• 대한치과기공학회지
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• 제33권4호
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• pp.271-281
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• 2011

Purpose: The aim of this study is to investigate the changes in hardness and microstructure of a dental multipurpose alloy after simulated complete firing with controlled cooling rate and holding time by characterizing the changes in hardness and microstructure after simulated firing with various cooling rates and holding times. Methods: Before hardness testing, the specimens were solution treated and then were rapidly quenched into ice brine. The specimens were completely fired in furnace. Hardness measurements were made using a Vickers microhardness tester. The specimens were examined at 15 kV using a field emission scanning electron microscope. Results: The maximum hardness value was obtained at stage 0 after simulated firing with various cooling rates (quick cooling, stage 0, stage 1, stage 2, stage 3). By the repetitive firing, the hardness of the tested alloy decreased gradually. By holding the specimen at $500^{\circ}C$ for 10-20min after simulated firing, the hardness increased apparently. However, to hold the alloy for long periods of time in the relatively high temperature after simulated firing resulted in the formation of thick oxidation layer. The oxide film formed on the surface of the alloy after simulated complete firing with controlled cooling rate, which was mainly composed of O and Zn. Conclusion: It is reasonable to hold the alloy at $500^{\circ}C$ for 10-20min after complete firing in other to improve the final hardness of the alloy.

• 대한치과재료학회지
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• 제43권4호
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• pp.343-349
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• 2016

This experiment was carried out to examine whether the post-firing heat treatment is effective in increasing the hardness of metal-ceramic alloy of the Pd-Au-Ag-Sn system. Precipitation hardening by holding at $600^{\circ}C$ after simulated complete porcelain firing in a metal-ceramic alloy of the Pd-Au-Ag-Sn system was examined by observing the change in hardness, crystal structure, and microstructure using a hardness test, X-ray diffraction (XRD), and field emission scanning electron microscopy (FE-SEM). The hardness of the alloy increased apparently by holding the specimen at $600^{\circ}C$ for 30 min after simulated complete porcelain firing. The formation of fine grain interior precipitates during holding at $600^{\circ}C$ caused the formation of lattice strain in the grain interior, resulting in apparent hardening. The faster cooling rate (stage 0) during simulated complete porcelain firing resulted in more effective precipitation hardening during holding at $600^{\circ}C$. From the above results, an appropriate post-firing heat treatment, such as holding at $600^{\circ}C$ for 30 min after complete porcelain firing may increase the durability of metal-ceramic prostheses composed of Pd-Au-Ag-Sn alloy.

• 대한치과재료학회지
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• 제42권2호
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• pp.95-106
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• 2015

Hardening mechanism associated with post-firing heat treatment of softening heat treated and then firing simulated Pd-Ag-Au alloy for bonding porcelain was examined by observing the change in hardness, crystal structure and microstructure. By post-firing heat treatment of as-cast, solution treated and pre-firing heat treated specimens at $650^{\circ}C$ after casting, the hardness value increased within 10 minutes. Then, hardness consistently increased until 30 minutes, and gap of hardness value among the specimens was reduced. The increase in hardness after post-firing heat treatment was caused by grain interior precipitation in the matrix. The softening heat treatment did not affect the increase in hardness by post-firing heat treatment. The precipitated phase from the parent Pd-Ag-Au-rich ${\alpha}$ phase with face-centered cubic structure by post-firing heat treatment was $Pd_3$(Sn, In) phase with face-centered tetragonal structure, which has lattice parameters of $a_{200}=4.0907{\AA}$, $c_{002}=3.745{\AA}$. From above results, appropriate post-firing heat treatment in order to support the hardness of Pd-Ag-Au metal substructure was expected to bring positive effects to durability of the prosthesis.

• 대한기계학회논문집B
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• 제27권10호
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• pp.1377-1384
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• 2003

An analysis has been performed for active thermal control of the KOMPSAT monopropellant rocket engine assembly, i.e., dual thruster module(DTM). The main efforts of this work have been directed at determining proper heater sizes for propellant valves and catalyst beds necessary to maintain their temperatures within specified temperature ranges under KOMPSAT environment and operational conditions. The TAS incorporated with TRASYS thermal radiation analyzer was used to establish a complete heat transfer model which allows to predict the DTM temperature as a function of time. The thermal analysis has been performed in transient mode to verify the appropriate power for catalyst bed heaters necessary to increase catalyst bed temperature to the required value within a specified period of time. Similar analysis has been executed to validate the heater power for the thermostatically controlled primary and redundant heater circuits used to prevent hydrazine freezing, i.e., single fault. Moreover the effect of the radiative property of thermal control coating of heat shield was examined. Thruster firing condition was also simulated for the heat soakback condition. As a consequence, all thermal analysis results for DTM satisfactorily met the thermal requirements for the KOMPSAT DTM under the worst case average voltage, i.e. 25 volt.

• 센서학회지
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• 제31권1호
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• pp.51-56
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• 2022

In this study an efficient method for detecting and monitoring engine misfiring, focusing on minute speed changes in the crankshaft is proposed., Its validity is verified using various misfiring cases. Typically, the crankshaft speed fluctuates around the normal value depending on the engine misfiring status. Even a minute speed change in the crankshaft can be estimated by measuring the rotation time of each tooth of the 118-tooth flywheel attached to the crankshaft with a 2-MHz timer. Therefore, a speed pattern for an in-line six-cylinder engine consists of 236 tooth rotation speeds corresponding to the two rotations of the crankshaft, in which all the cylinders complete four-stroke cycle. FFT analysis can reduce the number of components of a speed pattern from 236 to just four major components: - fundamental frequency_(f), 2f, 3f, 6f., - This makes the comparison of the misfiring cases simpler and faster. In the experiment, five engine status cases (one normal firing and, four misfiring cases) were simulated. While the 6f component was the largest for the normal case, the f component increased as misfiring occurred one, two apart, and two consecutive times. The 3D FFT pattern comprising the ratio of f, 2f, and 3f, 6f showed that the distance between the misfiring and normal states was larger