• Title/Summary/Keyword: Solidification Process

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Consolidation of Thermal Electric Material Powder by MPC Process and Thermal Electric Properties (MPC 공정에 의한 열전반도체 분말의 성형 및 열전특성)

  • Yun, J.S.;Koo, J.M.;Kim, T.S.;Hong, S.J.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.454-456
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    • 2009
  • N-Type $SbI_3$ doped $95%Bi_2Te_3+5%\;Bi_2Se_3$ compounds were newly fabricated by the combination of gas atomization process and Magnetic Pulsed Compaction process. The thermoelectric properties of the MPCed bulks according to consolidation temperatures were investigated by a combination of microscopy, XRD and thermoelectric property testing. The microstructure of MPCed bulk shows homogeneous and fine distribution through consolidated bulks due to the high solidification of compound powders. The research presented the challenges toward the successful consolidation of thermoelectric powder using magnetic pulsed compaction (MPC) and analysis of thermoelectric properties of the consolidated bulks.

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Transient Liquid Phase Bonding of Gamma Prime Precipitation Strengthened Ni Based Superalloy (석출강화형 Ni 기 초내열합금의 천이액상확산접합)

  • Kim, Jeong Kil;Park, Hae Ji;Shim, Deog Nam
    • Journal of Welding and Joining
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    • v.35 no.3
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    • pp.52-61
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    • 2017
  • Transient liquid phase (TLP) bonding is essential technology to repair micro-cracking on the airfoil of blades and vanes for gas turbines. Understanding of the characteristics of TLP bonding of the superalloys is necessary in the application of the technology for repairing these components. In this study, the focus was on investigating TLP bonding characteristics of ${\gamma}^{\prime}$ precipitation strengthened Ni based superalloy. TLP bonding was carried out with an amorphous filler metal in various bonding conditions, and the microstructural characterization was investigated through optical microscopy (OM) and electron probe micro-analysis (EPMA). The experimantal results explained clearly that bonding temperatures had critical effects on the TLP bonding behaviors, and that isothermal solidication of the joints made at higher temperatures than $1170^{\circ}C$ was controlled by Ti diffusion instead of B.

Nanocomposite SiEA-KNiFe sorbent - Complete solution from synthesis through radiocesium sorption to vitrification using the sol-gel method

  • Chmielewska, Dagmara;Siwek, Malgorzata;Wawszczak, Danuta;Henczka, Marek;Sartowska, Bozena;Starosta, Wojciech;Dudek, Jakub
    • Journal of Industrial and Engineering Chemistry
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    • v.67
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    • pp.407-416
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    • 2018
  • This study presents a novel complete solution starting with a synthesis of silica modified with potassium-nickel hexacyanoferrate and ethanolamine (SiEA-KNiFe) sorbent through radiocesium sorption in different process configurations and moving on to the vitrification of the spent sorbent, using the sol-gel method. The experimental data for deionized water solution, as well as seawater solution, correlates strongly with the Langmuir isotherm model. Moreover, the study also presents a method for spent sorbent solidification in the glass matrix. The cesium leaching test confirmed that spent sorbent can be stably bound in the glass matrix after radionuclide removal.

Structural defects in the multicrystalline silicon ingot grown with the seed at the bottom of crucible (종자결정을 활용한 다결정 규소 잉곳 내의 구조적 결함 규명)

  • Lee, A-Young;Kim, Young-Kwan
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.24 no.5
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    • pp.190-195
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    • 2014
  • Because of the temperature gradient occurring during the growth of the ingot with directional solidification method, defects are generated and the residual stress is produced in the ingot. Changing the growth and cooling rate during the crystal growth process will be helpful for us to understand the defects and residual stress generation. The defects and residual stress can affect the properties of wafer. Generally, it was found that the size of grains and twin boundaries are smaller at the top area than at the bottom of the ingot regardless of growth and cooling condition. In addition to that, in the top area of silicon ingot, higher density of dislocation is observed to be present than in the bottom area of the silicon ingot. This observation implies that higher stress is imposed to the top area due to the faster cooling of silicon ingot after solidification process. In the ingot with slower growth rate, dislocation density was reduced and the TTV (Total Thickness Variation), saw mark, warp, and bow of wafer became lower. Therefore, optimum growth condition will help us to obtain high quality silicon ingot with low defect density and low residual stress.

A Numerical Analysis on the Freeze Coating of a Non-Isothermal Flat Plate with a Binary Alloy (비등온 평판의 이성분 합금 냉각코팅에 관한 수치해석)

  • Nam, Jin-Hyeon;Kim, Chan-Jung
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.11
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    • pp.1437-1446
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    • 2000
  • A numerical analysis on the freeze coating process of a non-isothermal finite dimensional plate with a binary alloy is performed to investigate the growth and decay behavior of the solid and the mushy layer of the freeze coat and a complete procedure to calculate the process is obtained in this study. The continuously varying solid and mushy layers are immobilized by a coordinate transform and the resulting governing differential equations are solved by a finite difference technique. To account for the latent heat release and property change during solidification, proper phase change models are adopted. And the convection in the liquid melt is modeled as an appropriate heat transfer boundary condition at the liquid/mushy interface. The present results are compared with analytic solutions derived for the freeze coating of infinite dimensional plates and the discrepancy is found to be less than 0.5 percent in relative magnitude for all simulation cases. In addition the conservation of thermal energy is checked. The results show that the freeze coat grows proportional to the 1.2 square of axial position as predicted by analytic solutions ar first. But after the short period of initial growth, the growth rate of the freeze coat gradually decreases and finally the freeze coat starts to decay. The effects of various non-dimensional processing parameters on the behavior of freeze coat are also investigated.

Applicability of Air Cooling Heat-treatment for a Duplex Stainless Steel Casting (2상 스테인레스 주강의 공냉 열처리 적용 가능성)

  • Kim, Bong-Whan;Yang, Sik;Shin, Je-Sik;Lee, Sang-Mok;Moon, Byung-Moon
    • Journal of Korea Foundry Society
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    • v.26 no.1
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    • pp.17-26
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    • 2006
  • The substitution of cooling method from water quenching to air cooling after solution heat treatment was aimed for the development of a convenient and economical heat treatment process of duplex stainless steels without deterioration of mechanical and corrosion resistant properties for the industry. In order to achieve this goal, the mechanical properties and corrosion properties of a ASTM A890-4A duplex stainless steel were systematically investigated as functions of casting condition and cooling method after solution heat treatment. A 3-stepped sand mold and a permanent Y-block mold were used to check the effects of solidification structure and cooling rate after solution heat treatment. The microstructural characteristics such as the ferrite/austenite phase ratio and the precipitation behavior of ${\sigma}$ phase and carbides were investigated by combined analysis of OM and SEM-EDX with an aid of TTT diagram. Hardness and tension test were performed to evaluate the mechanical properties. Impact property at $-40^{\circ}C$ and corrosion resistance were also examined to check the possibility of the industrial application of this basic study. Throughout this investigation, air-cooling method was proved to effectively substitute for water-quenching process after the solution heat treatment, when the duplex stainless steel was sand mold cast with a thickness below 15 mm or permanent mold cast with a thickness below 20 mm.

A Study on the Relation of Tingling Disease and Accumulation in 『Huangdineijing』 (『황제내경(黃帝內經)』의 비(痺)와 적(積)의 관계에 대한 고찰(考察))

  • Baik, Yousang;Suh, Junho
    • Journal of Korean Medical classics
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    • v.32 no.4
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    • pp.109-118
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    • 2019
  • Objectives : In this study, the relationship between Tingling disease(痺證) and Accumulation (積) was examined focusing on the occurrence of Tingling disease and its development into tangible lesion. Methods : Based on related contents in the "Huangdineijing", the process of creation and development of Tingling and its transformation to Accumulation was mainly examined. Results : While Tingling disease is usually caused by the three Qis of Wind-Cold-Dampness, due to its Yin nature there is high tendency of Qi and blood to be blocked and Blood and Fluid-Humor agglomerating into Accumulation. Symptoms of dysaesthesia are merely expressions manifesting in this process. Development into colic accumulation [疝瘕], Gu(蠱), or convulsion[瘛] after Tingling has traveled to the five zang is also related to its transformation into Accumulation. In the case of Tingling disease of the five zang in the "Huangdineijing", it is not a diagnostic category for treatment but actual lesions in the five zang six fu. In other words, in the beginning stages of Tingling disease, some sort of solidification that causes abnormal senses among other symptoms happens, and this solidification starts taking up space within the flesh. If it is not eliminated and persists, it enters into the inner organs and develops Tingling disease of the zangfu. Conclusions : Understanding Tingling disease(痺證) as a presymptom to developing Accumulation, rather than abnormality of sense will enable people to have higher chances in treating tumor.

A Study on the Production of Landfill-Cover Material Using the Physical Characteristics of Sludge and the Reduction of Odor (슬러지의 물리적 특성을 이용한 매립복토재 생산과 악취저감에 대한 연구)

  • Park, Jung Hyun;Yeo, Woon Ho
    • Journal of the Korea Organic Resources Recycling Association
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    • v.28 no.2
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    • pp.15-29
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    • 2020
  • The aims of this study is to improve physical properties of the sewage sludge and the process sludge generated in the leachate treatment by mixing the dry fuel, to develop the neutral solidifing agents that reduce oder, and to recycle the sewage and the process sludges as landfill cover materials. The mixing ratio (W/W) of sludges and dry fuel was appropriate at about 1:1, and the mixed materials were shown to be homogeneous at that ratio. We could know that when the sludges were mixed with dry fuel, moisture contents and viscosities are reduced, and air passages are formed between particles and particles. The various mixing tests and odor tests showed that the neutral solidifing agent was effective for the odor reduction. The main ingredient of the solidifing agent is the ash of sewage sludge, enabling it competitive in waste recycling and production costs. The landfill cover, using developed neutral solidification agent, improved physical properties to satisfy the quality standards and to increase the compressive strength. It also proved to reduce the value of complex oder and the usage of solidification agent to 1/3 (3,000 to 1,000) and to 1/8 (50% to 6%), respectively, from the comparative study with alkaline solidified landfill cover. Further research is under way to prove that this can be mixed with general soil to be used as a soil improvement agent for plant cultivation.

Dynamics Simulation of Solid Particles in Compression Deformation of Rheology Material (레오로지 소재의 압축변형시 고상입자 거동의 동역학 해석)

  • Lee, C.S.;Kang, C.G.
    • Transactions of Materials Processing
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    • v.15 no.5 s.86
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    • pp.395-401
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    • 2006
  • It is reported that semi-solid forming process takes many advantages over the conventional forming process, such as a long die life, good mechanical properties and energy saves. It is important to predict the deformation behavior for optimization of the forging process with semi-solid materials and to control liquid segregation for mechanical properties of materials. But rheology material has thixotropic, pseudo-plastic and shear-thinning characteristics. So, it is difficult for a numerical simulation of the rheology process to be performed because complicated processes such as the filling to include the state of the free surface and solidification in the phase transformation must be considered. General plastic or fluid dynamic analysis is not suitable for the analysis of the rheology material behavior. Recently, molecular dynamics is used for the behavior analysis of the rheology material and turned out to be suitable among several methods. In this study, molecular dynamics simulation was performed for the control of liquid segregation, forming velocity, and viscosity in compression experiment as a part of study on the analysis of rheology forming process.

Risering of Steel Castings in Vacuum Molding Process (진공흡입주형 주조법에서 주강의 압탕 방안 설계)

  • Kang, Bok-Hyun;Kim, Ki-Young;Kim, Myung-Han;Hong, Young-Myung
    • Journal of Korea Foundry Society
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    • v.27 no.2
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    • pp.88-94
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    • 2007
  • General criteria for the risering design of steel castings and commercial codes for the flow and solidification analysis were used to design the optimized risering in V-process. Three type of specimens were chosen including thin plates and a thick disc. Sided riser installed in the front of a plate casting was effective to prevent the shrinkage defects and to increase the casting yield ratio. Exothennic sleeve and chill were also effective. It was possible to apply the general criteria for the risering design of steel castings to V-process. Temperature of a mold surface was expected to rise over $1,000^{\circ}C$ in the temperature calculation considering radiation effect of molten metal in the mold. Since weakening temperature of the vinyl used in V-process is about $70^{\circ}C$, it should be emphasized that a proper coating of the vinyl film is necessary to prevent the possibility of burning out of the vinyl by the molten metal.