• Title/Summary/Keyword: Solution reduction method

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A Study about Reduction Method of the X-Ray Film Image (X선 사진의 감력법에 대한 실험 고찰)

  • Lee, Sang-Suk
    • Journal of radiological science and technology
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    • v.14 no.2
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    • pp.55-55
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    • 1991
  • I reduced overexposed X-Ray film image with farmer reduction method and $KMnO_4$ reduction method. The results are as follows : 1. In farmer reduction method, there appears linear decreasing film image density. 2. In $KMnO_4$ reduction method, there appears over proportional reduction. 3. When red prussiate is compared with $KMnO_4$ reduction method, the latter shows more intense reduction. 4. If the reduction solution isn't used within 10 minutes after dilution, it becomes oxidized and the ability is decreased remarkably.

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Incremental Linear Discriminant Analysis for Streaming Data Using the Minimum Squared Error Solution (스트리밍 데이터에 대한 최소제곱오차해를 통한 점층적 선형 판별 분석 기법)

  • Lee, Gyeong-Hoon;Park, Cheong Hee
    • Journal of KIISE
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    • v.45 no.1
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    • pp.69-75
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    • 2018
  • In the streaming data where data samples arrive sequentially in time, it is difficult to apply the dimension reduction method based on batch learning. Therefore an incremental dimension reduction method for the application to streaming data has been studied. In this paper, we propose an incremental linear discriminant analysis method using the least squared error solution. Instead of computing scatter matrices directly, the proposed method incrementally updates the projective direction for dimension reduction by using the information of a new incoming sample. The experimental results demonstrate that the proposed method is more efficient compared with previously proposed incremental dimension reduction methods.

Preparation of Mono-Disperse Ni Powder for Multilayer Ceramic Capacitor by Solution-Reduction Method (용액환원법에 의한 MLCC용 단분산 니켈 미분말의 합성)

  • Kim, Kang-Min;Lee, Jong-Heun;Yoon, Seon-Mi;Lee, Yong-Kyun;Lee, Hyun-Chul;Choi, Jae-Young
    • Journal of the Korean Ceramic Society
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    • v.42 no.10 s.281
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    • pp.649-653
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    • 2005
  • A mono-disperse Ni powders for multilayer ceramic capacitors were prepared in a large scale by solution reduction method using $NiSO_{4}$ $N_{2}$$H_{4}$and NaOH. The exothermic reactions such as Ni-complex formation between highly concentrated $NiSO_{4}$ and $N_{2}$$H_{4}$ and the reduction of $Ni^{2+}$ into Ni provided thermal energy sufficient for spontaneous solution-reduction reaction. Because well-defined Ni particles could be prepared without external heating, the present method was named as 'auto-thermal method'. The formation of Ni­complex, the precipitation of $Ni(OH)_{2}$ gel triggered by NaOH addition, and its reduction into Ni by dissolution-recrystallization route were the reaction mechanism. The preparation of mono-disperse and spherical Ni powder was attributed to uniform distribution of reducing agent $N_{2}$$H_{2}$ within $Ni(OH)_{2}$ gel due to the decomposition of$NiSO_{4}$-$N_{2}$ $H_{4}$ complex.

Reduction of Hexavalent Chromium Collected on PVC Filters in Field Electroplating Process (현장 도금 공정에서 PVC 여과지에 채취된 6가 크롬의 환원)

  • Shin Yong Chul;Paik Nam Won;Yi Gwang Yong;Lee Byung Kyu;Lee Ji Tae
    • Journal of Environmental Health Sciences
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    • v.28 no.1
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    • pp.41-49
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    • 2002
  • Recently, pilot studies showed an evidence of reduction of airborne hexavalent chromium, Cr(VI), on PVC filter during air sampling and storage. However, the information on this in the field was limited. Thus, we studied the reduction behaviors of airborne Cr(VI) on PVC filters during sampling and storage at three field electroplating operations. Regression between sampling time and the reduction (ratio of Cr(VI) to total Cr concentrations) was not statistically significant (p>0.05). However, the reductions in samples collected for 240 ~ 340 minutes were significantly higher than those for 30 - 60 minutes. On the other hand, another experiment showed a good correlation (r=0.96) between sampling time and the reduction without an exceptional value. Storage temperature was not a factor affecting the reduction of Cr(VI) collected on PVC filter. The loss of Cr(VI) samples stored in alkali solution (2% NaOH/3% Na$_2$CO$_3$) was significantly lower than that stored in vial according to NIOSH method (p<0.05). Thus, dipping Cr(VI) samples into alkali solution was a storage method to minimize tile reduction.

NUMERICAL SOLUTION OF EQUILIBRIUM EQUATIONS

  • Jang, Ho-Jong
    • Communications of the Korean Mathematical Society
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    • v.15 no.1
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    • pp.133-142
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    • 2000
  • We consider some numerical solution methods for equilibrium equations Af + E$^{T}$ λ = r, Ef = s. Algebraic problems of this form evolve from many applications such as structural optimization, fluid flow, and circuits. An important approach, called the force method, to the solution to such problems involves dimension reduction nullspace computation for E. The purpose of this paper is to investigate the substructuring method for the solution step of the force method in the context of the incompressible fluid flow. We also suggests some iterative methods based upon substructuring scheme..

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Visible-light photo-reduction of reduced graphene oxide by lanthanoid ion

  • Kim, Jinok;Yoo, Gwangwe;Park, Jin-Hong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.290.1-290.1
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    • 2016
  • Grapehen, a single atomic layer of graphite, has been in the spotlight and researched in vaious fields, because its fine mechanical, electrical properties, flexibility and transparence. Synthesis methods for large-area graphene such as chemical vaper deposition (CVD) and mechanical, chemical exfoliation have been reported. In particular, chemical exfoliation method receive attention due to low cost process. Chemical exfoliation method require reduction of graphene oxide in the process of exfoliation such as chemical reduction by strong reductant, thermal reduction on high temperature, and optical reduction via ultraviolet light exposure. Among these reduction methods, optical reduction is free from damage by strong reductant and high temperature. However, optical reduction is economically infeasible because the high cost of short-wavelength ultraviolet light sorce. In this paper, we make graphene-oxide and lanthanoid ion mixture aqueous solution which has highly optical absorbency in selective wevelength region. Sequentially, we synthesize reduced graphene oxide (RGO) using the solution and visible laser beam. Concretely, graphene oxide is made by modified hummer's method and mix with 1 ml each ultraviolet ray absorbent Gd3+ ion, Green laser absorbent Tb3+ ion, Red laser absorbent Eu3+ ion. After that, we revivify graphene oxide by laser exposure of 300 ~ 800 nm layser 1mW/cm2 +. We demonstrate reproducibility and repeatability of RGO through FT-IR, UV-VIS, Low temperature PL, SEM, XPS and electrical measurement.

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Preparation of Ag Powder from AgNO3 by Wet Chemical Reduction Method1. The Establishment of Optimum Reaction System for the Preparation of Spherical Ag Powder (습식 화학적 환원법에 의한 AgNO3로부터 Ag 분말의 제조 1. 균일한 구형 Ag 분말의 제조를 위한 최적 반응계 확립)

  • Yuna, Ki-Seok;Park, Young-Chul;Yang, Beom-Seok;MIn, Hyun-Hong;Won, Chang-Whan
    • Journal of Powder Materials
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    • v.12 no.1
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    • pp.56-63
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    • 2005
  • Ag powder was prepared from $AgNO_3$ by wet chemical reduction method using various reduction agent system involving $AgNO_3$, $AgNO_2$(AgCl) and Ag complex ion aqueous solution. The pure Ag powder could be prepared regardless of reaction system but the particle shape and distribution were affected very much according to the kind of reduction agents and reaction systems. The optimum reaction system for the preparation of the silver powder having the uniform particle shape and size distribution was Ag complex ion aqueous solution-reduction agent system and in particular, $H_2O_2$ and $C_6H_8O_6$as a reduction agent leaded the more uniform particle shape and size distribution.

Data Reduction and Analysis Technique for the Resonant Column Testing by Its Theoretical Modeling (공진주 실험의 이론적 모델링에 의한 자료분석 및 해석기법의 제안)

  • 조성호;황선근;강태호;권병성
    • Proceedings of the Korean Geotechical Society Conference
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    • 2003.03a
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    • pp.291-298
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    • 2003
  • The resonant column testing is a laboratory testing method to determine the shear modulus and the material damping factor of soils. The method has been widely used for many applications and its importance has been increased. Since the establishment of the testing method in 1963, the low-technology electronic devices for testing and data acquisition have limited the measurement to the amplitude of the linear spectrum. The limitations of the testing method were also attributed to the assumption of the linear-elastic material in the theory of the resonant column testing and to the use of the wave equation for the dynamic response of the specimen. For the better theoretical formulation of the resonant column testing, this study derived the equation of motion and provided its solution. This study also proposed the improved data reduction and analysis method for the resonant column testing, based on the advanced data acquisition system and the proposed theoretical solution for the resonant column testing system. For the verification of the proposed data reduction and analysis method, the numerical simulation of the resonant column testing was performed by the finite element analysis. Also, a series of resonant column testing were peformed for Joomunjin sand, which verified the feasibility, of the proposed method and showed the limitations of the conventional data reduction and analysis method.

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Fast GPU Implementation for the Solution of Tridiagonal Matrix Systems (삼중대각행렬 시스템 풀이의 빠른 GPU 구현)

  • Kim, Yong-Hee;Lee, Sung-Kee
    • Journal of KIISE:Computer Systems and Theory
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    • v.32 no.11_12
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    • pp.692-704
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    • 2005
  • With the improvement of computer hardware, GPUs(Graphics Processor Units) have tremendous memory bandwidth and computation power. This leads GPUs to use in general purpose computation. Especially, GPU implementation of compute-intensive physics based simulations is actively studied. In the solution of differential equations which are base of physics simulations, tridiagonal matrix systems occur repeatedly by finite-difference approximation. From the point of view of physics based simulations, fast solution of tridiagonal matrix system is important research field. We propose a fast GPU implementation for the solution of tridiagonal matrix systems. In this paper, we implement the cyclic reduction(also known as odd-even reduction) algorithm which is a popular choice for vector processors. We obtained a considerable performance improvement for solving tridiagonal matrix systems over Thomas method and conjugate gradient method. Thomas method is well known as a method for solving tridiagonal matrix systems on CPU and conjugate gradient method has shown good results on GPU. We experimented our proposed method by applying it to heat conduction, advection-diffusion, and shallow water simulations. The results of these simulations have shown a remarkable performance of over 35 frame-per-second on the 1024x1024 grid.

Shape Design of Frame Structures for Vibration Suppression and Weight Reduction

  • Hase, Miyahito;Ikeda, Masao
    • 제어로봇시스템학회:학술대회논문집
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    • 2003.10a
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    • pp.2246-2251
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    • 2003
  • This paper proposes shape design of frame structures for vibration suppression and weight reduction. The $H_{\infty}$ norm of the transfer function from disturbance sources to the output points where vibration should be suppressed, is adopted as the performance index to represent the magnitude of vibration transfer. The design parameters are the node positions of the frame structure, on which constraints are imposed so that the structure achieves given tasks. For computation of Pareto optimal solutions to the two-objective design problem, a number of linear combinations of the $H_{\infty}$ norm and the total weight of the structure are considered and minimized. For minimization of the scalared objective function, a Lagrange function is defined by the objective function and the imposed constraints on the design parameters. The solution for which the Lagrange function satisfies the Karush-Kuhn-Tucker condition, is searched by the sequential quadratic programming (SQP) method. Numerical examples are presented to demonstrate the effectiveness of the proposed design method.

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