• Title/Summary/Keyword: SiC 휘스커

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The Basic Study on Fatigue Crack Growth Behavior of SiC Whisker Reinforced Aluminium 6061 Composite Material (SiC 휘스커 보강 Al 6061 복합재료의 피로균열진전 특성에 관한 기초 연구)

  • 권재도;안정주;김상태
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.9
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    • pp.2374-2385
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    • 1994
  • SiCw/Al composite material is especially attractive because of their superior specific strength, specific stiffness, corrosion fatigue resistance, creep resistance, and wear resistance compared with the corresponding wrought Al alloy. In this study, Fatigue crack growth behavior and fatigue crack path morphology(FCPM) of SiC whisker reinforced Al 6061 alloy with 25% SiC volume fraction and Al 6061 allay were performed. Result of the fatigue crack growth test sgiwed that fatigue crack growth rate of SiCw/Al 6061 composite was slower than that of Al 6061 matrix therefore it was confirmed that Sic whisker have a excellent fatigue resistance. And Al 6061 matrix had only FCPM perpendicular to loading direction. On the other hand SiCw/Al 6061 composite had three types in fatigue crack path morphology. First type is that both sides FCPM of artificial notch are perpendicular to loading direction. Second type is that a FCPM in artifical notch has slant angle to loading direction and the other side FCPM is perpendicular to loading direction. Third type is that both sides FCPM of notch have slant angle to loading direction. It was considered that this kinds of phenomena were due to non-uniform distribution of SiC whisker and confirmed by SEM observation for fracture mechanism study.

Preparation and Characterization of Mullite Whiskers (뮬라이트 휘스커의 제조와 특성)

  • Lee, Hong-Lim;Shim, Il-Yong;Kang, Jong-Bong
    • Journal of the Korean Ceramic Society
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    • v.41 no.1
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    • pp.51-56
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    • 2004
  • Mullite whiskers were synthesized using $Al(OH)_3$, amorphous $SiO_2$ and $AIF_3$ as starting materials by a vapor-solid reaction at relatively low temperature of $1100^{\circ}C$. Leaflet Fluorotopaz was observed for the specimen heat-treated at $800^{\circ}C$. Fluorotopaz was decomposed at $1000^{\circ}C$ and only mullite phase was observed for the specimen sintered at $1100^{\circ}C$ and above. It was found that the synthesized mullite at $1200^{\circ}C$ had grown to [001] direction and side planes were the {110}. The distance of (110} plane was $5.34^{\AA}C$. The amounts of $Al_2O_3$ in mullite was 73.56(1.39)wt%.

Thermal Characteristics of SiC Whisker Reinforced $Al_2$O$_3$-SiC Composite (SiC 휘스커 보강 $Al_2$O$_3$-SiC 복합체의 열간특성)

  • 김윤주;나용한
    • Journal of the Korean Ceramic Society
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    • v.35 no.1
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    • pp.1-4
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    • 1998
  • SiC whisker reinforced Al2O3-SiC composite was fabricated by reaction synthesis method whish is cost ef-fective and allows good dispersion of whiskers. Fracture strength at room temperature showed the highest value with 150$0^{\circ}C$ reaction temperature because a lot of SiC whiskers was formed. Fracture strength at 135$0^{\circ}C$ did not show big differences with reaction temperature due to agglomeration of whiskers and formation of sil-icon oxynitride during hot MO(modulus of rupture) test probably promoting grain boundary sliding.

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Synthesis of $\beta$-SiC Whiskers by Decomposition-Carbonization of Mullite (물라이트의 환원분해 및 탄화법에 의한 $\beta$-SiC 휘스커의 합성)

  • 김종엽;남원식;최상욱
    • Journal of the Korean Ceramic Society
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    • v.32 no.10
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    • pp.1139-1146
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    • 1995
  • $\beta$-SiC whiskers could be formed from a system of mullite-carbon-hydrogen by VLS mechanism at elevated temperatures. It was considered that methane gases were generated from the reaction of hydrogen gases with carbon black, and were reacted with mullite to produce two kinds of gases; silicon suboxide (SiO) and carbon monoxide (CO) of precursors of SiC. With increasing the synthesizing temperature up to 146$0^{\circ}C$, the formation of $\beta$-SiC whisker increased from 0.58 mg/$\textrm{cm}^2$ to 3.98 mg/$\textrm{cm}^2$ on the basis of unit area of carbon block, and the diameters of whiskers had their uniformity due to the reduction in stacking faults.

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Characteristics of SiC Whisker-Reinforced LAS Matrix Composites Fabricated by the Mixed Colloidal Route and the Sol-Gel Process (콜로이드 혼합법 및 Sol-Gel 법에 의해 제조한 SiC 휘스커 강화 LAS 기지 복합체의 특성)

  • 김광수;장현명;정창주;백용기
    • Journal of the Korean Ceramic Society
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    • v.28 no.12
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    • pp.1012-1018
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    • 1991
  • SiC whisker-reinforced LAS matrix composites were developed by a mixed colloidal processing route. An optimization of processing conditions was made using the zeta potential data of silica, boehmite, and SiC whisker dispersions. Similarly, the SiC whisker-reinforced composites were also fabricated by the conventional sol-gel process using the hydrolysis-condensation reaction of relevant metal alkoxides. The composites fabricated by the mixed colloidal processing route were characterized by a uniform spatial distribution of SiC whisker throughout the matrix. The fracture toughness increased from 1.3 MPa.m1/2 for the LAS specimen to 5.0 Mpa.m1/2 for the hot-pressed composite (95$0^{\circ}C$ and 20 MPa for 20 min) containing 20 wt% SiC whisker. The increase in fracture toughness appears to result mainly from the crack deflection and the crack bridging by whiskers with some additional toughenings from the whisker pullout and the matrix prestressing mechanisms.

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