• Title/Summary/Keyword: Solution-evaporation

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The Characteristics of Al Thin Films by Vacuum Evaporation for Bulb Reflector (전구 Reflector용 진공증착 Al박막의 특성)

  • 김동구;김경남;김석기;구경완;한상옥
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.688-691
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    • 1999
  • Light was of electric lamp was reflected by bulb reflector. In order to improve the efficiency of the electric lamp. it is inevitable that lamp, it is inevitable that improve the reflectance of bulb reflector. Important factors that affect the reflectance of bulb reflector is working pressure, distance between evaporation source to substrate, the situation of surface of glass. etch rate of glass, etc. In this paper. confirmed the effect of etching, working pressure etc. , and its effect for the reflectance of bulb reflector. Especially, concentration of HF in the etching solution and etching time is to be importnace for characteristic of bulb reflector.

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Thin film process of anodic aluminum oxidation for optoelectronic nano-devices (나노 광소자 응용을 위한 알루미늄 양극산화박막 공정)

  • Choi, Jae-Ho;Baek, Ha-Bong;Kim, Keun-Joo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.106-107
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    • 2007
  • We fabricated anodic aluminium oxides (AAO) on Si and sapphire substrates from the electrochemical reactions of thin AI films in an aqueous solution of oxalic acid. The thin AI films have deposited on Si and Sapphire substructure by using E-beam evaporation and thermal evaporation, respectively. The formation of AAO structures has investigated from FE-SEM measurement image and showed randomly distributed phase of nanoholes instead of the periodic lattice of photonic crystals. The AAO structure on sapphire shows the double layers of nanoholes.

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Development of SS-AG20-loaded Polymeric Microparticles by Oil-in-Water (o/w) Emulsion Solvent Evaporation and Spray Drying Methods for Sustained Drug Delivery

  • Choi, Eun-Jung;Bai, Cheng-Zhe;Hong, A-Reum;Park, Jong-Sang
    • Bulletin of the Korean Chemical Society
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    • v.33 no.10
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    • pp.3208-3212
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    • 2012
  • Controlled drug delivery systems employing microparticles offer lots of advantages over conventional drug dosage formulations. Microencapsulation technique have been conducted with biodegradable polymers such as poly(lactic-co-glycolic acid) (PLGA) and poly(lactic acid) (PLA) for its adjustable biodegradability and biocompatibility. In this study, we evaluated two techniques, oil-in-water (o/w) emulsion solvent evaporation and spray drying, for preparation of polymeric microparticles encapsulating a newly synthesized drug, SS-AG20, for the long-term drug delivery of this low-molecular-weight drug with a very short half-life. Drug-loaded microparticles prepared by the solvent evaporation method showed a smoother morphology; however, relatively poor encapsulation efficiency and drastic initial burst were discovered as drawbacks. Spray-dried drug-loaded microparticles had an imperfect surface with pores and distorted portions so that its initial burst was critical (70.05-87.16%) when the preparation was carried out with a 5% polymeric solution. By increasing the concentration of the polymer, the morphology was refined and undesirable initial burst was circumvented (burst was reduced to 35.93-74.85%) while retaining high encapsulation efficiency. Moreover, by encapsulating the drug with various biodegradable polymers using the spray drying method, gradual and sustained drug release, for up to 2 weeks, was achieved.

Structure Development of Solvent Casting Triacetyl Cellulose Film (트리아세틸 셀룰로오스 필름의 용액가공에 의한 구조변화)

  • Kim, Hyo-Gap;Kim, Hong-Suk;Kim, Han-Sung;Cho, Jin-Sik;Kim, Yong-Won;Kang, Ho-Jong
    • Polymer(Korea)
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    • v.34 no.3
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    • pp.210-214
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    • 2010
  • The structural development of triacetyl cellulose (TAC) was studied as a function of solution casting processing parameters such as dope concentration, evaporation temperature, annealing temperature and the addition of plasticizer. The crystalline structure was developed by the solution casting and the level of crystallinity was increased with increasing dope concentration and evaporation temperature. The crystalline structure could be enhanced by the annealing process after formation of TAC film. Introducing plasticizer resulted in decreasing melting temperature and crytallinity of TAC film due to the increase of chain mobility. It was also found that thermal stability of TAC was improved due to the rigid structure of applied plasticizer.

Performance analysis for the Characteristics of Double Stage Evaporator/Absorber for Large temperature Difference Absorption System (흡수식 대온도차 시스템에서 2단 증발/흡수기의 성능 특성에 관한 수치적 연구)

  • Park, Chan-Woo;Kang, Yong-Tae;Im, Ick-Tae;Moon, Sang-Done
    • Proceedings of the SAREK Conference
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    • 2008.06a
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    • pp.304-308
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    • 2008
  • The optimal design of two stage evaporation & absorption system which is related to the large temperature difference system was investigated numerically in the absorption refrigeration system. The concentrations at inlet & oulet of absorber are 62.9% and 56.9%, but in two stage absorption system the values are 62.2% and 56.2%. Therefore strong solution & weak solution became diluted than the standard value. The amount of weak solution circulation can be reduced in absorption refrigeration system, and the sensible heat load is more reduced to enhance the COP of system. As UAR is increased, COP becomes larger, and this means the role of top section is more important than bottom section in two stage evaporation & absorption system. But the increase of COP becomes slower at 0.7 of UAR ratio. The performance of Type2 is higher than Type1 in COP with the flow direction of cooling waters. This phenomena is due to the active absorption of vapor -absorption & lower temp. cooling water is more effective. The pressure at bottom section becomes higher & that at top section becomes lower and therefore the circulation rate can be diminished more.

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Optimum design of the Characteristics of Double Stage Evaporator/Absorber for Large temperature Difference Absorption System (냉수 대온도차 흡수식 냉동기용 2단 증발기/ 흡수기 최적 설계)

  • Park, Chan-Woo;Im, Ick-Tae;Kang, Yong-Tae
    • Proceedings of the SAREK Conference
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    • 2008.11a
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    • pp.203-211
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    • 2008
  • The optimal design of two stage evaporation & absorption system which is related to the large temperature difference system was investigated numerically in the absorption refrigeration system. The concentrations at inlet & oulet of absorber are 62.9% and 56.9%, but in two stage absorption system the values are 62.2% and 56.2%. Therefore strong solution & weak solution became diluted than the standard value. The amount of weak solution circulation can be reduced in absorption refrigeration system, and the sensible heat load is more reduced to enhance the COP of system. As UAR is increased, COP becomes larger, and this means the role of top section is more important than bottom section in two stage evaporation & absorption system. But the increase of COP becomes slower at 0.7 of UAR ratio. The performance of Type2 is higher than Type1 in COP with the flow direction of cooling waters. This phenomena is due to the active absorption of vapor -absorption & lower temp. cooling water is more effective. The pressure at bottom section becomes higher & that at top section becomes lower and therefore the circulation rate can be diminished more.

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Recycling of Organic Materials Using Purification by Recrystallization for Solution-Processed OLEDs (재결정화법에 의한 유기물 재활용 및 이를 이용한 습식 OLED 제작)

  • Lee, Jin-Hwan;Hong, Ki-Young;Shin, Dong-Kyun;Lee, Jin-Young;Park, Jong-Woon;Seo, Hwa-Il;Seo, Yu Seok
    • Journal of the Semiconductor & Display Technology
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    • v.15 no.1
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    • pp.65-69
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    • 2016
  • We have investigated the possibility of recycling of an organic material that is wasted during thermal evaporation. To this end, we have collected a wasted organic material (N,N'-diphenly-N,N'-bis(1,1'-biphenyl)-4,4'-diamine(NPB)) from a vacuum chamber, purified it by recrystallization, and fabricated bilayer organic light-emitting diodes (OLEDs) with the recycled NPB. It is found that the surface roughness of thin films coated with the purified NPB is much enhanced. OLEDs fabricated by thermal evaporation of the purified NPB show lower device efficiency than OLEDs with the original NPB. However, the power efficiency of OLED fabricated by spin coating of the purified NPB is comparable with that of OLED with the original NPB. Therefore, such a recycling method by recrystallization would be more suitable for solution-processed OLEDs.

Recovery of High Purity KI Crystal from Aqueous Waste of Polarizing Film Manufacturing Process (LCD용(用) 편광(偏光)필름제조폐용액(製造廢溶液)으로부터 고순도(高純度) KI결정(結晶) 회수(回收)에 관한 연구(硏究))

  • Kim, Dae-Weon;Jang, Seong-Tae;Choi, Soon-Ryung
    • Resources Recycling
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    • v.21 no.2
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    • pp.53-58
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    • 2012
  • A laboratory study was carried out to recover KI crystals with high purity from a waste solution generated from the production of polarizing film for LCD industry. The waste solution contains 1 to 4% KI, and other impurities such as B, PVA and etc. More than 95% purity of KI crystals were produced through refining process such as vacuum evaporation and fractional crystallization. Most of B compounds and impurities were removed by concentrating the waste solution until KI content reached about 50%. The KI crystals were washed with solvents to remove most of PVA which gave result in producing 99.5% purity of crystals. The overall recovery of KI was about 90% during the concentration process.

Second-Order Perturbation Solutions of Liquid Pool Spreading with Instantaneous Spill (순간 누출된 액체의 확산에 관한 2차 섭동 해)

  • Kim, Myung-Bae;Do, Kyu-Hyung;Han, Yong-Shik;Choi, Byung-Il
    • Journal of Hydrogen and New Energy
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    • v.21 no.6
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    • pp.513-518
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    • 2010
  • In the present work the second-order perturbation solutions of the simple physical model for liquid pool spreading is obtained for the case of instantaneous spill. To generalize the solution governing equations are non-dimensionalized, and two dimensionless parameters, dimensionless evaporation rate and aspect ratio of the initial pool, are identified to control the governing equations. The dimensional governing equations have three parameters. The second-order solution improves fairly the first-order solution for the pool volume.

Evaporation of Water in an Aqueous Lithium Bromide Solution flowing over a Horizontal Tube

  • Kim, Dong-Kwan;Kim, Moo-Hwan
    • International Journal of Air-Conditioning and Refrigeration
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    • v.9 no.3
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    • pp.57-62
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    • 2001
  • Falling film heat transfer analyses with aqueous lithium bromide solution were performed to investigate the transfer characteristics of the copper tubes. Finned (knurled) tube and a smooth tube were selected as test specimens. Averaged generation fluxes of water and the heat flux were obtained. As the film flow rate of the solution increased, the generation fluxes of water decreased for both tubes due to the fact that the heat transfer resistance increased with the film thickness. The effect of the enlarged surface area at the knurled tube was supposed to be dominant at a small flow rate. The generation fluxes of water increased with the increasing degree of tube wall superheat. Nucleate boiling is supposed to occur at a wall superheat of 20K for a smooth tube, and at 10K for a knurled tube. The increased performance of the knurled tube was supposed to mainly come from the effect of the increased heating surface area.

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