
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    • 제6권2호
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    • pp.1-13
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    • 2004
  • 본 논문은 정하중하에서 김테스트를 사용하여 아스팔트 콘크리트의 소성변형과 변형강도가 공시체에 크기에 미치는 영향에 대해 연구하였다. 2가지 골재(편마암, 화강암)와 6가지 아스팔트를 사용하여 총14개의 밀입도 혼합물을 사용하였다. 마샬 배합설계를 통해 최적아스팔트 함량을 구하고 결정된 최적아스팔트 함량으로 마샬공시체 (S=10cm)와 자이레토리 공시체(S=15cm)를 제작하여 마샬안정도시험, 휠트래킹시험, 개발된 김테스트(Kim test)를 수행하였다. SAS 분석을 통하여 공시체의 지름이 김테스트의 결과에 중요한 변수가 아닌 것을 알았으나 공시체의 두께는 $K_D$에 주용한 변수가 되는 것을 알았다. $K_D$값에 y값이 사용되어 영향을 미치는 것으로 판단되었다. 공시체의 두께를 6.6cm 이상으로 제작하여 김테스트에 적용 할때에는 마샬안정도에서와 같이 y 값에 따른 보정계수를 사용하거나 시험시 6.6cm 미만으로 제작하여야 할 것이다. 향후 보정계수 사용에 관한 연구도 가능할 것으로 판단된다.

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Improved Accuracy of Cytodiagnosis using the Kato Self-Collection Devise: the Usefulness of Smear Preparation in Liquid-based Cytology Methods

  • Okayama, Kaori;Okodo, Mitsuaki;Fujii, Masahiko;Kumagai, Tomoko;Yabusaki, Hiromi;Shiina, Yoshio;Iwami, Fumihiro;Teruya, Koji;Hatta, Kenmei
    • Asian Pacific Journal of Cancer Prevention
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    • 제13권9호
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    • pp.4521-4524
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    • 2012
  • Object: In the present study, we compared the positive cytodiagnostic test rates with discrepancies using self-collection devices for cervical cancer screening. We made this survey to examine whether or not our self-smear preparation method using the Kato self-collection device contributed to an improved rate of detecting atypical cells compared with existing recommended preparation methods. Methods: Specimens were collected at 14 facilities handling self-collection methods, and samples were collected by a physician in 2 facilities. The chisquared test was performed using the SPSS ver. 20 statistical software to determine the relationships between the positive cytodiagnostic rate, specimen preparation methods, and self-collection devices. Results: Collecting cells using the Kato self-collection device and preparing liquid-based specimens, we obtained a significantly higher rate of positive cytodiagnosis and our results were equal to those obtained with the direct method. Conclusions: Taking into consideration increased needs for screening using the self-collection method in future, with even more improved test accuracy, a screening test that is acceptable to society needs to be established.

초고전압투과 전자현미경의 효율적인 관리와 공유를 위한 메타데이터 모형 개발에 관한 연구 (A Study on the Development of High Voltage Electron Microscope Metadata Model for Efficient Management and Sharing)

  • 곽승진;김정택
    • 한국도서관정보학회지
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    • 제38권3호
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    • pp.117-138
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    • 2007
  • 초고전압투과 전자현미경(HVEM)을 이용한 e-Science 환경을 구축하기 위해서는 HVEM의 원격제어시스템과 HVEM에 의해 생성된 데이터의 효율적인 관리와 공유를 위한 데이터포털이 필요하다. 그리고 이러한 데이터포털에서 생성된 데이터의 구조화, 저장 및 관리, 탐색, 공유를 위해서는 HVEM에 적합하게 특화된 메타데이터가 필요하다. 본 연구에서는 e-Science 환경 하에서 HVEM에 의해 생성된 데이터의 보다 효율적인 관리와 공유를 위하여 HVEM에 적합하게 특화된 메타데이터 모형을 제시하였다.

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(Ba,Sr,Mg)$TiO_3$를 이용한 입계층 캐패시터의 제작 및 유전특성에 관한 연구 (The preparation and characteristics of (Ba,Sr,Mg) $TiO_3$ ceramic for BL capacitor)

  • 오재유;오의균;강도원;김범진;박태곤
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 추계학술대회 논문집
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    • pp.251-254
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    • 1998
  • The ($0.8BaTiO_3-0.1SrTiO_3-0.1MgTiO_3$)+$0.006Nb_2O_5$ ceramics were fabricated by conventional ceramic process. The dielectric property of specimen was investigated that the specimen was sintering temperature at 1,300C for 3hours and then annealed at $1,100^{\circ}C$ for 3hours in a atmosphere (air) to be painted on the surface with CuO paste. The results of the temperature and frequency are varied, the dielectric constant and loss tangent are unsuitable for BL capacitor. The dielectric constants were varied to be negative temperature coefficient(2.000-3,000) in the temperature range between -10 and $140^{\circ}C$, the dissipation factors (tan $\delta$) were some high(0.1-0.3). It was not grain insulation, in cause of the some difficult to be annealed temperature with CuO paste and fired atmosphere. But, we have some different annealing temperature and fired atmosphere, it will be suitable BL(Boundary Layer)capacitor.

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반복하중 크리프시험에 의한 아스팔트 혼합물의 소성변형특성 평가 (Rutting Potential Evaluation of Asphalt Mixtures by Repeated-Load Creep Test)

  • Zhu L.Y.;Fwa T.F.
    • 한국도로학회논문집
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    • 제8권3호
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    • pp.21-28
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    • 2006
  • Field or laboratory wheel tracking tests have been employed for the evaluation of the rutting potential of asphalt paving mixtures. Compared to field tests, laboratory wheel tracking tests are much less expensive and more manageable for most road projects. However, most test laboratories are not equipped to perform such tests because there does not exist any standard test procedure, and the required equipment is rather expensive. Futhermore, the size of test specimens and the relatively large quantity of test mixture required present difficulties for laboratory specimen mixing and compaction. This paper describes a project conducted to study the feasibility of replacing wheel tracking testsby a repeated-load creep test for rutting potential evaluation. Comparisons were made between the results of the two tests for different test temperatures, loading speeds and applied pressures. Three types of asphalt mixtures were studied in the test program. Favorable conclusions concerning the use of the repeated-load test for rutting potential evaluation were drawn based on the findings of the experimental test results. The correlation between the two types of tests was found to be good for all threeasphalt mixtures. Adopting the repeated-load creep test would lead to cost savings since it employs standard test equipment already available in most laboratories. It would also result in substantial time savings due to the much smaller quantity of mix needed, and the ease in specimen preparation.

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THREE DIMENSIONAL ATOM PROBE STUDY OF NI-BASE ALLOY/LOW ALLOY STEEL DISSIMILAR METAL WELD INTERFACES

  • Choi, Kyoung-Joon;Shin, Sang-Hun;Kim, Jong-Jin;Jung, Ju-Ang;Kim, Ji-Hyun
    • Nuclear Engineering and Technology
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    • 제44권6호
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    • pp.673-682
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    • 2012
  • Three dimensional atom probe tomography (3D APT) is applied to characterize the dissimilar metal joint which was welded between the Ni-based alloy, Alloy 690 and the low alloy steel, A533 Gr. B, with Alloy 152 filler metal. While there is some difficulty in preparing the specimen for the analysis, the 3D APT has a truly quantitative analytical capability to characterize nanometer scale particles in metallic materials, thus its application to the microstructural analysis in multi-component metallic materials provides critical information on the mechanism of nanoscale microstructural evolution. In this study, the procedure for 3D APT specimen preparation was established, and those for dissimilar metal weld interface were prepared near the fusion boundary by a focused ion beam. The result of the analysis in this study showed the precipitation of chromium carbides near the fusion boundary between A533 Gr. B and Alloy 152.

Equo-Tip 경도값에 미치는 실험변수의 영향 (The Effect of Test Variables on the Accuracy of Equo-Tip Hardness)

  • 남승훈;전승범;김종집
    • 열처리공학회지
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    • 제3권2호
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    • pp.32-36
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    • 1990
  • For the accurate measurements of hardness in a material, it is necessary to have a thorough understanding of the effects of test variables on the accuracy of hardness value. For the rebound hardness test, major test variables are the radius of hammer ball tip, type of backing materials, size and roughness of the specimen. In this study, effects of these variables on Equo-Tip hardness value were investigated. Hardness measurements were carried out using WC balls with various sizes of worn-ot zone. The sample materials chosen for the experiments were commercial standard hardness blocks and SM45C steel bars subjected to either normalization or quench and temper treatments. As backing materials, aluminum, steel and rubber plates were used in all the experiments. Experimental results show that for the accurate measurements of Equo-tip hardness, it is necessary to use the hammer ball with a worn-out zone parameter of less than 0.23, and the recommended minimum thickness and width of the specimen are 25mm and 70mm, respectively. Further for the surface preparation, the specimens need to be polished with an emery paper of No. 400 or finer, and for the backing matrials, it is recommended to use steels or rubbers.

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Expansion performance and mechanical properties of expansive grout under different curing pressures

  • Yiming Liu;Yicheng Ye;Nan Yao;Changzhao Chen
    • Geomechanics and Engineering
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    • 제33권4호
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    • pp.327-339
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    • 2023
  • The expansion capacity and strength of expansive grout have a significant influence on the stress state of a supported rock mass and the strength of a grout-rock mass structure. The expansion and strength characteristics are vital in grouting preparation and application. To analyze the expansion performance and mechanical properties of expansive grout, uniaxial compressive strength (UCS) tests, expansion ratio tests, XRD, SEM, and microscopic scanning tests (MSTs) of expansive grout under different curing pressure conditions were conducted. The microevolution was analyzed by combining the failure characteristics, XRD patterns, SEM images, and surface morphologies of the specimens. The experimental results show that: (1) The final expansion ratio of the expansive grout was linear with increasing expansion agent content and nonlinear with increasing curing pressure. (2) The strength of the expansive grout was positively correlated with curing pressure and negatively correlated with expansion agent content. (3) The expansion of expansive grout was related mainly to the development of calcium hydroxide (Ca(OH)2) crystals. With an increase in expansion agent content, the final expansion ratio increased, but the expansion rate decreased. With an increase in the curing pressure, the grout expansion effect decreased significantly. (4) The proportion of the concave surfaces at the centre of the specimen cross-section reflected the specimen's porosity to a certain extent, which was linear with increasing expansion agent content and curing pressure.

Ambient Variable Pressure Field Emission Scanning Electron Microscopy for Trichome Profiling of Plectranthus tomentosa by Secondary Electron Imaging

  • Kim, Ki Woo
    • Applied Microscopy
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    • 제43권1호
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    • pp.34-39
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    • 2013
  • Glandular and nonglandular trichomes on the leaf surface of Plectranthus tomentosa were investigated by variable pressure field emission scanning electron microscopy (VP-FESEM). The segments of the plant's leaves were directly mounted without any specimen preparation, and examined at ambient temperature using a variable pressure secondary electron (SE) detector under ca. 15 Pa. Foliar trichomes maintained their shapes and structures without severe surface collapse or charging. The adaxial leaf surface was abundantly covered with different types of trichome. Nonglandular trichomes consisted of a basal cell and a long (up to ca. $300{\mu}m$) stalk. Meanwhile, capitate glandular trichomes had a secretory head and a short or long stalk. Peltate glandular trichomes with globose secretory heads were observed in close contact with the leaf epidermis. Spherical projections on the secretory head showed the secretion process of glandular trichomes. In addition to the trichomes, oval stomata were distributed on the abaxial leaf surface. These results suggest that ambient VP-FESEM can be used to classify the dehydration-sensitive foliar trichomes of succulent plants by SE imaging. At the FESEM resolution, this approach facilitates the rapid and detailed morphological analysis of a variety of trichomes in diverse plant taxa with reduced labor and preparation.

TA-ESPI에 의한 외팔보의 탄성계수 측정 (Evaluation of Young's Modulus of a Cantilever Beam by TA-ESPI)

  • 이항서;김경석;강기수;정현철;양승필
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2005년도 춘계학술대회 논문집
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    • pp.1115-1119
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    • 2005
  • The paper proposes the elastic modulus evaluation technique of a cantilever beam by vibration analysis based on time-average electronic speckle pattern interferometry (TA-ESPI) with non-contact and nondestructive and Euler-Bernoulli equation. General approaches for the measurement of elastic modulus of thin film are Nano indentation test, Bulge test and Micro-tensile test and so on. They each have strength and weakness in the preparation of test specimen and the analysis of experimental result. ESPI has been developed as a common measurement method for vibration mode visualization and surface displacement. Whole-field vibration mode shape (surface displacement distribution) at a resonance frequency can be visualized by ESPI. And the maximum surface displacement distribution from ESPI is a clue to find the resonance frequency at each vibration mode shape. And the elastic modules of test material can be easily estimated from the measured resonance frequency and Euler-Bernoulli equation. The TA-ESPI vibration analysis technique is able to give the elastic modulus of materials through the simple processing of preparation and analysis.

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