• The Journal of Advanced Prosthodontics
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• v.14 no.1
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• pp.56-62
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• 2022

PURPOSE. The aim of this study was to investigate shade changes in fully- and pre-crystalized CAD-CAM lithium disilicate crowns after the required and additional firing processes. MATERIALS AND METHODS. One hundred and five crowns of shade A1 with high translucency were milled out of CAD-CAM lithium disilicate blocks and categorized as follows (n = 15): (1) restorations fabricated from Straumann n!ce with no additional sintering process; (2) restorations fabricated from Straumann n!ce with one additional sintering process; (3) restorations fabricated from Straumann n!ce with two additional sintering processes; (4) restorations fabricated from Amber Mill with one sintering process; (5) restorations fabricated from Amber Mill with two sintering processes; (6) restorations fabricated from IPS e.max CAD with one sintering process; (7) restorations fabricated from IPS e.max CAD with two sintering processes. All restorations were evaluated with a color imaging spectrophotometer. RESULTS. All restorations presented some color alteration from the original shade both after a single and after two firing processes. CONCLUSION. The required and additional sintering processes for restorations fabricated with chairside CAD-CAM lithium disilicate blocks cause an alteration of the original shade selected. Shade A1 high translucency restorations tend to change to a more yellowish B1 shade after a sintering process.

• Journal of Powder Materials
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• v.5 no.4
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• pp.324-328
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• 1998

This paper is aimed to study the computer simulation of sintering process for ceramics by Monte Carlo and molecular dynamics methods. Plural mechanisms of mass transfer were designed in the MC simulation of sintering process for micron size particles; the transfer of pore lattices for shrinkage and the transfer of solid lattices for grain growth ran in the calculation arrays. The MD simulation was performed in the case of nano size particles of ionic ceramics and showed the characteristic features in sintering process at atomic levels. The MC and MD simulations for sintering process are useful for microstructural design for ceramics.

• 한국연소학회:학술대회논문집
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• 2012.04a
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• pp.19-20
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• 2012

Flue gas recirculation(FGR) is applied to sintering process to cope with issues including plant efficiency and environmental effects. However, it inevitably brings changes of incoming and outgoing gas conditions as plant configurations. Objective of this study was to build a process model for a sintering bed using a flowsheet process simulator and obtain information of mass and heat balance for gas flows over various process configurations with FGR.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.20 no.6
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• pp.729-734
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• 2011

The full sintering process of zirconia has some extent of shrinkage and the custom abutment design should consider the pre-compensation volume of the shape. In this paper, we concentrated to reveal the asymmetric sintering characteristics. The circular profile of all six samples were measured using the three dimensional coordinate machine. After the full sintering process, the profiles were measured again. The roundness were compared to those of the original shapes and the percent of shrinkage were calculated. On the other hand, surface roughness was also investigated after the full sintering process. The final average surface roughness was improved by the sintering of the machined zirconia surface.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1997.04a
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• pp.53-61
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• 1997

The effect of sintering condition on tribological behavior in the Cu-base sintered friction materials was studied through pin-on-disk type wear tester. Especially, the experiment was focused on making a comparative study between presstwed sintering and pressureless sintering. Pressureless sintering process showes more stable friction coefficient and lower wear rate than pressure sintering process. This result is related to pore size and density of pore in the sintered materials.

• Journal of the Korean Society of Combustion
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• v.16 no.4
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• pp.23-30
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• 2011

In the iron and steel manufacturing, sintering process precedes blast furnace to prepare feed materials by agglomerating powdered iron ore to form larger particles. There are several techniques which have devised to improve sintering production and productivity including flue gas recirculation(FGR) and additive gas enriched operation. The application of those techniques incurs variations of process configurations as well as inlet and outlet gas conditions such as temperature, composition, and flow rate which exert direct influence on reactions in the bed or the operation of the entire plant. In this study, an approach of sintering bed modeling using flowsheet process simulator was devised in consideration of FGR and the change of incoming and outgoing gas conditions. Results of modeling for both normal and FGR sintering process were compared in terms of outgoing gas temperature, concentration, and moisture distribution pattern as well as incoming gas conditions. It is expected to expand the model for various process configurations with FGR, which may provide the usefulness for design and operation of sintering plant with FGR.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.1389-1393
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• 2007

Selective Laser Sintering (SLS) is currently recognized as a leading process in the new field of solid freeform fabrication (SFF). It is used to fabricate in a short time any 3 dimensional shapes by layer-by-layer sintering of polymer, ceramic or metal powder. To develop this SFF system, it needs effective laser scanning path, temperature and z-axis control for lamination. Therefore, in this study, through the application of control algorithm for sintering process have performed, temperature evaluation for sintering process has performed and the manufacturing sample using SLS process.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2012.05a
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• pp.227-228
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• 2012

In interfaces between carbon black or Pt and FTO glass in dye-sensitized solar cell counter electrodes, a marginal resistant channel for electrons, we tried to improve the connection by modifying the sintering process. A stepwise sintering process for carbon black and Pt counter electrodes was applied and its effect on power conversion efficiency was studied. Power conversion efficiencies of built-in DSSC made by a one-step sintering process with carbon black and Pt counter electrodes were about 5.01% and 5.02%, respectively. Cells made with the stepwise sintering process were 5.96% and 6.21%, respectively, indicating an 20% improvement. Fill factor (FF) increased, and it was them main reason for the power conversion efficiency improvement. Step wise sintering increased the adhesion of the interface and reduced the film thickness and surface roughness. As a result, the resistivity of the counter electrode and EIS impedance of DSSCs decreased.

• Journal of Sensor Science and Technology
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• v.30 no.3
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• pp.148-153
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• 2021

During the manufacture of a ZnS lens with excellent transmittance in the mid-infrared region (3-5 ㎛) by the hot-press process, a single-layer sintering method is used in which one lens is manufactured in one process. Additional research is required to improve this single-layer sintering method because of its low manufacturing efficiency. To solve this problem, the variation in optical properties of ZnS lenses with change in sintering temperature was investigated by introducing a Stack sintering method that can sinter multiple lenses simultaneously. A carbon paper was placed between the molded lenses and sintered into five layers. The average permeability of 67% at medium infrared wavelengths of 3-5 ㎛ was excellent under the following sintering conditions: pressure of 50 MPa and temperature of 850℃. This value is 1% less than the average permeability in the case of single-layer sintering of the ZnS lens. It was confirmed that the stack sintering method developed in this study can be used to manufacture a large number of lenses with excellent characteristics in a single process.

• Journal of Powder Materials
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• v.27 no.5
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• pp.365-372
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• 2020

Predicting the quality of materials after they are subjected to plasma sintering is a challenging task because of the non-linear relationships between the process variables and mechanical properties. Furthermore, the variables governing the sintering process affect the microstructure and the mechanical properties of the final product. Therefore, an artificial neural network modeling was carried out to correlate the parameters of the spark plasma sintering process with the densification and hardness values of Ti-6Al-4V alloys dispersed with nano-sized TiN particles. The relative density (%), effective density (g/㎤), and hardness (HV) were estimated as functions of sintering temperature (℃), time (min), and composition (change in % TiN). A total of 20 datasets were collected from the open literature to develop the model. The high-level accuracy in model predictions (>80%) discloses the complex relationships among the sintering process variables, product quality, and mechanical performance. Further, the effect of sintering temperature, time, and TiN percentage on the density and hardness values were quantitatively estimated with the help of the developed model.