• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1999.06a
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• pp.220-224
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• 1999

Sliding wear test was employed to determine the effect of whisker content and orientation on the firiction and wear behavior of SiC whisker reinforced alumina. Composites containing unidirectionally oriented whiskers were prepared by a modified tape casting followed by lamination, binder removal and hot pressing in order to align the whiskers in the tape casting direction. Wear coefficients on three directions were measured; parallel and normal to the tape casting direction on the tape casting surface and normal to lamination direction on surfnce normal to the tape casting direction. In the effect of whisker orientation, the highest wear rate was obtained in the direction parallel tape casting direction and the lowest in the direction normal to lamination direction at all temperatures. Silicon oxide layer amoothing the surface was detected by energy dispersive X-ray analysis on the worn surface.

• Journal of Korea Foundry Society
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• v.20 no.3
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• pp.167-172
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• 2000

Squeeze casting was performed to fabricate the SiC whisker reinforced magnesium matrix composites, and the suitability of the squeeze casting for the production of the sound composites was determined by micro/macro-structures observations and tensile test. The two-directional infiltration of the melt and the removal of air during infiltration using the devised mold were necessary to produce the composites. The pressure of 100 MPa was effective for the production of composites with the SiC whisker volume fraction of 30%, but the pressure should be lower than 50 MPa in case of below 20% in the volume fraction. The SiC whiskers in the squeeze cast composites were randomly and densely aligned, and the SiC whiskers/magnesium interfaces were continuously well-bonded. The elastic modulus, 0.2% proof stress and tensile strength in the composite were about 2.5times, l0times and 4times as large as those of magnesium, respectively, indicating that the squeeze casting sufficiently provides the high strength magnesium composites reinforced with SiC whiskers.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.05a
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• pp.97-100
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• 2002

In this research, the impact behavior of the boundary between MMC-reinforced SiC whisker and Al alloy were studied. It is known that the resultant of the interfacial reaction between SiC whisker and Al alloy has brittle and low toughness property. In this paper, impact behavior of graded MMC & Al alloy shows the interfacial opening at the boundary. Generally this phenomenon is generated by thermal residual stress, brittle interfacial reaction resultant and difference of the deflection. So, these results may be interpreted as a macroscopic method of measuring the interfacial strength between matrix and reinforcement

• Journal of the Korean Ceramic Society
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• v.24 no.4
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• pp.313-320
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• 1987

Fracture toughness of hot pressed cordierite-SiC whisker ceramic composites contained up to 40vol.% SiC whiskers were determined by using the indentation crack length(IC), indentation strengthin-bending(IS), and single-edge notched-beam(SENB) methods. The results were compared to stress intensity factor, KB, at the crack branching boundary measured by using the mirror zone radius (MZ) method. IS method seems to provide a more reasonable estimation of fracture toughness than other methods for these composites.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.9
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• pp.2374-2385
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• 1994

SiCw/Al composite material is especially attractive because of their superior specific strength, specific stiffness, corrosion fatigue resistance, creep resistance, and wear resistance compared with the corresponding wrought Al alloy. In this study, Fatigue crack growth behavior and fatigue crack path morphology(FCPM) of SiC whisker reinforced Al 6061 alloy with 25% SiC volume fraction and Al 6061 allay were performed. Result of the fatigue crack growth test sgiwed that fatigue crack growth rate of SiCw/Al 6061 composite was slower than that of Al 6061 matrix therefore it was confirmed that Sic whisker have a excellent fatigue resistance. And Al 6061 matrix had only FCPM perpendicular to loading direction. On the other hand SiCw/Al 6061 composite had three types in fatigue crack path morphology. First type is that both sides FCPM of artificial notch are perpendicular to loading direction. Second type is that a FCPM in artifical notch has slant angle to loading direction and the other side FCPM is perpendicular to loading direction. Third type is that both sides FCPM of notch have slant angle to loading direction. It was considered that this kinds of phenomena were due to non-uniform distribution of SiC whisker and confirmed by SEM observation for fracture mechanism study.

• Journal of Korea Foundry Society
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• v.21 no.6
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• pp.359-365
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• 2001

The superplastic behavior of whisker reinforced aluminum alloy matrix composites fabricated by squeeze casting as one of high pressure routes was investigated. The preforms of ${\alpha}-Si_3N_4$ and ${\beta}-SiC$ whiskers without any binder as a reinforcement were used. The matrix materials were 2024 and 7075 aluminum alloys. For the purpose of optimum superplastic condition, respectively, the whiskers volume fraction, extrusion temperature, tensile test temperature and initial strain rate were changed. Fracture surface of tested specimens were observed by SEM. By the results, it became possible to produce superplastic composites by applying only a hot extrusion process to composites obtained by the squeeze casting. The superplastic composites developed are ${\alpha}-Si_3N_4w/7075$, ${\alpha}-Si_3N_4w/2024$ and ${\beta}-SiCw/2024$ systems at high strain rate.

• Journal of the Korean Ceramic Society
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• v.45 no.2
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• pp.132-137
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• 2008

The main purpose of this study is enhancing the filtering efficiency, performance and durability of filter by growing SiC whiskers on cordierite honeycomb substrate. The experiment was performed by Chemical Vapor Infiltration (CVI) in order to control pore morphology of substrate. Increasing the mechanical strength of porous substrate is one of important issues. The formation of "networking structure" in the pore of porous substrate increased mechanical strength. The high pressure gas injection to the specimen showed that a little of whiskers were separated from substrate but additional film coating enhanced the stability of whisker at high pressure gas injection. Particle trap test was performed. More nano-particle was trapped by whisker growth at the pore of substrate. Therefore it is expected that the porous cordierite which deposited the SiC whisker will be the promising material for the application as filter trapping the nano-particles.

• Journal of the Korean Ceramic Society
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• v.32 no.10
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• pp.1139-1146
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• 1995

$\beta$-SiC whiskers could be formed from a system of mullite-carbon-hydrogen by VLS mechanism at elevated temperatures. It was considered that methane gases were generated from the reaction of hydrogen gases with carbon black, and were reacted with mullite to produce two kinds of gases; silicon suboxide (SiO) and carbon monoxide (CO) of precursors of SiC. With increasing the synthesizing temperature up to 146$0^{\circ}C$, the formation of $\beta$-SiC whisker increased from 0.58 mg/$\textrm{cm}^2$ to 3.98 mg/$\textrm{cm}^2$ on the basis of unit area of carbon block, and the diameters of whiskers had their uniformity due to the reduction in stacking faults.

• Journal of the Korean Ceramic Society
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• v.36 no.5
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• pp.513-520
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• 1999

Alumina-coated SiC whiskers wee prepared by the calcination (1150$^{\circ}C$, 1h, Ar) of the alumina hydrate layer which was precipitated homogeneously on whisker surface from a solution of Al2(SO4)3 and urea as a precipitant. In addition carbon coated SiC whiskers were prepared by the pyrolysis (1000$^{\circ}C$, 4h Ar) of phenolic resin coated whisker. The effects of coating conditions on the thickness and morphology of the coated layers were examined by SEM and TEM. It was found that Al2O3-coating layers become thinner and more uniform with decreasing the Al2(SO4)3 concentration. Thin (0.075-0.1$\mu\textrm{m}$) and uniformly alumina-coating layers were obtained at the Al2(SO4)3 concentration 0.010mol/l. On the other han carbon-coating layers were uniform but very thin (5-16 nm) in thickness. For thicker carbon-coating layers ethanol as a disperse medium was found to be more efficient compared tousing acetone.

• Journal of Energy Engineering
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• v.2 no.2
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• pp.187-193
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• 1993

Porous matrices to contain and support phosphoric acid were prepared with PTFE as binder and SiC whisker or SiC powders of various particle size for phosphoric acid fuel cell(PAFC). Among the matrix characteristics the most important factors in stack performances were thought to be the bubble pressure and electrolyte wettability And then matrix was constructed to have pore size smaller than that of electrode. The bubble pressures and wettabilities of matrices manufactured with various size of SiC and different PTFE contents were investigated and related with the porosities measured by porosimeter, and then the optimum manufacturing condition of matrix for PAFC was determined.