• 제목/요약/키워드: Softening temperature

검색결과 405건 처리시간 0.025초

염절임 및 가열에 의한 배추조직의 구조와 펙틴의 변화 (Changes in Tissue Structure and Pectins of Chinese Cabbage during Salting and Heating)

  • 유명식;김주봉;변유량
    • 한국식품과학회지
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    • 제23권4호
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    • pp.420-427
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    • 1991
  • 배추의 염절임 및 가열처리 중의 조직구조 변화를 현미경적으로 관찰하고 펙틴질을 분별 정량하였으며 조직의 내부구조를 cytorrhysis로 측정하였다. 배추줄기 조직의 유세포의 세포막은 염절임시 수축 파괴되며 세포간 공간의 포집공기와 세포액은 세포수축과 함께 중엽을 파괴하면서 유출되었다. 배추조직의 펙틴은 주로고 메톡실 펙틴인 pA와 저 메톡실 펙틴인 pB로 구성 되었고 염절임 및 $60{\sim}70^{\circ}C$의 저온 가열시 상당량의 pA는 작용으로 pB로 전환되었고 $80^{\circ}C$ 이상으로 가열처리하면 열분해로 pB가 감소되었으며 열처리 중 조직의 firmness는 pB의 함량과 상관관계가 높았다(r=0.996). Cytorrhysis 실험결과 염절임 및 $60^{\circ}C$의 저온처리에서는 조직의 pore size가 더 작아졌고 $80^{\circ}C$ 이상의 고온 열처리에 의하여 조직의 pore size가 커졌는데 이는 저온에서 pB의 증가에 의해 조직이 더 치밀해지고 고온 열처리에서는 가열분해된 pB가 용출되면서 조직이 더 엉성해졌기 때문인 것으로 판단되었다.

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파일 니트의 복합 후가공 기술에 의한 고품위 침장제품 개발에 관한 연구 - 원사 종류에 따른 원단의 물리적 특성 고찰을 중심으로 - (Development of Hi-Quality Bedding Items by Multi-Finishing System of Pile Knitted Fabrics - Physical Properties of Textile according to Yarn Types -)

  • 손은종;황영구;박신웅;최윤선;정성훈
    • 한국염색가공학회지
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    • 제29권4호
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    • pp.231-238
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    • 2017
  • There are many kinds of elements and processes for the development of high quality bedding products like fiber, high-temperature heat treatment, dyeing process, tenter drying with softening agent and multiple final finishing. Especially we examined the mechanical characteristic properties of fabrics according to different yarn types. The critical physical properties of the yarn consisting the pile knitted fabrics were obtained for the development of the hi-grade bedding items. The material property and the exhaustion behaviour of the developed pile knitted fabrics composing of different yarns were measured and observed. The physical properties of the developed fabric were evaluated through the material property analysis of the yarn, the physical nature of the pile knitted fabrics and the data of the exhaustion performance; tensile strength, tensile elongation, tearing strength, cross section of yarn types, dyeing properties etc. And then high-class of bedding items were knitted using the double raschel machine to make the pile knitted fabrics.

초고강도 합금강의 이종마찰교반 접합부에서의 미세조직 특성 및 기계적 물성 연구 (Microstructural and Mechanical Analysis of a Friction Stir Welded Joint of Dissimilar Advanced High-Strength Steels)

  • 이지우;조훈휘;;;홍성태
    • 소성∙가공
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    • 제29권1호
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    • pp.11-19
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    • 2020
  • For microstructural analysis of a friction stir welded (FSWed) joint of advanced high-strength steels, dual phase (DP) and complex phase (CP) steels, are studied. FSWed joints are successfully fabricated in the following four cases: (i) DP/DP; (ii) CP/CP; (iii) DP/CP, where the advancing side is DP and the retreating side is CP; (iv) CP/DP, where the advancing side is CP and the retreating side is DP. The stir zone (SZ) of (i) the DP/DP joint mainly consists of lath martensite, while the stir zone of (ii) the CP/CP joint consists not only of lath martensite but also of bainite. In the case of (iii) DP/CP and (iv) CP/DP, they exhibit a similar microstructure including acicular-shaped phases in the joints; however, cross-sections of the joints show differences in material mixing in each case. In (iv) the CP/DP joint, temperature towards the CP steel is sufficient to cause softening, thus leading to better mixing than that in (iii) DP/CP. The phases of the SZ in each of the four cases are formed by phase transformation during the FSWed process; however, the transformed phase volume fraction of CP steel is lower than that of DP steel, indicating that dynamic recrystallization occurs mainly in CP steel. The hardness values of the SZ are significantly higher than those of the base materials, especially, the SZ of (iii) the DP/CP joint has the highest value due to highest fraction of lath martensite.

$CaO-P_2O_5-SiO_2$계 유리의 물성 (Properties of $CaO-P_2O_5-SiO_2$ Glasses)

  • 조정식;김철영
    • 한국세라믹학회지
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    • 제30권4호
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    • pp.289-298
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    • 1993
  • Properties in terms of the variation of the glass compositions, which were density (p), molar volume(Vm), atom/ion packing density (Dp), refractive index (nD), transformation temperature (Tg), dilatometric softening point (Td), thermal expansion coefficient (α), Young's modulus (E), and knoop hardness (KHN) were investigated in CaO-SiO2 glasses and CaO-P2O5-SiO2 glasses containing less than 10mole% of P2O5. Those properties were measured by density measurement kit, Abbe refractometer, dilatometer, ultrasonic pulse echo equipment, and micro hardness tester. When CaO content was increased in CaO-SiO2 glasses, p, Dp, nD, Tg, Td, α, E and KHN were increased, while Vm was decreased. When P2O5 was added to the CaO-SiO2 glasses with constant CaO/SiO2 ratio as 1.07, p, Dp, nD, Tg, Td, α, E and KHN were decreased, while Vm was increased. When the amount of P2O5 in glasses was kept constant, the changes of the properties with variation of CaO content in the CaO-P2O5-SiO2 glasses were very similar to those of CaO-SiO2 glasses. These phenomena could be explained by the structural role of P2O5 in the CaO-P2O5-SiO2 glasses, which was polymerization of siicate structures and resulted in [PO4] monomer structure in glasses. Due to this structural characteristics, the bond strength and packing density were changed with compositions. Proportional relationships between 1) np and Dp, 2) Tg, Td, α and CaO content, 3) E and Vm-1, and 4) KHN and P2O5 content were evaluated in this investigation.

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Effect of Distribution System Materials and Water Quality on Heterotrophic Plate Counts and Biofilm Proliferation

  • 장영철;정권
    • Journal of Microbiology and Biotechnology
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    • 제14권6호
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    • pp.1114-1119
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    • 2004
  • The biofilms on pipe walls in water distribution systems are of interest since they can lead to chlorine demand, coliform growth, pipe corrosion, and water taste and odor problems. As such, the study described in this paper is part of an AWWARF and Tampa Bay Water tailored collaboration project to determine the effect of blending different source waters on the water quality in various distribution systems. The project was based on 18 independent pilot distribution systems (PDS), each being fed by a different water blend (7 finished waters blended in different proportions). The source waters compared were groundwater, surface water, and brackish water, which were treated in a variety of pilot distribution systems, including reverse osmosis (RO) (desalination), both membrane and chemical softening, and ozonation-biological activated carbon (BAC), resulting in a total of 7 different finished waters. The observations from this study consistently demonstrated that unlined ductile iron was more heavily colonized by a biomass than galvanized steel, lined ductile iron, and PVC (in that order) and that the fixed biomass accumulation was more influenced by the nature of the supporting material than by the water quality (including the secondary residual levels). However, although the bulk liquid water cultivable bacterial counts (i.e. heterotrophic plate counts or HPCs) did not increase with a greater biofilm accumulation, the results also suggested that high HPCs corresponded to a low disinfectant residual more than a high biofilm inventory. Furthermore, temperature was found to affect the biofilms, plus the AOC was important when the residual was between 0.6 and 2.0 mg $Cl_2/l$. An additional aspect of the current study was that the potential of the exoproteolytic activity (PEPA) technique was used along with a traditional so-called destructive technique in which the biofilm was scrapped off the coupon surface, resuspended, and cultivated on an R2A agar. Both techniques indicated similar trends and relative comparisons among the PDSs, yet the culturable biofilm values for the traditional method were several orders of magnitude lower than the PEPA values.

페라이트계 스테인리스강 재현 용접 열 영향부의 석출거동 및 열피로 특성에 미치는 구속응력의 영향 (Effect of Restraint Stress on the Precipitation Behavior and Thermal Fatigue Properties of Simulated Weld Heat Affected Zone in Ferritic Stainless Steel)

  • 한규태;강용준;이상철;홍승갑;정홍철;이창희
    • Journal of Welding and Joining
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    • 제33권6호
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    • pp.6-12
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    • 2015
  • Thermal fatigue life of the automobile exhaust manifold is directly affected by the restraint force according to the structure of exhaust system and bead shape of the welded joints. In the present study, the microstructural changes and precipitation behavior during thermal fatigue cycle of the 18wt% Cr ferritic stainless steel weld heat affected zone (HAZ) considering restraint stress were investigated. The simulation of weld HAZ and thermal fatigue test were carried out using a metal thermal cycle simulator under complete constraint force in the static jig. The change of the restraint stress on the weld HAZ was simulated by changing the shape of notch in the specimen considering the stress concentration factor. Thermal fatigue properties of the weld HAZ were deteriorated during cyclic heating and cooling in the temperature range of $200^{\circ}C$ to $900^{\circ}C$ due to the decrease of Nb content in solid solution and coarsening of MX type precipitates, laves phase, $M_6C$ with coarsening of grain and softening of the matrix. As the restraint stress on the specimen increased, the thermal fatigue life was decreased by dynamic precipitation and rapid coarsening of the precipitates.

질화규소 세라믹의 레이저 예열선삭에 관한 연구 (III) - SSN 및 HIPSN의 예열선삭시 절삭력 및 공구수명의 특성 - (A Study on Laser Assisted Machining for Silicon Nitride Ceramics (III) - Variation of the Main Cutting Force and Life of Cutting Tool by LAM of SSN and HIPSN -)

  • 김종도;이수진;강태영;서정;이제훈
    • Journal of Welding and Joining
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    • 제28권6호
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    • pp.35-39
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    • 2010
  • Generally, ceramic material is very difficult to machine due to high strength and hardness. However, ceramic material can be machined at high temperature by plastic flow as metallic material due to the deterioration of the grain boundary glassy phase. Recently, a new method was developed to execute cutting process with CBN cutting tool by local heating of surface with laser. There are various parameters in LAM because it is a complex process with laser treatment and machining. During laser assisted machining, high power results in reducing of cutting force and increasing tool life, but excessive power brings oxidation of the surface. The effect of laser power, feed rate, cutting depth and etc. were investigated on the life of cutting tool. Chips were observed to find out suitable machining conditions. Chips of SSN had more flow-types than HIPSN. It means SSN is easier to machining. The life of cutting tool was increased with increasing laser power and decreasing feed rate and cutting depth.

12% Cr 로터강의 강도 개선에 관한 연구 (Study on the Improvement of Strength for 12% Chromium Steel Rotor)

  • 장윤석;오세욱
    • 한국해양공학회지
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    • 제3권2호
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    • pp.125-137
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    • 1989
  • To check technical improvement in the soundness and strength of 12% Cr steel rotor, a 25 tons of rotor with 65 tons of ingot was made in real size and was cut to pieces to take test samples, and the various mechanical tests such as impact, tensile, creep, and fatigue were carried out. The strengths are compared with those of 1% Cr-Mo-V rotor of same size. Microstructures of the samples are examined and reviewed. The results can be summarized as follows. 1) Fracture appearance transition temperatures are 80.deg. C at the center part and 60.deg. C near surface of 12% Cr rotor, and 8.deg. C near surface of 1% Cr-Mo-V rotor. 2) Comparative rapid softening occurs at higher temperatures above 600.deg. C for 12% Cr steel and 550.deg. C for 1% Cr-Mo-V steel in tension tests. 3) Fatigue crack propagation rate of 12% Cr steel is almost same as that of 1% Cr-Mo-V steel at the same corresponding surface part of the rotors. The crack growth rate of center part of 12% Cr rotor is faster than near surface part of the rotor, and the crack growth rate at the load condition of R=0.04 is slower than that of the load condition of R=0.5 for both 12% Cr steel and 1% Cr-Mo-V steel. 4) Crack growth rate of radial direction near surface of 12% Cr rotor is faster than that of transverse direction at the same part because of the difference in residual stresses. 5) Both creep and fatigue strengths of 12% Cr steel are superior to those of 1% Cr-Mo-V steel and the difference is thought the effect of climb and glide controlled creep by solid solution of alloying elements and dispersion of carbides.

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12% Cr 로터강의 강도 개선에 관한 연구 (Study on the Improvement of Strength for 12% Chromium Steel Rotor)

  • 장윤석;오세욱
    • 한국해양공학회지
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    • 제3권2호
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    • pp.625-625
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    • 1989
  • To check technical improvement in the soundness and strength of 12% Cr steel rotor, a 25 tons of rotor with 65 tons of ingot was made in real size and was cut to pieces to take test samples, and the various mechanical tests such as impact, tensile, creep, and fatigue were carried out. The strengths are compared with those of 1% Cr-Mo-V rotor of same size. Microstructures of the samples are examined and reviewed. The results can be summarized as follows. 1) Fracture appearance transition temperatures are 80.deg. C at the center part and 60.deg. C near surface of 12% Cr rotor, and 8.deg. C near surface of 1% Cr-Mo-V rotor. 2) Comparative rapid softening occurs at higher temperatures above 600.deg. C for 12% Cr steel and 550.deg. C for 1% Cr-Mo-V steel in tension tests. 3) Fatigue crack propagation rate of 12% Cr steel is almost same as that of 1% Cr-Mo-V steel at the same corresponding surface part of the rotors. The crack growth rate of center part of 12% Cr rotor is faster than near surface part of the rotor, and the crack growth rate at the load condition of R=0.04 is slower than that of the load condition of R=0.5 for both 12% Cr steel and 1% Cr-Mo-V steel. 4) Crack growth rate of radial direction near surface of 12% Cr rotor is faster than that of transverse direction at the same part because of the difference in residual stresses. 5) Both creep and fatigue strengths of 12% Cr steel are superior to those of 1% Cr-Mo-V steel and the difference is thought the effect of climb and glide controlled creep by solid solution of alloying elements and dispersion of carbides.

세탁용수의 특성에 따른 코코아 오구의 세척성과 색상 (Effect of Washing Solution Characteristics on the Removal and Color of Cocoa Stains)

  • 정혜원;김효정
    • 한국의류산업학회지
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    • 제14권3호
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    • pp.492-500
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    • 2012
  • Cocoa is a popular drink for children and contains healthy polyphenols however; a deep brown stain is left when cocoa is spilled over clothes. The main pigments in cocoa are anthocyanins that change in washing solutions with different alkalinity and metals. The removal and color changes in a cocoa stain after washing with various pH solutions and water hardness were studied. Alkalinity and the water hardness of washing solutions were important factors for the removal of cocoa stains. The removal of cocoa things in washing solutions without detergent was low (and even became negative after removal and darker) in solutions with a pH 9 and above. The cocoa stain was not removed and only the fabric color faded, although the cocoa stained cloth was washed with Korea tap water that has a pH of 7. The cocoa stain removal in detergent solutions was conspicuously higher than for only water. Even in detergent solutions, the cocoa stain removal decreased as water hardness increased. Cocoa stain removal was more effective and the color dimmest when the stained cloth was washed in a solution without the metal cations, and the bleach added with the detergent at a temperature of $40^{\circ}C$ and for longer than 20 minutes. Effective and economical equipment for tap water softening for a washing machine should be developed and used to improve cocoa stain removal.