• Title/Summary/Keyword: Softening temperature

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Inhibition of the Texture Softening of Shrimp Litopenaeus vannamei Pressured at High-temperature in a Retort Using a Mixed Solution of Calcium Chloride and Potato Starch (염화칼슘 및 감자전분의 혼합용액을 활용한 고온가압 처리 새우(Litopenaeus vannamei)살의 물성 연화 억제)

  • Choe, Yu Ri;Park, Ji Hoon;Cho, Hye Jeong;Lee, Jung Suck;Kim, Jin-Soo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.55 no.6
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    • pp.817-826
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    • 2022
  • This study was conducted to determinean optimal soaking solution for inhibiting the texture softening of shrimp Litopenaeus vannamei pressured at high temperature (S-P/HT) in a retort, and also to optimize concentrations of 0.5% calcium chloride (CC) and 5.0% potato starch (PS) for preparation of a mixed solution (MS) and soaking time (ST) in the MS. On the basis of the results of expressible drip (4.6%), water holding capacity (95.1%), hardness (18.4 N/cm2) and sensory texture (7.2 score), the MS was found to be the optimal soaking solution for inhibition of texture softening under S-P/HT conditions, The concentrations of CC (X1, %), PS (X2, %), and ST (X3, min) were selected as independent variables, and hardness (Y1), springiness (Y2) and sensory texture (Y3) were selected as dependent variables. The optimal conditions of X1, X2, and X3 were 0.51%, 6.34%, and 364 min, respectively. Under the optimal conditions, the experimental values of Y1, Y2 and Y3 were 18.3±0.8 N/cm2, 4.4±0.3 mm and 7.7±0.2, respectively, which did not diffr significantly from the predicted values (P>0.05). In conclusion, the optimized models of X1, X2, and X3 for the preparation of S-P/HT using CC-PS were suitably fitted.

Preparation of Porous Glass by the Sintering (소결법에 의한 다공질유리의 제조)

  • 박용완;이준영
    • Journal of the Korean Ceramic Society
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    • v.31 no.9
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    • pp.957-968
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    • 1994
  • Manufacturing process of porous glass by the filler method was studied. Commercial soda-lime-silicate glass powder was mixed with inorganic salt as the filler such as KCl, K2SO4, Na2SO4. Sintering shrinkages of mixed powders with the variation of sintering temperature were compared, and the effects of the fillers to shrinkages of mixed powder were increased in the order of Na2SO4${\mu}{\textrm}{m}$ of pore diameter were manufactured when the filler sizes 100~200 ${\mu}{\textrm}{m}$. The open pore volume of porous glass is determined by the quantity of filler and porous glasses having open pore volume between 30 and 70 vol% are available. Available sintering temperature range for preparation of porous glass is from the softening temperature of the glass powder to eutectic melting temperature of DTA curve of mixed powder.

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The Effects of Temperature Conditions on the Tensile Adhesive Characteristic of the Bridge Decks Waterproofing Systems (온도조건이 교면방수시스템의 인장접착특성에 미치는 영향)

  • 이병덕;박성기;김도형;옥창권
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.05a
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    • pp.293-298
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    • 2003
  • In this study, tensile adhesive strength(TAS) test was carreid out for evaluated the effects of temperature conditions(-20, -10, 5, 20, 30, $40^{\circ}C$) on the tensile adhesive characteristics about six waterproofing membranes which were commercially used in bridge decks. And, failure appeariences of waterproofing systems in each temperature were investigated and observed the sawing surfaces of waterproofing systems for whether or not damaged of waterproofing membranes. TAS test results were increased when test temperature was decrease in all waterproofing membrane. The type of failure was ductile in $30^{\circ}C$ and $40^{\circ}C$, but brittle failure below $20^{\circ}C$. This results were shown that if temperature above $30^{\circ}C$ is continued for a long time, waterproofing material will be damaged by softening and a part of membranes were damaged by hot aggregate in SMA. So we will consider the type of asphalt for choice of the waterproofing membranes.

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Presown Seed Treatments to Promote Seed Germination of Zoysiagrass (Zoysia japonica) (한국잔디 종자의 발아율 향상을 위한 파종전 종자처리)

  • 전병삼;강진호;조상철;권혁식;류영섭
    • Korean Journal of Plant Resources
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    • v.14 no.2
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    • pp.175-181
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    • 2001
  • Dormancy of intact zoysiagrass seeds hinders its seed propagation in which presowing seed treatment must be done to overcome it. The study was done to remodel the presowing treatments of zoysiagrass seeds by determining the treatment effects of seedcoat softening, prechilling, drying and combined light treatment with them or during germination stage. Seedcoat softening with different chemicals (NaOH 20%, KOH 20%, $H_2SO_4\;8M, acetone 20%) and periods (10, 30, 60 min.), prechilling with different periods at 3$^{\circ}C$, and drying with 4 hours at 35$^{\circ}C$ was done. Light sources were also applied with 660 nm red LED light, commercial fluorescent and incandescent light and darkness. Germination test was done in alternative day and night temperature of 35 and 2$0^{\circ}C$ to check the daily germination rates. With seeds treated with NaOH 20% for 30 minutes, red and incandescent light showing similar responses inclined their germination rates compared to dark conditions. Drying resulted in its higher rate than non-drying but fluorescent light treatment forced during drying more enhanced the rate than red light. While mean germination rate considering all the seedcoat softening treatment periods was the greatest in $H_2SO_4$ in comparison with NaOH, KOH and acetone, NaOH treatment for 30 minutes showed the best rate among the all the treatment levels. In the conditions of sowing them to no-mulching field, presowing treatment procedure of zoysiagrass seeds was remodeled: the seedcoat softening treatment with NaOH 20% for 30 minutes was done, washed, and chilled at 3$^{\circ}C$ for 2 weeks before dried under 4 hour fluorescent light illumination at 35$^{\circ}C$.

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A Study on Low-Cycle Fatigue Behavior at Elevated Temperature of High Carbon Steel Used For Structural Purpose (構造용高炭素鋼材 의 高溫 低 사이클 피勞擧動 에 關한 硏究)

  • 옹장우;김재훈
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.6 no.2
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    • pp.101-106
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    • 1982
  • This study was undertaken to determine tensile properties and low-cycle fatigue behavior of 0.6%C high carbon steel used of structural purposes at temperatures up to 500.deg.C. In the low-cycle fatigue test the upper limit was decided by elongation(i.e. the total strain range), while the lower limit was defined by the load (i.e. zero load). The following results were obtained. Both, the ultimate tensile strength and low-cycle fatigue resistance attain the maximum values near 250.deg.C. Above this temperature the values decrease rapidly as the temperature increases. The low-cycle fatigue resistance decreases whenever there is an increase of the total strain range. Because the hardness of cycle fatigued specimen correlates cyclic hardening and cyclic softening, therefore the hardness of cycle fatigued specimen is smaller than that of the nonfatigued specimen at room temperature and 500.deg.C but much larger than the hardness of the nonfatigued specimen near 250.deg.C.

Synthesis and Characterization of Cordierite Glass-Ceramics for Low Firing Temperature Substrate: (I) Crystallization and Shrinkage Behavior of $MgO-Al_2O_3-SiO_2$ Glass Powders (저온소결 세라믹 기판용 Cordierite계 결정화유리의 합성 및 특성조사에 관한 연구: (I) $MgO-Al_2O_3-SiO_2$계 유리분말의 결정화 및 수축거동)

  • 이근헌;김병호;임대순
    • Journal of the Korean Ceramic Society
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    • v.29 no.6
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    • pp.451-458
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    • 1992
  • Dense glass-ceramics for low firing temperature substrate were prepared by addition of CeO2 flux to the glass of MgO-Al2O3-SiO2 system. Glass powders were fabricated by melting at 150$0^{\circ}C$ and ball milling. Glass powder compacts were sintered at 800~100$0^{\circ}C$ for 3h. The crystallization and the shrinkage behaviors of glass powder compacts were analyzed by XRD, DTA and TMA. The shrinkage of glass powder compact increased with increasing the amount of CeO2. Because the softening temperature decreased and the crystallization temperature increased with increasing the amount of CeO2. Apparently, addition of CeO2 prevented formation of $\mu$-cordierite phase from the glass-ceramics and improved formation of $\alpha$-cordierite phase. Therefore crystallization properties were enhanced.

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The study of crystallization to Si films deposited using a sputtering method on a Mo substrate (Mo기판 위에 sputtering 법으로 성장된 Si 박막의 결정화 연구)

  • 김도영;고재경;박중현;이준신
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.36-39
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    • 2002
  • Polycrystalline silicon (poly-Si) thin film transistor (TFT) technology is emerging as a key technology for active matrix liquid crystal displays (AMLCD), allowing the integration of both active matrix and driving circuit on the same substrate (normally glass). As high temperature process is not used for glass substrate because of the low softening points below 450$^{\circ}C$. However, high temperature process is required for getting high crystallization volume fraction (i.e. crystallinity). A poly-Si thin film transistor has been fabricated to investigate the effect of high temperature process on the molybdenum (Mo) substrate. Improve of the crystallinity over 75% has been noticed. The properties of structural and electrical at high temperature poly-Si thin film transistor on Mo substrate have been also analyzed using a sputtering method

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Low Temperature Deposition of TiN on the Steel Substrate by Plasma-Assisted CVD (플라즈마 화학증착에 의한 강재위에 TiN의 저온증착)

  • 이정래;김광호;조성재
    • Journal of the Korean Ceramic Society
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    • v.30 no.2
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    • pp.148-156
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    • 1993
  • TiN films were deposited onto high speed steel (SKH9) by plasma assisted chemical vapor deposition (PACVD) using a TiCl4/N2/H2/Ar gas mixture at around 50$0^{\circ}C$. The effects of the deposition temperature, R.F. power and TiCl4 concentration on the deposition of TiN and the microhardness of TiN film were investigated. The crystallinity and the microhardness of TiN films were improved with increase of the deposition temperature. Optimum deposition temperature in this study was 50$0^{\circ}C$, because a softening or phase transformation of the substrate occurred over 50$0^{\circ}C$. A large increase of the film growth rate with a strong(200) preferred orientation was obtained by increasing R.F. power. Much chlorine content of about 10at.% was found in the deposited films and resulted in relatively low average microhardness of about 1, 500Kgf/$\textrm{mm}^2$ compared with the theoretical value(~2, 000Kgf/$\textrm{mm}^2$).

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Three Point Bending Fatigue Property with Heat Treatment Condition in a Powder Metallurgical High Speed Steel JYPS-23 (분말고속도공구강 JYPS-23에서 열처리조건에 따른 3점 굽힘피로특성)

  • 홍성현;배종수;김용진
    • Journal of Powder Materials
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    • v.7 no.3
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    • pp.131-136
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    • 2000
  • The effect of tempering temperature on the three point bending fatigue behavior of a P/M high speed steel JYPS-23 (1.28% C, 4.20% Cr, 6.40% W, 5.00% Mo, 3.10% V, bal. Fe) was investigated. The number of cycles to failure of the specimen austenitized at $1175^{\circ}C$ drastically increased with increasing tempering temperature. As tempering temperature increased from 500 to $620^{\circ}C$, the volume fraction and average size of carbides (MC or M6C) did not significantly changed, while hardness decreased drastically. The reduced hardness is due to the softening of matrix, which increased the resistance of the fatigue crack propagation. For a practical application, powder compacting test were also conducted with the P/M high speed steel punches tempered at 500, 580, and $620^{\circ}C$. The number of compacting cycles to failure of the punches also increased with increasing tempering temperature.

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Quality Change and Weight Loss of Fresh Ginseng Individually Packaged in a Soft Film According to its Storage Condition (연포장재 필름으로 개별포장한 수삼의 저장조건에 따른 외관품질 변화 및 개체무게 감소)

  • 손현주;김은희;이성계;노길봉
    • Journal of Ginseng Research
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    • v.25 no.3
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    • pp.122-126
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    • 2001
  • Fresh ginseng was washed with water and packaged individually in a soft film bag (ONY/LDPE/L-LDPE;200${\times}$300mm, 90$\mu\textrm{m}$), then stored at 25$^{\circ}C$, 10$^{\circ}C$, or 4$^{\circ}C$ to investigate quality and weight changes of the packaged fresh ginseng according to its storage time. Softening was the major phenomenon which influenced on the quality of the packaged fresh ginseng while spoilage and color-change were relatively minor phenomena. There were very good correlations not only between the quality change rate constant and the storage temperature but between the weight change rate constant and the storage temperature. This result suggests that the shelf-life and the weight loss of the packaged fresh ginseng being store at low temperature can be estimated by an accelaerated sotrage test.

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