• 한국결정성장학회지
• /
• 제8권3호
• /
• pp.508-512
• /
• 1998

마이크로파(2.45GHz) 에너지를 이용한 소결법으로 $1100^{\circ}C$~$1300^{\circ}C$의 온도범위에서 반도체 세라믹스인 $Mn_3O_4{\cdot}Co_3O_4{\cdot}3NiO$ 조성의 NTC 서미스터를 소결하였으며, 그 전기적 특성을 조사하였다. 소결온도가 높아질수록 소결밀도가 높은 치밀한 소결체를 얻을 수 있었으며, 25~$85^{\circ}C$ 범위의 온도변화에 따른 전기저항변화 특성으로부터 구한 비저항 $B_{25^{\circ/85^{\circ}}$ 정수는 3100~3200K이었다. 마이크로파 하이브리드, 소결법으로 소결된 시편과 일반소결법으로 소결된 시편을 비교하면 소결특성과 전기적물성에서 비슷한 결과를 얻을 수 있었다. 마이크로파 에너지를 이용한 소결공정은 20분 안에 완료되는 짧은 시간의 급속소결법으로 공정 시간과 에너지를 크게 절감할 수 있었다.

• 한국세라믹학회지
• /
• 제39권9호
• /
• pp.890-895
• /
• 2002

$Mg_{0.93}Ca_{0.07}TiO_3(MCT)$와 $(Ca_{0.3}Li_{0.14}Sm_{0.42})TiO_3(CLST)$ 세라믹스를 적층형 경사기능재료 구조로 제조한 뒤 소결시간에 따른 마이크로파 유전특성의 변화를 고찰하였다. 소결시간의 변화에 대하여 유전상수는 거의 일정한 값을 유지하였으나, 품질계수는 밀도와 각 유전체 층에 인가되는 열응력의 변화에 의해 영향을 받았다. 적층형 시편의 밀도가 증가할수록, 각유전체 층에 작용하는 열응력이 감소함에 따라 전체 품질계수 값은 증가하였으며, CLST 보다 열팽창 계수가 작은 MCT층에 인가되는 압축응력의 변화에 대하여 품질계수 값은 민감하게 영향을 받았다. 1300$^{\circ}C$에서 9시간 소결한 적층형 경사기능재료 구조의 시편의 MCT층에 가장 큰 압축응력이 인가되었으며, 이 때 가장 낮은 품질계수를 나타냈다.

• 한국세라믹학회지
• /
• 제26권3호
• /
• pp.297-304
• /
• 1989

The dielectric properties of SrTiO3 GBL Capacitor have been investigaetd as a function of the second heat treatment time and the amount of Ta. The grain size of semiconductive SrTiO3 after sintering at 1,46$0^{\circ}C$ for 4 hours in N2/H2 atmosphere increased as the amount of Ta increased, and then decreased as the amount of Ta exceed 0.01 mole. Also, the dielectric constant after the second heat treatment showed the same tendency. When the semiconductive SrTiO2 was second heat treated at 1,10$0^{\circ}C$ in air with varying time, the dielectric constant increased as the second heat treatment time increased up to 60 minutes, and then decreased as the time became longer than 60 minutes.

• 한국세라믹학회지
• /
• 제30권10호
• /
• pp.852-858
• /
• 1993

The effect of coal tar ptch-impregnated carbon materials which were made from petroleum coke was investigated at various pressure time and impregnation-sintering cycle. As a result, density and bending strength of the carbon materials were remarkably increased in the condition of pressure times of 5hrs and of the cycle of 3rd times. And the value of d002 and Lc of the graphitic carbon sintered at 230$0^{\circ}C$ shwoed 3.387$\AA$ and 167$\AA$, respectively.

• 한국세라믹학회지
• /
• 제32권2호
• /
• pp.227-233
• /
• 1995

By using homestyle microwave oven, Al-Al2O3 powder mixture could be oxidized and sintered into Al2O3 body. The differences in powder characteristics among the differently processed raw materials affect the oxidation and sintering behaviours, and these effects were more pronounced in case of microwave oven than of conventional furnace. Al-Al2O3 powder mixture was oxidized and sintered within 2hrs, which could save both processing time and energy.

• 한국세라믹학회지
• /
• 제24권4호
• /
• pp.392-396
• /
• 1987

Pure barium titanate was sintered at $1340^{\circ}C$ for 2, 4, 8, 16 hr to control their grain size. The measurements of breakdown strength and partial discharge characteristics were performed under rising AC voltage(60Hz). With increase of sintering time, the average grain size was increased and breakdown strength was slightly decreased. Partial discharge in pores was observed under high voltage, and a model of dielectric break down in barium titanate ceramics is proposed.

• 한국분말야금학회:학술대회논문집
• /
• 한국분말야금학회 2005년도 추계학술강연 및 발표대회강연 및 발표논문 초록집
• /
• pp.30-30
• /
• 2005

• 한국초전도학회:학술대회논문집
• /
• 한국초전도학회 2002년도 High Temperature Superconductivity Vol.XII
• /
• pp.77-77
• /
• 2002

• 한국분말야금학회:학술대회논문집
• /
• 한국분말야금학회 2005년도 춘계학술강연 및 발표대회강연 및 발표논문 초록집
• /
• pp.50-51
• /
• 2005

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2007년도 춘계학술대회B
• /
• pp.2222-2227
• /
• 2007

Newly structured metal-supported solid oxide fuel cell was fabricated and characterized by impedance analysis and galvanodynamic experiment. Using a cermet adhesive, thin ceramic layer composed of anode(Ni/YSZ) and electrolyte(YSZ) was joined with STS430 metal support of which flow channel was fabricated. $La_{0.8}Sr_{0.2}Co_{0.4}Mn_{0.6}O_3$ perovskite oxide was used as cathode material. Single cell performance was increased and saturated at operating time to 300hours at 800$^{\circ}C$ because of cathode sintering effect. The sintering effect was reinvestigated by half cell test and exchange current density was measured as 0.005A/$cm^2$. Maximum power density of the cell was 0.09W/$cm^2$ at 800$^{\circ}C$. Numerical analysis was carried out to classify main factors influencing the single cell performances. Compared to experimental IV curve, simulated curve based on experimental parameters such as exchange current density was in good agreement.