• Applied Biological Chemistry
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• 제42권3호
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• pp.223-228
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• 1999

제주산 궁천조생 온주밀감의 저장효과를 검토하기 위하여 저장 중 각각 $3^{circ}C$, 90%와 85% 상대습도에서 저온저장하였으며, 습도 조절이 안된 상온저장과 비교하였다. 중량감소는 저장 98일까지 각각 90% 습도에서는 3.40%, 85% 습도에서는 6.92%, 상온저장에서는 11.87%로서 습도가 높을수록 중량감소는 적었다. 그러나 90% 습도에서 저장한 감귤은 저장 98일 이후 부패율이 3.87%에서 급격히 증가하여 126일에 48.75%에 이르렀다. 과육율과 가용성고형물은 저장기간 중 큰 변화를 보이지 않았다. 경도는 저장 중 계속하여 감소하였고, 특히 상온저장에서 감소가 심하였다. 산 함량과 비타민 C 변화는 호흡작용에 의해 저장기간이 경과함에 따라 계속하여 감소하였다. 상온저장에서는 저온저장에 비해 착색이 계속 진행됨을 알 수 있었다. 관능평가와 내용성분을 기준한다면 품질 유지를 위해서는 $3^{circ}C$, 85% 상대습도에서 수확후 100일 정도가 조생온주 밀감의 최적 저장기간으로 판단되었다.

• 대한기계학회논문집A
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• 제34권8호
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• pp.981-987
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• 2010

Split Hopkinson Pressure Bar(SHPB) 실험기법은 고변형률 하중 조건하에서 변형하는 여러 가지 공업 재료의 변형 거동 특성을 규명하는데 가장 널리 사용되는 실험 방법 중의 하나이다. 본 논문에서는 봉을 통하여 전파하는 응력파의 모양과 라이징 시간을 제어할 수 있는 pulse shaper를 사용하는 수정 SHPB 실험기법을 이용하였다. 수정 SHPB 실험 장치에 고온 장치를 부착하고 알루미늄 합금 7075-T6의 고변형률 하에서의 고온 변형거동에 대한 연구를 수행하였다. 고온 수정 SHPB 실험 장치를 이용하여 알루미늄 합금 7075-T6의 온도와 변형률속도에 따른 기계적 특성을 규명하고, 실험적으로 얻어진 데이터를 Johnson-Cook 구성방정식을 적용하여 알루미늄 합금 7075-T6의 동적 거동을 모델 하는 변수를 결정하였다.

• 한국표면공학회지
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• 제32권2호
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• pp.144-156
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• 1999

Thermal Barrier Coating with Functional Gradient Materials (FGM-TBC) can play an important role to protect the parts from harmful environments in high temperatures such as oxidation, corrosion, and wear and to improve the efficiency of aircraft engine by lowering the surface temperature on turbine blade. FGM-TBC can increase the life spans of product and improve the operating properties. Therfore, in this study the evaluations of mechanical and thermal properties of FGM-TBC such as fatigue, oxidation and wear-resistance at high temperatures have been conducted. The samples of both the TBC with 2, 3, 5 layers (YSZ/NiCrAlY) to be produced by Air Plasma Spray method (APS) and the bulk TBC with 6 layers to be produced by Plasma Assisted Sintering method (PAS) were used. Furthermore, residual stress, bond strength, and thermal conductivity were evaluated. The average thickness of the APS was 500$\mu\textrm{m}$ to 600$\mu\textrm{m}$ and the average thickness of the PAS was 3mm. The hardness number of the top layer of APS was 750 Hv to 810Hv and that of PAS was 950 Hv to 1440Hv. The $ZrO_2$ coating layer of APS was composed of tetragonal structure after spraying as the result of XRD analysis. As shown in the results of the high temperature wear test, the 3 layer coating of APS had the best wear resistance at $800^{\circ}C$ and the 5 layer coating of APS had the best wear resistance at $600^{\circ}C$. But, these coatings had the tendency of the low-temperature softening at $300^{\circ}C$. The main mechanism of wear was the adhesive wear and the friction coefficient of coatings was increased as increasing the test temperatures. A s results of thermal conductivity test, the ${\Delta}T$ of the APS coating was increased as number of layer and the range of thermal conductivity of the PAS was $800^{\circ}C$ to $1000^{\circ}C$.

• 한국포장학회지
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• 제15권1호
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• pp.17-23
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• 2009

한국에서 미국으로의 단감의 수출확대를 위하여 미국에서의 단감 생산 및 유통 현황을 현지 방문하여 조사하였다. 그리고 해상을 통한 단감 포장의 시범적 수송과 현지 판매를 수행하여 유통 중의 문제점을 파악하였다. 이러한 조사로부터 고품질 상태로의 단감을 미국에 수출하기 위한 방안을 도출하고자 하였다. 미국 현지에서의 단감 산업은 생산량 증가로 가격이 하락하고 있으며 이에 따른 수지 악화로 재배면적 및 생산량이 감소 추세에 진입하였다. 단감 소비는 현재 아시안에 의하여 주도적으로 이루어지고 있지만 최근 히스패닉과 백인들에 의한 소비도 증가하고 있었다. 타국으로부터 수출되는 감에 비해 한국산 단감은 색도와 당도를 증진시키는 노력이 필요하며 지나치게 대과인 경우는 국내 가격이 높아 가격 경쟁력이 떨어지고 수출확대가 어려운 것으로 나타났다. 대미 수출 단감 포장은 수송 중 저온 컨테이너 별로 온도차가 심하게 발생되었고 온도차가 많은 컨테이너의 과실은 흑변, 연화 등의 발생으로 품질이 크게 저하되었다. 과실의 플라스틱 봉지를 결속하는 상태가 불량하여 포장내 공기조성이 단감저장에 적절한 수준으로 형성되지 않았고(산소농도가 높고 이산화탄소농도가 낮음), 과피흑변 및 흑점, 연화과 등 생리장해과의 발생이 많았다.

• 한국전기전자재료학회논문지
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• 제11권8호
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• pp.581-586
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• 1998

This paper describes athermally stimulated displacement current (TSDC) of arachidic acid(AA) and polyamic acid alkylamine salts(PAAS) Langmuir-Blodgett(LB) films, which is a precursor of polyimide(PI). The TSDC measurements of AA LB film were performed from temperature to about 11$0^{\circ}C$ at a rate of 0.2$^{\circ}C$/ｓ inside a vacuum chamber for a reference. And the TSDC measurements PAAS LB film were performed from room temperature to about 25$0^{\circ}C$ and temperature was increased at the same rate as that of AA LB film. They show that there are TSDC peaks at about 7$0^{\circ}C$ in the arachidic acid LB films, and at about 7$0^{\circ}C$ and 16$0^{\circ}C$ in the PAAs LB films. Results of these measurements indicate the one small peak at 7$0^{\circ}C$ is resulted from a softening of the alkyl group and the large peak at 16$0^{\circ}C$ is possibly due to dipole of C-O group in the PASS molecule. We have calculated the vertical component of the AA and PAAs L film out of the TSDC curves. It shows that the dipole moment of the AA LB film is about 70-mD at 7$0^{\circ}C$. And the dipole moment of PAAS LB film is about 040mD at 7$0^{\circ}C$ and about 200mD at 16$0^{\circ}C$ in the first measurement of TSDC. In the second measurement of TSDC of PASS LB film after cooling down to room temperature, the TSDC peaks are almost disappeared.

• 한국재료학회지
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• 제22권7호
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• pp.342-345
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• 2012

The dielectric properties and phase transformation of poled <001>-oriented $Pb(Mg_{1/3}Nb_{2/3})O_3-x%PbTiO_3$(PMN-x%PT) single crystals with compositions of x = 20, 30, and 35 mole% are investigated for orientations both parallel and perpendicular to the [001] poling direction. An electric-field-induced monoclinic phase was observed for the initial poled PMN-30PT and PMN-35PT samples by means of high-resolution synchrotron x-ray diffraction. The monoclinic phase appears from $-25^{\circ}C$ to $100^{\circ}C$ and from $-25^{\circ}C$ to $80^{\circ}C$ for the PMN-30PT and PMN-35PT samples, respectively. The dielectric constant (${\varepsilon}$)-temperature (T) characteristics above the Curie temperature were found to be described by the equation$(1/{\varepsilon}-1/{\varepsilon}_m)^{1/n}=(T-T_m)/C$, where ${\varepsilon}_m$ is the maximum dielectric constant and $T_m$ is the temperature giving ${\varepsilon}_m$, and n and C are constants that change with the composition. The value of n was found to be 1.82 and 1.38 for 20PT and 35PT, respectively. The results of mesh scans and the temperature-dependence of the dielectric constant demonstrate that the initial monoclinic phase changes to a single domain tetragonal phase and a to paraelectric cubic phase. In the ferroelectric tetragonal phase with a single domain state, the dielectric constant measured perpendicular to the poling direction was dramatically higher than that measured in the parallel direction. A large dielectric constant implies easier polarization rotation away from the polar axis. This enhancement is believed to be related to dielectric softening close to the morphotropic phase boundary.

• Design & Manufacturing
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• 제15권2호
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• pp.23-29
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• 2021

The specific strength of magnesium alloy is four times that of iron and 1.5 times that of aluminum. For this reason, its use is increasing in the transportation industry which is promoting weight reduction. At room temperature, magnesium alloy has low formability due to Hexagonal closed packed (HCP) structure with relatively little slip plane. However, as the molding temperature increases, the formability of the magnesium alloy is greatly improved due to the activation of other additional slip systems, and the flow stress and elongation vary greatly depending on the temperature. In addition, magnesium alloys exhibit asymmetrical behavior, which is different from tensile and compression behavior. In this study, a jig was developed that can measure the plane deformation behavior on the surface of a material in tensile and compression tests of magnesium alloys in warm temperature. A jig was designed to prevent buckling occurring in the compression test by applying a certain pressure to apply it to the tensile and compression tests. And the tensile and compressive behavior of magnesium at each temperature was investigated with the developed jig and DIC equipment. In each experiment, the strain rate condition was set to a quasi-static strain rate of 0.01/s. The transformation temperature is room temperature, 100℃. 150℃, 200℃, 250℃. As a result of the experiment, the flow stress tended to decrease as the temperature increased. The maximum stress decreased by 60% at 250 degrees compared to room temperature. Particularly, work softening occurred above 150 degrees, which is the recrystallization temperature of the magnesium alloy. The elongation also tended to increase as the deformation temperature increased and increased by 60% at 250 degrees compared to room temperature. In the compression experiment, it was confirmed that the maximum stress decreased as the temperature increased.

• 생물환경조절학회지
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• 제25권4호
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• pp.262-269
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• 2016

본 연구는 '상주둥시' 감을 3개월동안 -1, 0.5, $3^{\circ}C$에 저장하면서 감 과실의 과실품질 변화와 저장장해 증상에 미치는 영향을 구명하고자 실시하였다. 저장온도에 따른 감 과실의 에틸렌 발생량은 저장온도가 낮을수록 그 발생량이 낮았으나 호흡율은 영향을 받지 않았다. 과실의 경도는 모든 처리구들에서 저장기간이 길어지면서 감소하였고 저장온도가 높을수록 과실 경도의 저하는 더 빠르게 진행되었다. 또한 저장기간이 길어지고 저장온도가 높을 수록 과실의 연화가 급속히 진행되었다. 과실의 감모율도 저장온도가 높을수록 증가하였고, 가용성 고형물 함량도 저장온도가 낮을수록 더 높게 유지되었다. 감 과실의 과정부와 과실측면의 과피색 $L^*$, $a^*$, $b^*$ 값의 변화는 저장온도 $-1^{\circ}C$와 $0.5^{\circ}C$에서는 저장기간에 따른 차이를 거의 보이지 않았으나, $3^{\circ}C$처리구에서는 과피색의 변화가 현저히 적었다. 저장중 발생하는 생리장해증상인 과피흑변, 과실연화 및 부패정도는 온도가 높을수록 그 증상이 심하게 발생하여 과실품질이 현저히 감소하였다.

• 한국재료학회지
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• 제22권11호
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• pp.591-597
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• 2012

For heat exchanger applications, 2-ply clad materials were fabricated by rolling of aluminum (Al) and mild steel sheets. Effects of annealing temperature on interface properties, especially on inter-layer formation and softening of strain hardened mild-steel, for Al/mild steel clad materials, were investigated. To obtain optimum annealing conditions for the Al/mild steel clad materials, annealing temperature was varied from room temperature to $600^{\circ}C$. At the annealing temperature about $450^{\circ}C$, an inter-layer was formed in an island-shape at the interface of the Al/mild steel clad materials; this island expanded along the interface at higher temperature. By analyzing the X-ray diffraction (XRD) peaks and the energy dispersive X-ray spectroscopy (EDX) results, it was determined that the exact chemical stoichiometry for the inter-layer was that of $Fe_2Al_5$. In some samples, an X-layer was formed between the Al and the inter-layer of $Fe_2Al_5$ at high annealing temperature of around $550^{\circ}C$. The existence of an X-layer enhanced the growth of the inter-layer, which resulted in the delamination of the Al/mild-steel clad materials. Hardness tests were also performed to examine the influence of the annealing temperature on the cold deformability, which is a very important property for the deep drawing process of clad materials. The hardness value of mild steel gradually decreased with increasing annealing temperature. Especially, the value of hardness sharply decreased in the temperature range between $525^{\circ}C$ and $550^{\circ}C$. From these results, we can conclude that the optimum annealing temperature is around $550^{\circ}C$ under condition of there being no X-layer creation.

• 한국재료학회지
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• 제14권1호
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• pp.67-72
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• 2004

The glass-forming conditions are investigated in the $K_2$O-CaO-$SiO_2$ $-P_2$$O_{5}$ system with 10~65 mole% of$ P_2$$O_{5}$. Thermal properties and dissolution properties were investigated according to variation of the SiO and KO contents in selected compositions. The glass formation condition was determined when $K_2$O/$P_2$$O_{5}$ mole ratio 0~0.24, $SiO_2$/($SiO_2$+$P_2$$O_{5}$ ) mole ratio 0～0.29, and CaO/$P_2$$O_{5}$ mole ratio 0~1.00. In the result of the thermal properties, the glass transition temperature($T_{g}$) and softening temperature($T_{s}$ ) were gradually shifted to the lower temperature range with increase of $K_2$O contents. The maximum value of the chemical durability was shown in $K_2$$PO_2$$O_{5}$ mole ratio 0.17 when the $SiO_2$ contents were changed, and $K_2$O was fixed at 10 mole%. Hence the change of the $K_2$O/$P_2$$O_{5}$ mole ratio was found that a new main factor of the chemical durability.