• Journal of the Korean Society for Heat Treatment
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• v.11 no.1
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• pp.10-16
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• 1998

The softening behavior of squeeze cast Mg-Li-Al and Mg-Li-Al-Zr alloys have been investigated. The highest hardness values of Mg-Li-Al and Mg-Li-Al-Zr alloys were obtained after solution treatment at $400^{\circ}C$ for 1 hour. The hardness value, however, decreased as the aging temperature and time increased. Microstructural and calorometric analyses showed that quenched-microstructure changed from primary (${\alpha}$ and ${\beta}$)+secondary ${\alpha}$ to primary(${\alpha}$ and ${\beta}$)+secondary ${\alpha}+{\theta}$ after aging. The softening during aging was due to the coarsening of ${\theta}$ precipitates.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2002.05a
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• pp.163-168
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• 2002

Hot forging is widely used in the manufacturing of industry machine component. The mechanical, thermal load and thermal softening which are happened by the high temperature in hot forging process. Tool life decreases considerably due to the softening of the surface layer of a tool caused by a high thermal load and long contact time between the tool and billet. Also, tool life is to a large extent limited by wear, heat crack and plastic deformation in hot forging process. These are one of the main factors affecting die accuracy and tool life. That is because hot forging process has many factors influencing tool life, and there was not accurate in-process data. In this research, life prediction of hot forging tool by wear and plastic deformation analysis considering tempering parameter has been carried out for automobile component. The new developed technique in this study for predicting tool life can give more feasible means to improve the tool life in hot forging process.

• Transactions of Materials Processing
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• v.12 no.4
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• pp.308-313
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• 2003

High temperature deformation and softening behavior of SAF 2507 super duplex stainless steel (SDSS) has been investigated in connection with an FEM analysis of hot forging process. Flow curves at various strain rates and temperatures were determined first from compression tests, and the kinetics of dynamic recrystallization were also formulated through the analysis of load relaxation test results. Using the dynamic materials theory proposed by Prasad, the deformation behavior was effectively determined for various conditions. Constitutive relations and recrystallization kinetics formulated from the test results were then implemented in a commercial FEM code. The forming load as well as the distribution of recrystallized volume fraction after forging was successfully predicted by means of the flow stress compensation formulated upon the volume fraction of recrystallization and adiabatic heating.

• Journal of Welding and Joining
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• v.16 no.6
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• pp.44-51
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• 1998

It is well known that the fine bainitic microstructure obtained by TMCP(thermo-mechanical control process) secures the high toughness of base metal. Besides, TMCP steel is very suitable for high heat input in welding as it has low carbon equivalent. In HAZ, however, the accelerated cooling effect imparted on the matrix by the weld thermal cycles is relieved and thus the weldment of TMCP steel has softening zone which shows low fracture toughness compared with base metal. Therefore, PHWT of weldment is carried out to improve the fracture toughness in weldment of TMCP steel which has softening zone. In this study, the effects of PWHT on the weldment of AH36-TMCP steel are investigated by the small punch (SP) test. From the several results such as SP energy and displacement at room temperature, the behavior of transition curves, the fracture strength at -196$^{\circ}C$, distribution of (DBTT)sp and (DBTT)sp, the PWHT condition of A.C. after 85$0^{\circ}C$-1 sec W.C. was suitable condition for recovering a softening zone of HAZ as welded.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.6 no.4
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• pp.558-563
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• 1996

Fracture strength of $Si_{3}N_{4}/20$ vol% SiC nanocomposites with fifferent sintering additives was measured. Strength of nanocomposites with 6 wt% $Y_{2}O_{3}$ and 2 wt% $Al_{2}O_{3}$ as sintering additives was higher at room temperature but significant strength degradation at elevated temperature was occured due to the softening of grain boundary phase. Fracture strength of 8 wt% $Y_{2}O_{3}$ doped sample was higher than that of $Al_{2}O_{3}$ added sample at $1400^{\circ}C$. The retention of high temperature strength in 8 wt% $Y_{2}O_{3}$ doped sample can be attributed to high softening temperature and crystallization of grain boundary glassy phase.

• Korean Journal of Food Science and Technology
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• v.20 no.1
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• pp.95-99
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• 1988

The changes of texture, composition of cell wall polysaccharides, polygalacturonase (PG) activity and soaking effect during preserving of persimmon at various tempoeratures were estimated for the purpose of investigating the softening characteristics of persimmon fruit. The softening of persimmon was most promoted at $25^{\circ}C$, where in the higher temperature, at $45^{\circ}C$ it was inhibited. During softening adhesiveness increased, cohesiveness and gumminess decreased. This phenomenon was obvious at $25^{\circ}C$. By soaking in water at $50^{\circ}C,\;70^{\circ}C$ for 30 minutes PG activity and softening was inhibited. Ionically associated pectin (IAP) and covalently bounded pectin (CBP) fractionated from crude cell wall of fresh persimmon were respectively degraded about 60% by PG curde enzyme of softened persimmon. And the degraded ratio of polysaccharides composed of pentose and hexose was very similar to that of polyuronide.

• Journal of the Korean Ceramic Society
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• v.25 no.5
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• pp.431-436
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• 1988

The properties of scid-resistance to boiling HCl, thermal expansion coefficient and softening temperature of mother glass and glass-ceramic of LAS systems were investigated at the contents of SiO2 varing from 57 to 67wt%. The nucleation and growth of crystalline phase of LAS compositions were carried out at 50$0^{\circ}C$ and $700^{\circ}C$. The crystalline phase jconsists of lithium alumino silicate, lithum meta silicate, lithium disilicate, $\alpha$-crystobalite and $\alpha$-quartz. Lithium alumino silicate(virgilite) is the major crystalline phase in the glass ceramics. The degree of acid resistant property was increased in proportion with the silica content for both glass and ceramics. Glass-ceramic gives lower acid-resistance and thermal expansion coefficient while softening temperature shows higher for glass-ceramic than for mother glass.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.05a
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• pp.23-26
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• 2003

This paper explains the die cooling method for improving tool life in the hot forging process. In continuous forming operation such as hot forging process, performed at high speeds, temperature increases of several hundred degrees may be involved. Die hardness was reduced due to thermal softening. Factor of die fracture are wear and plastic deformation of die due to hardness reduction by high temperature. Because die service life was reduced due to this phenomenon during hot forging, quantified data for optimal die cooling method is required. The new developed techniques for predicting tool life applied to estimate the production quantity for a spindle component and these techniques can be applied to improve the tool life in hot forging process

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03b
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• pp.135-139
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• 1999

The static softening behavior of AISI 4140 could be characterized by the hot torsion test in the temperature ranges of 10$0^{\circ}C$~120$0^{\circ}C$ and strain rate ranges of 0.05/sec~5/sec. Deformation efficiency which was based on dynamic materials model was calculated from flow stress curves obtained continuous deformation. Interrupted deformation was performed with 2 pass deformation in the pass strain ranges of 0.25{{{{ epsilon _p}}}} ~3{{{{ epsilon _p}}}} and interrupted time ranges of 0.5~100sec. The dependences of process variables pass strain ({{{{ epsilon _i}}}}) stain rate ({{{{ {. } atop {$\varepsilon$ } }}}}) temperature (T) and interpass time ({{{{ {t }_{i } }}}}) on static recrystallization (SRX) and metadynamic recrystallization .(MDRX) could be indicidually predicted from the modified Avrami's equations. Comparison of the softening kinetics between MDRX and SRX showed that the rate of MDRX was more rapid than that of SRX for the same deformation variables. Controlled multipass deformations were performed using deformation efficiency static and metadynamic recrystallization of AISI 4140.

• The Korean Journal of Food And Nutrition
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• v.13 no.2
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• pp.103-110
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• 2000

This study was conducted to determine changes in phenolic compounds of astrigent persimmons before and after softening process and evaluate discoloring properties of major phenolic compounds. Phenolic compounds in soft persimmons were mainly composed of catechins and chlorogenic acid. Although contents of phenolic compounds were reduced during the softening process, little change in the ratio of catechins to total phenolic compounds was observed. Most of phenolic compounds in damaged astringents persimmons were existed in the high molecular weight fraction and more phenolic compounds were extracted at the temperature higher than room temperature. To evaluate discoloring abilities of phenolic compounds, phenolic compounds were dissolved separately into water or 80% methanol. With presence of various amounts of anti-discoloring agents such as vitamin C, citric acid, and L-cystein, (+)catechin was significantly reduced.