• 한국잠사곤충학회지
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• 제43권1호
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• pp.41-48
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• 2001

The purification, dissolution and powdering of stained waste silk obtained from weaving and dyeing process were studied for the surface modification of textile fabric and plastic materials. The whiteness of stained waste silk could be improved through degumming and bleaching with sodium hydrosulfite. The water-soluble fibroin solution can be obtained by dissoving the degummed waste silk in a boiling solution of 50% calcium chloride for 60 minutes. The salts and heavy metals contained in fibroin solution were removed by electric dialysis, wool fiber filtration and gel filtration chromatography. The fibroin powder was prepared by using a fine grinder after the alkali treatment for weakening the silk fiber. The fine fibroin powder of particle size around 30 ㎛ was obtained with a ultra fine-mill, while it was finer below 10 ㎛ with a ball-mill. The dissolved or powdered silk was applied to the surface of fabric with addition of the binder (a urethane resin). The moisture content of polyester and nylon fabrics treated with the silk solution was improved due to hygroscopic property of silk. The fine fibroin powder mixed with the binder ws coated on the surface of synthetic film by use of the air pressed sprayer. It was revealed that the hygroscopicity as well as the softness of fibroin powder coated film was much improved. Therefore, it is thought that the fine silk fibroin powder is applicable as an coating agent for the surface modification of plastic and synthetic leather.

• Fibers and Polymers
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• 제6권3호
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• pp.269-276
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• 2005

In this study, cross-cultural comparison of sound sensation for Korean traditional silk fabrics between Korea and America was performed and prediction models for sound sensation by objective measurements including sound parameters such as level pressure of total sound (LPT), Zwicker's psychoacoustic characteristics, and mechanical properties by Kawabata Evaluation System were established for each nation to explore the objective parameters explaining sound sensation of the Korean traditional silk. As results, Koreans felt the silk fabric sounds soft and smooth while Americans were revealed as perceiving them hard and rough. Both Koreans and Americans were pleasant with sounds of Gongdan and Newttong and especially Newttong was preferred more by Americans in terms of sound sensation. In prediction models, some of subjective sensation were found as being related mainly with mechanical properties of traditional silk fabrics such as surface and compressional characteristics.

• 복식문화연구
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• 제22권3호
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• pp.431-439
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• 2014

This research verified the usefulness and practicality of citrus peel extract as a natural dye. This study dyed cotton, silk, and cotton/mulberry fiber blended fabrics using citrus peel extract, and measured the dyeability and functional property to verify their usefulness and practicality. The dyeing affinity of the citrus peel extract was measured by dyeing under alkaline conditions to determine the temperature and time for optimal dyeing conditions of the solution. The results show that a temperature and time of $60^{\circ}C$ and 30 minutes were optimal for dyeing cotton fabrics with citrus peel extract, $50^{\circ}C$ and 60 minutes for silk fabrics, and $60^{\circ}C$ and 60 minutes for cotton/mulberry fiber blended fabrics, respectively. In addition the results of measuring the color fastness of the cotton, silk, and cotton/mulberry fiber blended fabrics dyed with the citrus peel extract show that the color fastness was superior for washing, friction, sweat, and water. However, the color fastness for sunlight appeared to be slightly weak. In addition, it was found that fabric dyed with the citrus peel extract showed partial antimicrobial properties. The antimicrobial property appeared the greatest in the silk fabric. The cotton/mulberry fiber blended fabrics had 90% or more Staphylococcus aureus present, but the antimicrobial properties were not high in the cotton fabric. Additionally, the heavy metal content, which is harmful to the human body, appeared to be lower than standard figures, so the dye was found to be innocuous to humans. Therefore, when the results of this study are put together, citrus peel extract is sufficiently useful and practical as an ingredient for a natural dye. Moreover, there is ample possibility to develop citrus peel dyed fabrics as environmentally friendly fashion materials.

• 한국의류학회지
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• 제23권6호
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• pp.898-908
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• 1999

This paper was aimed to identify the hand and sensibility of silk woven fabrics for neckties to find their relationships to the hand and purchasing preferences and to make their image scale. 56 male and female students evaluated 20 specimens with semantic differential scale of 21 hand and 25 sensibility adjectives. Data were analyzed through factor analysis pearson correlational coefficient t-test using PC SAS package. the hand adjectives were grouped as 4 surface property thermal property flexibility and dryness. The sensibility adjectives were modern classic character and natural,. The flat fabrics with warm hand displayed 'modern' sensibility but those with col hand show 'classic' The rough fabrics with warm hand showed 'natural' but those with cool hand showed 'character' The fabrics rated as high hand preference and purchasing preference showed soft and flat hand occuring 'modern' and 'classic' sensibility.

• International Journal of Industrial Entomology and Biomaterials
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• 제13권1호
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• pp.45-50
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• 2006

Papers were prepared from cut cocoons and mulberry branches, which are byproducts from sericulture industry. The long filament of silk should be cut into appropriate length in order to prepare paper and this was achieved by chemical method. By a mixture of sodium hydroxide and sodium carbonate solution, the silk filaments were cut into short fibers (less than 1 mm in length). Since the short silk fibers (sSf) could not bind each other by itself, starch and poly(ethylene oxide)(PEO) were added as a bonding agent. When starch and PEO were used in a ratio of 3:7, the silk papers had optimum mechanical properties for paper. Fibers from the skin of mulberry branches (MBF) were added to sSf to enhance the mechanical properties of pure silk paper. Bleaching of MBF was performed with a mixture of hydrogen peroxide and sodium silicate. The mechanical properties were greatly enhanced and the optimum blend ratio of MBF and sSf were 7:3. The mulberry/silk paper has good absorption property against formaldehyde, and therefore, the paper could be applied as a wall paper for preventing the sick house syndrome.

• 한국염색가공학회지
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• 제5권1호
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• pp.10-18
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• 1993

Epoxy compound was synthesized from bisphellol-A with epichlorophydrine. Epoxy compound and siloxane were emulsified conjugative one or another. The water repellency of silk fabrics was also highly improved by the treatment of epoxy-siloxane mixed emulsions containing stannic chloride and zirconium oxychloride. The maximum wrinkle recovery was obtained from the fabrics treated under the condition 2.5%-epoxy-siloxane emulsion at 16$0^{\circ}C$. The breaking elongation, the reflectance, the tensile strength and the bending properties of silk fabrics were not degraded severely by the treatment of epoxy-siloxane emulsion.

• 한국의류산업학회지
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• 제10권6호
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• pp.1036-1044
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• 2008

This research from analyzing dyed silk fabrics treated with persimmon juice by padding concludes as follows : The add on is increased as the number of padding increase and the color of the dyed fabrics holds red-yellow colors which has low brightness and high chromatic colors. The fabrics dyed with persimmon juice have properties such as 2nd grade of light fastness, 4~5th grade of perspiration fastness and rubbing fastness, and 3~4th grade of washing fastness. The dyed fabrics exposed to UV light have deeper yellow-red color than things exposed to sunlight. The silk fabrics treated premordants have shown strong yellow colors, especially the fabrics added Fe mordant have shown greenish red-yellow colors. As the padding times of dyeing with persimmon juice are increased, strength and water-repellent property are enhanced along warp and weft direction respectively but anti-crease property is decreased. Also, the dyed fabrics have good antibacterial activity and deodorization.

• Biomaterials and Biomechanics in Bioengineering
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• 제1권2호
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• pp.63-71
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• 2014

This study aimed to develop a novel bioactive hybrid xerogel consisting of silk fibroin /$SiO_2-CaO-P_2O_5$ by sol-gel process at room temperature. Scanning electron microscopy (SEM), FT-IR Spectroscopy, pore measurement, mechanical property testing, in vitro bioactivity test and cytotoxicity assay were performed to characterize the xerogel for bone tissue engineering application. We have found that the xerogel possessed excellent pore structures and mechanical property. Once immersed in a simulated fluid (SBF), the xerogel exhibited profound bioactivity by inducing hydroxyapatite layers on its surfaces. The cell toxicity study also demonstrated that there was little toxic to MC3T3-E1 cells. These results indicate that silk fibroin /$SiO_2-CaO-P_2O_5$ hybrid xerogel potentially could be used as a bone tissue engineering material.

• 한국염색가공학회지
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• 제14권3호
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• pp.19-25
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• 2002

Silk/cotton fabrics were treated with butanetetracarboxylic acid(BTCA) under various treating conditions such as concentration, treated time and curing temperatures. Bending property, tensile strength, wrinkle recovery angle, and shrinkage were measured. The BTCA concentration in the saponfication mixture was measured by an isocratic HPLC equipped with the strong cationic exchange column Aminex HPX-87-H and a UV detector. The detected concentration of BTCA was shown in silk side much more than that of cotton side. The bending and shrinkage properties were improved at minimum curing condition and the lower concentration of BTCA. Tensile strength decreased with increasing concentration of BTCA, curing temperature and treated time, while wrinkle recovery angle increased.

• 한국잠사곤충학회지
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• 제39권1호
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• pp.56-61
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• 1997

The silk fibroin solution was prepared and applied to the surface of fabrics for the purpose of weighting as well as a surface modification. The water-soluble fibroin solution can be obtained by dissolving the cocoon fibroin in a boiling solution of 50% calcium chloride for 60 minutes. For the fixation of a water soluble fibroin onto the fabric surface, the various methods were investigated. The fixation can be achieved on a silk fabric by the after treatment with ethanol, stannous choride and methacrylamide. On the other hand, the epichlorhydrin compound is the most promising fixation agent for a cotton fabric. As a result of the examination of property changes, the softness and crease recovery were lessened for a silk crepe fabric by treating with 1-2% fibroin solution, while those properties were improved for a silk knit fabric.