• 제목/요약/키워드: Sintering Time

검색결과 673건 처리시간 0.033초

Fabrication of Nano-sized Metal Dispersed Magnesia Based Composites and Related Mechanical and Magnetic Properties

  • Choa, Yong-Ho;Tadachika Nakayama;Tohru Sekino;Koichi Niihara
    • The Korean Journal of Ceramics
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    • 제5권4호
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    • pp.395-399
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    • 1999
  • MgO/metal nanocomposite powder mixtures were prepared by solution chemical processes to obtain suitable structure for ceramic/metal nanocomposites. Nickel or cobalt nitrate, as a source of metal dispersion, was dissolved into alcohol and mixed with magnesia powder. After calcined in air, these powders were reduced by hydrogen. Densified nanocomposites were successively obtained by Pulse Electric Current Sintering (PECS) process. The dispersed metal partical size depended on temperature and time in calcination and reduction processes. The phase analyses in the synthesized powders as a functioni of temperature were tracked using a dynamic high temperature X-ray diffractioni (HTXRD) system. Phase and crystallite size analyses were done using X-ray diffractioni and TEM. The MgO/metal nanocomposites were successfully fabricated, and ferromagnetic responses with enhanced coercive force were also investigated for these composites.

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9.5/65/35 PLZT의 HYSTERESIS와 AGING현상에 관한 연구 (Properties on Hysteresis and Aging phenomenon of 9.5/65/35 PLZT)

  • 이호걸;김상연;송준태
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1993년도 춘계학술대회 논문집
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    • pp.88-91
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    • 1993
  • In this study 9.5/65/35 PLZT was selected which has the excellent quadratic electro-optic property and slim-loop. It was fabricated by the methods of vacuum hot-pressing and sintering. The electrode of color filter was evaporated using the interdigital type masks. Hysteresis and transmission characteristics were measured. The coercive field and the nontransmited field were correlative. Aging effect was measured according to time at same temperature. Wavelengths of RGB were chosen 700[nm] for red, 545[nm] for green and 435[nm] for blue by the standard of the Commission Internationale del Eclaiage.

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알루미나 기판에 스크린 프린팅된 Ag(Ta,Nb)O3 후막의 유전특성 및 초고주파 특성에 대한 연구 (An Investigation on the Dielectric and Microwave Properties of Ag(Ta,Nb)O3 Thick Films on the Alumina Substrates)

  • 이규탁;고중혁
    • 한국전기전자재료학회논문지
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    • 제24권11호
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    • pp.925-928
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    • 2011
  • Perovskite niobates and tantalates have been placed on a short list of functional materials for future technologies. This article was investigated ferroelectric materials $Ag(Ta,Nb)O_3$ thick film. In this study, we have fabricated the $Ag(Ta,Nb)O_3$ thick film on the $Al_2O_3$ substrates by screen printing method. The $Ag(Ta,Nb)O_3$ thick film were fabricated by the mixed oxide method. The sintering temperature and time were 1,150$^{\circ}C$, 2 hr. The electrical properties of $Ag(Ta,Nb)O_3$ thick film were investigated at 30~100$^{\circ}C$.

롤 포밍에 의한 미세 격벽 성형에 대한 연구 (A Study on Forming of Micro Rib Barriers by Roll Forming Technique)

  • 박종진;황한섭
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2003년도 춘계학술대회
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    • pp.1136-1141
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    • 2003
  • Among various methods to manufacture the PDP barrier ribs, the pressing and the roll forming methods are simple and economical because they form the ribs by utilizing the plastic flow of the green tape in a relatively short time without generating air-polluting dusts. In the present study, the roll forming method was investigated by experiments as well as numerical analyses and in result the groove roll and the preform were designed. The effect of draft angle, comer radius, and initial thickness of the green tape on the plastic flow was examined by a series of parametric studies. The preform was recommended to ease the plastic flow into the grooves and to avoid the occurrence of crack during rolling and sintering processes.

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SLS의 공정 파라미터 최적화에 관한 연구 (Optimization of Build Parameters in SLS Process)

  • 허성민;오도근;최경현;이석희
    • 대한기계학회논문집A
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    • 제24권3호
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    • pp.769-776
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    • 2000
  • RP(Rapid Prototyping) technology is gaining its popularity in building a prototype in all industries. SLS(Slective Laser Sintering) is one of RP technologies, which is focused on tooling processes as well as three dimension solid model. There are several factors, the length and the cross-sectional area of a part, that have an effect on build setup in SLS process. In this paper, the computation on geometrical relationship is used to slice STL file and to estimate these factors. Based on these values, the build setup parameters such as the heating temperature, the laser power, and the powder cartridge feed rate are determined by neural network approaches. The test results show that the computation time is saved and the neural network approach is able to apply to get the optimal parameters of build process within an acceptable error rate.

고에너지볼밀법을 이용한 PMN-PZT 세라믹스의 제조와 압전특성 (Preparation and Piezoelectrical Properties of PMN-PZT Ceramics Prepared by High-Energy Ball Milling)

  • 명성재;구본급
    • 한국세라믹학회지
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    • 제42권10호
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    • pp.685-690
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    • 2005
  • Pb(Zr,Ti)$O_{3}$Pb($Mn_{1/3}$$Nb_{2/3}$)$O_{3}$ powder was successfully synthesised by high-energy milling method, and the behavior of low­temperature sintering and piezoelectrical properties of Pb(Zr,Ti)$O_{3}$-Pb($Mn_{1/3}$$Nb_{2/3}$)$O_{3}$ ceramics were investigated as a function of mechanical alloying time. In order to confirm whether the Perovskite phase in this composition was formed by mechanical activation technique or not, we performed X-Ray Diffraction pattern analysis (XRD). The microstructure for the sintered samples were characterized using a Scanning Electronic Microscope (SEM). And the piezoelectrical properties ($k_{p}$ and $Q_{m}$) of the sintered samples was measured using HP 4194A impedance analyzer.

$BaTiO_3$계 SBLC의 표면 재산화 형성 기구 및 전기적 성질 (Surface Reoxidation Mechanism and Electrical Properites of SBLC in $BaTiO_3$ System)

  • 이형규;김호기
    • 한국세라믹학회지
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    • 제23권5호
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    • pp.55-60
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    • 1986
  • A mechanism for formation of surface reoxidation layer in Surface Boundary Layer Capacitor (SBLC) has been studied. SBLC were prepared by reduction of $BaTiO_3$ doped with $Bi_2O_3$ and electrode firing of silver paste containing $Bi_2O_3$ The apparent dielectric constant was in the order of $10^5$ and the insulation resistance larger than $10^6$$\Omega$ It can be expected that $Bi_2O_3$ dopant in $BaTiO_3$ plays the role of inhibition of grain growth and decreasing the resistivity of $BaTiO_3$. In order to confirm the process of surface reoxidation layer effects of atmosphere and annealing time in electrode sintering were investigated.

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용융염 합성법에 의한 반도성 $BaTiO_3$의 PTCR 효과 (PTCR Effects in Molten Salt System Synthesized Semiconductive $BaTiO_3$)

  • 윤기현;오기영
    • 한국세라믹학회지
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    • 제22권3호
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    • pp.13-18
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    • 1985
  • Semiconductive $Ba_{0.9}Sr_{0.1}TiO_3$ was prepared by both the Calcining of mixed Oxides (C. M. O) and the Molten Salt Synthesis(M.S.S) methods to investigate the PTCR effects. In the Molten Salt Synthesis method the temperature of calcination for Synthesis of $BaTiO_3$ could be lowered from 110$0^{\circ}C$ to 80$0^{\circ}C$. The M.S.S Specimens had smaller grain size and more homogeneous size distribution at the same sintering temperature as compared with the C. M. O specimens. The M. S. S. specimens showed greater PTCR effects and current variations in the time vs. current charac-teristics than those of C. M. O Specimens.

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CrN 소결체의 고온 안정성 (High Temperature Stability of Sintered Bulk CrN)

  • 최정호;이동복
    • 한국표면공학회지
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    • 제40권1호
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    • pp.39-43
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    • 2007
  • The pure CrN powders oxidized to $Cr_2O_3$ noticeably above $850^{\circ}C$ in air. When these powders were sintered into bulk samples at $1500^{\circ}C$ under 40 atm of $N_2$ pressure, the CrN phase partly changed into the $Cr_2N$ phase, owing to the partial loss of nitrogen from CrN. When the bulk sample was heated at $1000-1200^{\circ}C$ for 100 hr under vacuum, the CrN phase also progressively changed into $Cr_2N$. At the same time, a relatively thin $Cr_2O_3$ layer formed on the bulk sample due to the reaction of chromium with residual oxygen in vacuum.

현장인화 $SiC-Si_3N_4$ 복합재료의 절삭성능 평가 (Cutting characteristics of in situ toughened $SiC-Si_3N_4$ composite)

  • 김경재;박준석;권원태;김영욱
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 2000년도 추계학술대회논문집 - 한국공작기계학회
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    • pp.386-391
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    • 2000
  • It is known that Si$_3$N$_4$ceramic insert has less hardness than A1$_2$O$_3$ceramic insert. But Si$_3$N$_4$ceramic insert has not only high toughness and strength but also low thermal expansion coefficient, which makes it has longer tool life under thermal stress condition. In this study, commercial Si$_3$N$_4$ ceramic insert and home-made SiC-Si$_3$N$_4$ceramic insert which has different sintering time and chemical composition is tested under various cutting conditions. The experimental result is compared in terms of tool life and cutting force. Generally, As the cutting speed and the feed rate increased, the cutting force and the flank wear increased too. The performance of SiC-Si$_3$N$_4$ceramic insert shows the possibility to be a new ceramic tool.

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