• 제목/요약/키워드: Specimen Changes

검색결과 548건 처리시간 0.024초

Ultrastructural Changes in the Cuticle of Palaemon serrifer (Palaemonidae, Crustacea) during the Intermolt Cycle

  • Park Jeung Sook
    • Fisheries and Aquatic Sciences
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    • 제2권1호
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    • pp.78-84
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    • 1999
  • Ultrastructural changes in the cuticle of Paleamon serrifer associated with the intermolt cycle were examined and quantified as changes in the cuticular thickness. The cuticular thickness in each zoea stage increased with time elapsed after molting. The cuticle in the premolt stage was about 1.5 and 3 times thicker than that in the postmolt and intermolt stage, respectively. The cuticle in the premolt stage, including the molting space, was more than 5 times as thick as in the postmolt stage. In addition, newly hatched larvae were individually reared in the laboratory and body length for each specimen was measured frequently until the end of zoea VI. An average increase in body length between one zoea stage and the next is about $10\%$ of the length of the previous stage. Within individual zoea stages, the premolt stage had a body length some 0.3% longer than that of the postmolt stage, indicating a growth rate of about 0.03 mm/d.

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수화-소성법에 의한 $Ca_2$ 클린커의 합성: (III) 클린커소성 중의 미구조 변화 (Synthesis of $Ca_2$-based Clinker by Hydration-Burning Method: (III) Study on the Microstructural Changes during Clinker Burning)

  • 송태웅;한기성
    • 한국세라믹학회지
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    • 제28권10호
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    • pp.751-756
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    • 1991
  • Continuous microstructural changes on heating of hardened paste prepared from primary clinker of CA2 composition was studied. On heating period, several characteristic shrinkages and microstructural changes took place in the specimen due to the dehydration and recrystallization of calcium aluminates without regard to the accelerative shrinkage resulted from sintering. Though micropores formed by dehydration decreased with recrystallization of calcium aluminates, micropores formed by plate-type gibbsite in the hydrates were maintained up to the temperature at which CA2 becomes main phase and had influence to the microstructure of the final clinker.

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The Mechanical Behavior and the Anatomical Changes of Wood due to Variation of Deflection Rates

  • Kang, Chun Won
    • Journal of the Korean Wood Science and Technology
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    • 제33권5호통권133호
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    • pp.7-12
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    • 2005
  • The objective of this study is to estimate the mechanical behavior in bending and the anatomical changes of wood under several deflection rates. Sample specimens of water-saturated Japanese cedar (Cryptomeria japonica) were stressed to rupture under several deflection rates. Mechanical properties of wood such as modulus of elasticity, modulus of rupture and stress at proportional limit, and anatomical changes affected by deflection rates were estimated. Microscopic observations on compression side of the test specimens when the specimen was loaded to rupture were carried out by the SEM (scanning electron microscopy). The results are summarized as follows: 1. The mechanical properties of wood were affected by variations of the deflection rates. The modulus of elasticity (MOE), modulus of rupture (MOR) and stress at proportional limit were in proportion to the logarithm of deflection rates. 2. The deflection of wood at rupture in bending increased as deflection rates decreased. 3. The variations of the microscopic deformations of sample specimens were closely related to the deflection of wood at rupture. In case of largely deflected wood by maximum bending load, severe and abundant microscopic deformations were observed.

수열합성반응에 의한 경량콘크리트 블록 개발에 관한 기초적 연구 (The Fundamental Study on the Development of Light Weight Concrete Block by the Hydro-Thermal Synthetic Reaction)

  • 강철;강기웅;정지용;곽은구;권기주;김진만
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2005년도 봄학술 발표회 논문집(II)
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    • pp.461-464
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    • 2005
  • As the research on the development of the lightweight concrete block by the hydro-thermal synthetic reaction mixed with the calcareous material and bottom ash that is used less among siliceous material, we studied on the physical and chemical characteristics in the changes of hydro-thermal synthetic reaction of lightweight concrete block compounded with the PP fiber to increase flexural toughness and to prevent fragility failure. The results of the experiment are as follow. According to the increase of hydro-thermal synthetic reaction and the fiber content, compressive and flexural strength increased. Despite the changes of the hydro-thermal synthetic reaction time, tobermorite was produced on each of the specimens similarly. However, the phase of tobermorite was changed in accordance with the changes of time. Also, $CaCo_{3}$ appeared on the surface of the 9 hour hardened specimen.

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Construction and Application of Experimental Formula for Nonlinear Behavior of Ferroelectric Ceramics Switched by Electric Field at Room Temperature during Temperature Rise

  • Ji, Dae Won;Kim, Sang-Joo
    • 한국세라믹학회지
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    • 제55권1호
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    • pp.67-73
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    • 2018
  • A poled lead zirconate titanate (PZT) cube specimen that is switched by an electric field at room temperature is subject to temperature increase. Changes in polarization and thermal expansion coefficients are measured during temperature rise. The measured data are analyzed to obtain changes in pyroelectric coefficient and strain during temperature change. Empirical formulae are developed using linear or quadratic curve fitting to the data. The nonlinear behavior of the materials during temperature increase is predicted using the developed formulae. It is shown that the calculation results can be compared successfully with the measured values, which proves the accuracy and reliability of the developed formulae for the nonlinear behavior of the materials during temperature changes.

Effect of carbonated water manufactured by a soda carbonator on etched or sealed enamel

  • Ryu, Hyo-kyung;Kim, Yong-do;Heo, Sung-su;Kim, Sang-cheol
    • 대한치과교정학회지
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    • 제48권1호
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    • pp.48-56
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    • 2018
  • Objective: The purpose of this study was to determine the effects of carbonated water on etched or sealed enamel according to the carbonation level and the presence of calcium ions. Methods: Carbonated water with different carbonation levels was manufactured by a soda carbonator. Seventy-five premolar teeth were randomly divided into a control group and 4 experimental groups in accordance with the carbonation level and the presence of calcium ions in the test solutions. After specimen preparation of the Unexposed, Etched, and Sealed enamel subgroups, all the specimens were submerged in each test solution for 15 minutes three times a day during 7 days. Microhardness tests on the Unexposed and Etched enamel subgroups were performed with 10 specimens from each group. Scanning electron microscopy (SEM) tests on the Unexposed, Etched, and Sealed enamel subgroups were performed with 5 specimens from each group. Microhardness changes in different groups were statistically compared using paired t-tests, the Wilcoxon signed rank test, and the Kruskal-Wallis test. Results: The microhardness changes were significantly different between the groups (p = 0.000). The microhardness changes in all experimental groups except Group 3 (low-level carbonated water with calcium ions) were significantly greater than those in the Control group. SEM showed that etched areas of the specimen were affected by carbonated water and the magnitude of destruction varied between groups. Adhesive material was partially removed in groups exposed to carbonated water. Conclusions: Carbonated water has negative effects on etched or sealed enamel, resulting in decreased microhardness and removal of the adhesive material.

고상 압출된 폴리프로필렌/탈크 복합재료의 기계적 물성 (Mechanical Properties of Polypropylene/Talc Composites Prepared via Solid-State Extrusion)

  • 이재춘;하창식
    • 접착 및 계면
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    • 제17권4호
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    • pp.131-135
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    • 2016
  • 본 연구에서는 고상압출을 통하여 제조된 폴리프로필렌/탈크 복합재료의 배향 전후의 비중과 기계적 물성을 조사하였다. 탈크 충진제의 함량이 증가할수록 복합재료의 비중이 증가하였는데, 배향에 따라 발생된 미세공극으로 인해 배향된 복합재료의 비중은 배향되지 않은 복합 재료에 비해 작은 것으로 나타났다. 미배향 시료일 경우 탈크의 함량이 10중량%일 때 인장물성이 증가하였으나 탈크의 함량이 더 증가하면 인장물성은 감소하였다. 배향 시료 경우, 중량% 증가에 따라 인장 물성은 단조 감소를 보였다. Halpin-Tsai 식에 의해 이론적으로 분석한 결과 10중량% 첨가 때는 이론식에 잘 맞았으나 20중량% 이상일 때는 탈크 함량의 증가에 따라 이론식에서 벗어나는 정도가 더 커졌다. 굴곡강도 경우, 미배향 시료 와 배향 시료 모두 탈크의 함량이 10중량%일 때 최대 굴곡 강도 및 굴곡 탄성률을 보였다.

환경시료은행의 국제적 동향 및 우리의 대응 (International Trends of Environmental Specimen Bank and Our Response)

  • 김명진;유병호;이석조;이종천;이철우
    • 환경영향평가
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    • 제17권4호
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    • pp.225-233
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    • 2008
  • An Environmental Specimen Bank (ESB) is an archive for samples that can be used to document and assess the quality of the environment in which we live. An ESB program looks at changes in the concentration of human and environmental specimens over long periods of time through retrospective analysis of archived samples of a particular area collected at regular intervals. The idea of ESB was first proposed by German and American scientists in the early 1970s and has been established since 1979 in Germany, USA, and Japan. Korea plans to establish a National Environmental Specimen Bank (NESB) in 2010. The NESB will be able to assess and improve the quality of analytical measurements as well as to compare the past and current environmental quality as a time capsule. The concept and design for the NESB facility was developed and its Standard Operation Procedures (SOPs) are being developed based on an evaluation of ESBs and SOPs of Germany, USA, and Japan. Environmental specimens proposed for banking are based on typical representatives of every level of the food chain from each type of ecosystem that are widely distributed thus enabling comparisons between different sampling areas. Through retrospective analysis of environmental specimens, the NESB will improve the reliability of environmental monitoring, ecological risk assessment, and health impact assessment.

촉진열화실험에 의한 소나무의 물성 및 조직 변화에 대한 연구 (Study on the Change of Physical and Anatomical Properties in the Pine Wood by Accelerated Weathering Test)

  • 김광철
    • 한국가구학회지
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    • 제23권3호
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    • pp.324-331
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    • 2012
  • The domestic pine was used to investigate the change of specific gravity, moisture contents, color and anatomical structure by accelerated weathering test (AWT). According to visual inspection, a few knot separation and looseness as well as considerable surface discoloration was found out. However, the crack and split of surface texture have been never occurred till the last step of AWT. On the whole, as the time of accelerated weathering test has increased, the specific gravity has decreased. Finally, after the 9th week of AWT, the specific gravity was 0.38 that reached to 82% compared to the control specimen. In case of moisture content (MC), it showed rising trend in its early stages, however, after 3th week of AWT it have displayed steady state. A deterioration of cell-wall components was not remarkably observed by scanning electron microscope (SEM), however the ray fractures of AWT specimen were observed more than those of control specimen. The full fracture of epithelial cell around resin canal was observed by optical microscope. The fracture of ray of 2th cycle AWT specimen was first, followed by 1th week and control group. A distortion of tracheid for early spring wood and fracture of epithelial cell were generally observed by a similar level, regardless of duration time of AWT. Therefore, it is obvious that increasing duration time of AWT does not affect the deterioration of micro-structure for wood members from this study. Although a considerable change of anatomical properties was not found, there is a need of further research to understand how will the changes of specific gravity and MC on the physical properties of wood member.

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수퍼 2상 스테인리스강의 열처리 조건변화에 따른 첨가원소 질소의 거동 (Behavior of Nitrogen in the Variation of Heat Treatment Conditions of Super Duplex Stainless Steel)

  • 주동원;성장현
    • 열처리공학회지
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    • 제10권1호
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    • pp.30-39
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    • 1997
  • After changing the heat treating atmosphere of nitrogen gas, argon gas and vacuum, the nitrogen contents, microstructural changes, hardness and corrosion resistance of 0.25wt.%N alloyed super duplex stainless steel have been investigated in the temperature range from $1050^{\circ}C$ to $1350^{\circ}C$. The nitrogen content showed to be increased up to 0.36wt.% after heat treating the specimen in nitrogen gas at $1200^{\circ}C$, while the decrement of nitrogen content in vacuum atmosphere was shown down to 0.03wt.% at $1350^{\circ}C$. After heat treating in the mixed gas atmosphere of argon and nitrogen at $1250^{\circ}C$, the surface ${\gamma}$ phase existed as ${\alpha}+{\gamma}$ phase increased with increasing nitrogen gas content. The ${\gamma}$ single phase appeared at the surface above $80%N_2$ gas, while the surface ${\alpha}$ single phase was shown below $20%N_2$ gas. When heat treating the specimen in nitrogen gas at $1050^{\circ}C$, the hardness of austenite phases increased above Hv 40 at the surface layer compared to the hardness of the core parts, while decrement of denitriding effect caused to the hardness nearly unchanged between surface and the core parts after heat treating in vacuum atmosphere. The surface ${\gamma}$ single phase specimen showed superior corrosion resistance than the surface ${\alpha}$ single phase specimen. The surface ${\alpha}$ phase existed in the ${\alpha}+{\gamma}$ microstructure showed higher corrosion resistance after heat treating in the nitrogen gas atmosphere than the ${\alpha}$ phase heat treated in the argon gas and vacuum atmosphere.

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