• Title/Summary/Keyword: SiC-AlN composites

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Effect of TiC and AlN on the Wear Behavior and Mechanical Properties of Hypereutectic Al-Si Alloys (과공정 Al-Si 합금의 마모 거동과 기계적 성질에 미치는 TiC와 AlN의 영향)

  • Ju, Seung Hwan;Choi, Jin Myung;Kim, Yong Jin;Park, Ik Min;Park, Yong Ho
    • Korean Journal of Metals and Materials
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    • v.48 no.11
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    • pp.1003-1008
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    • 2010
  • In this study, the effect of the reinforcement on the wear behaviour and mechanical properties of hypereutectic Al-Si alloys was investigated. The Gas atomized hypereutectic Al-20Si alloy powders were mixed with 1, 3, and 5 wt.% AlN and TiC ceramic particles and consolidated by hotpress. The Al-20Si powder has both finely dispersed primary Si phases and eutectic structures. The Al-20Si-AlN, TiC composites showed that the reinforcements were distributed along the boundary of the Al-20Si alloy. The UTS increased with increasing the AlN, TiC contents. At a lower load, with an increasing weight fraction of reinforcements, the wear rate decreased in both composites and the wear mechanism was adhesive wear. At a higher load, the shape of the debris changes the mechanism of the AlN composites to abrasive-adhesion wear and this resulted in an increase of the wear rate.

High Temperature Deformation Behavior of $SiC_p/Al-Si$ Composites ($SiC_p/Al-Si$ 복합재료의 고온변형 특성)

  • 전정식;고병철;김명호;유연철
    • Transactions of Materials Processing
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    • v.3 no.4
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    • pp.427-439
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    • 1994
  • The high temperature deformation behavior of $SiC_p/Al-Si$ composites and Al-Si matrix was studied by hot torsion test in a range of temperature from $270^{\circ}C$ to $520^{\circ}C$ and at strain rate range of $1.2{\times}10_{-3}~2.16{\times}10_{-1}/sec$. The hot restoration mechanisms for both matrix and composites were found to be dynamic recrystallization(DRX) from the investigation of flow curves and microstructural evolutions. The Si precipitates and SiC particles promoted DRX, and the peak strain$({\varepsilon}_p)$ of the composites was smaller than that of the matrix. Flow stresses of $SiC_p/Al-Si$ composites were found to be generally higher than the matrix, but the difference was quite small at higher temperature due to the decrease of capability of load transfer by SiC particles. With increasing temperature, failure strain of matrix and composites are inclined to increase, the increasing value of failure strain for the $SiC_p/Al-Si$ composites was small compared to that of matrix. The stress dependence of both materials on strain rate() and temperature(T) was examined by hyperbolic sine law, $\.{\varepsilon}=A_1[sinh({\alpha}{\cdot}{\sigma})]_n$exp(-Q/RT)

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Wear Behavior of Al/SiC Composites Fabricated by Thermal Spray Process (2) - Effect of Applied Load on Wear Behavior - (용사법에 의해 제조된 Al/SiC 복합재료의 마모거동 (2) - 작용하중의 영향 -)

  • Lee, Kwang Jin;Kim, Kyun Tak;Kim, Yeong Sik
    • Tribology and Lubricants
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    • v.29 no.5
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    • pp.298-303
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    • 2013
  • In this work, the effect of applied load on the wear behavior of Al/SiC composites was studied. Al/SiC composites were fabricated following the thermal spray process. Dry sliding wear tests were performed on these composites under four different applied loads, i.e., 5, 10, 15, and 20 N. The wear behaviors of the composites under these applied loads were investigated using scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). Under applied loads of up to 15 N, the wear rates of Al/SiC composites decreased with an increase in the applied load because of the formation of an adhesion layer on the worn surface. However in the case of an applied load of 20 N, the wear rate was significantly high because the formation and fracture of the adhesion layer were repeated continuously. These results show that the wear behaviors of the tested composites are significantly influenced owing to the applied loads.

Wear Behavior of Al-based Composites according to Reinforcements Volume Fraction (강화상의 분율에 따른 알루미늄기 복합재료의 마모거동)

  • Lee, K.J.;Kim, K.T.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.15 no.5
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    • pp.77-82
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    • 2011
  • SiC particulate reinforced Al matrix composites with different SiC volume fractions were fabricated by thermal spray process. And the dry sliding wear test were performed on these composites using the applied load of 10 N, rotational speed of 30 rpm, radius of rotation 15 mm. Wear tracks on the Al/SiC composites were investigated using scanning electron microscope(SEM) and energy dispersive spectroscopy (EDS). It was observed that wear behavior of Al/SiC composites and formation of MML was changed dramatically according to reinforcement volume fraction.

Fabrication and Mechanical Properties of $SiC_p/Al$ Composites by Pressureless Infiltration Technique (무가압침투법에 의한 $SiC_p/Al$ 복합재료의 제조 및 기계적 특성)

  • Jin, H.G.;Oh, M.S.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.5 no.4
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    • pp.74-81
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    • 2001
  • The infiltration behavior of molten Al-alloy, microstructures, hardness, and the interfacial reactions of $SiC_p/Al$ composites fabricated by the pressureless infiltration technique were investigated. It was made clear that both the weight fraction of SiC reinforcement and additive Mg content considerably influenced on the infiltration behavior of the molten Al-alloy matrix. Complete infiltration of molten Al-alloy achieved under the conditions that weight fraction of SiC content is more than 30wt%, and additive Mg content is more than 9wt%. Interfacial region of Al-alloy matrix and SiC reinforcement phase, $Mg_2Si$ was formed by the reaction between Mg and SiC. Another reaction product AlN was also formed by the reaction between Al-alloy matrix and gas atmosphere nitrogen.

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Fractographic Analysis of Ceramic Composites by Transmission Electron Microscopy using Surface Replication Technique (표면복제법을 이용한 세라믹 복합재료 파괴현상의 투과전자현미경 분석)

  • Jun, Hyeung-Woo;Kim, Gyeung-Ho;Kim, Byung-Ho
    • Applied Microscopy
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    • v.26 no.4
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    • pp.447-456
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    • 1996
  • Fracture surfaces of materials contain useful information ranging from crack path to the mechanism of fracture. Since limitation of electron transparency requires a sample in the form of thin foil for TEM observations, it is impossible to extract such information directly from the fracture surfaces. In this study, the method of surface replication from the ceramic fracture surface is employed to characterize the process of crack propagation in ceramic matrix composites using TEM analysis. The surface replica from the fracture surface in ceramic materials provides detailed surface morphology and more importantly, loosened particles on the fracture surface are collected. Electron diffraction and chemical composition analyses of these particles reveal crack path in the specimen. Furthermore, one can determine the mode of fracture by observing the fracture surface morphology from the image of replica. Two examples are given to illustrate the potential of the surface replication technique. In the first example, apparent toughness increase in $B_{4}C-Al$ composites at high strain rate is investigated by surface replication to elucidate the mechanism of fracture at different strain rates. The polytypes of SiC formed during the sintering of SiC-AlN composite and their effect on the fracture behavior of SiC-AlN composite are analyzed in the second example.

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Mechanical Properties of Silicon Carbide-Silicon Nitride Composites Sintered with Yttrium Aluminum Garnet (YAG상 첨가 탄화규소-질화규소 복합재료의 기계적 특성)

  • 이영일;김영욱;최헌진;이준근
    • Journal of the Korean Ceramic Society
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    • v.36 no.8
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    • pp.799-804
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    • 1999
  • Composites of SiC-Si3N4 consisted of uniformly distributed elongated $\beta$-Si3N4 grains and equiaxed $\beta$-SiC grains were fabricated with $\beta$-SiC,. $\alpha$-Si3N4 Al2O3 and Y2O3 powders. By hot-pressing and subsequent annelaing elongated $\beta$-Si3N4 grains were grown via$\alpha$longrightarrow$\beta$ phase transformation and equiaxed $\beta$-Si3N4 composites increased with increasing the Si3N4 content owing to the reduced defect size and enhanced crack deflection by elongated $\beta$-Si3N4 grains and the grain boundary strengthening by nitrogen incorporation. Typical flexural strength and fracture toughness of SiC-40 wt% Si3N4 composites were 783 MPa and 4.2 MPa.m1/2 respectively.

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High Strength $Si_3N_4/SiC$ Structural Ceramics (고강도 $Si_3N_4/SiC$ 구조세라믹스에 관한 연구)

  • 김병수;김인술;장윤식;박홍채;오기동
    • Journal of the Korean Ceramic Society
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    • v.30 no.12
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    • pp.999-1006
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    • 1993
  • Si3N4(p)-SiC(p) composites were prepared by gas pressure sintering at 190$0^{\circ}C$ for 1 hour. $\alpha$-SiC with average particle size of 0.48${\mu}{\textrm}{m}$ were dispersed from zero to 50vol% in $\alpha$-Si3N4 with average particle size of 0.5${\mu}{\textrm}{m}$. Y2O3-Al2O3 system was used as sintering aids. When 10vol% of SiC was added to Si3N4, optimum mechanical properties were observed; relative density of 98.8%, flextural strength of 930MPa, fracture toughness of 5.9MPa.m1/2 and hardness value of 1429kg/$\textrm{mm}^2$. Grain growth of $\beta$-Si3N4 was inhibited as the amount of added SiC was increased. SiC particles were found inside the $\beta$-Si3N4 intragrains in case of 10, 20 and 30vol%SiC added composites.

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Wear Behavior of Al/SiC Composites Fabricated by Thermal Spray Process (1) - Effect of Sliding Speed on Wear Behavior - (용사법에 의해 제조된 Al/SiC 복합재료의 마모거동 (1) - 미끄럼 속도의 영향 -)

  • Lee, Kwang-Jin;Kim, Kyun-Tak;Kim, Yeong-Sik
    • Tribology and Lubricants
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    • v.27 no.6
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    • pp.351-355
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    • 2011
  • Al/SiC composites were fabricated by thermal spray process, and the dry sliding wear tests were performed using the various sliding speed of 10, 30, 60 and 90 RPM through 1000 cycles. The applied load was 10 N and radius of wear track was 15 mm. Wear tracks on the Al/SiC composites were investigated using scanning electron microscope(SEM) and energy dispersive X-ray spectroscopy (EDS). In the case of sliding speed of 10 RPM, adhesive wear behavior caused by plastic deformation of composits surface was observed. In the cases of sliding speed of 30, 60, 90 RPM, abrasive wear behavior on the adhered layer formed by debris were observed. Through this study, it was found that the wear behavior of Al/SiC composites was mainly influenced by the sliding speed.

Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN Composite (상압소결에 의하여 제조된 SiC-AlN 복합체에서의 고용체 형성과 미세구조)

  • Lee, Jong-Kook;Kim, Duk-Jun;Kim, Hwan
    • Journal of the Korean Ceramic Society
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    • v.33 no.7
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    • pp.785-792
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    • 1996
  • Formation of Solid Solution and Microstructure in Processureless sintered SiC-AlN compo-site using oxides as a sintering aid at 185$0^{\circ}C$ and 195$0^{\circ}C$ Regardless of SiC/AlN ratio in composition most of sintered specimens showed he complex structure mixed with 2H solid solution and SiC particles. High sintering temperature and large AlN content in starting composition enhanced the formation of 2H solid solution in sintered specimen 2H solid solution showed the spherical shape and core-rim structure. AlN content in the core is higher than that in the rim but SiC content . The size of 2H solid solution on fracture showed the transgranular fracture mode compared with the dispersed SiC particles which showed the intergranular fracture mode.

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