• Transactions of Materials Processing
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• v.15 no.8 s.89
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• pp.562-567
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• 2006

Micro-alloyed steel or heat-treatment-free used in clean technology have been replacing for conventional quenched-and-tempered structural steels since the micro-alloyed forging steel was developed in early 1970s in Germany for saving money of heat treatment, simplified process, short delivery and good productivity. In this paper, ball stud assembled in steering system for automobile was selected to compare conventional process making heat treatment with new process using high strength micro-alloyed steel without heat treatment. The conventional process for ball stud was composed of a total of 6 steps including upsetting, forward extrusion, machining, burnishing and tread rolling with heat treatment and shot blasting. As opposed to conventional process, newly proposed process for ball stud using the clean technology without heat treatment is simplified such as forward extrusion, heading, upsetting, forming having a flange shape and tread rolling. Also net shape forming process to achieve specified process not to include machined step fur manufacturing the ball stud was applied to newly simplified process since micro-alloyed steel is difficult to be formed.

• Journal of the Korean Society for Heat Treatment
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• v.20 no.1
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• pp.11-16
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• 2007

The fatigue properties of Ti-Ni shape memory alloy wires were investigated. In Ni-rich Ti-Ni shape memory alloys, $Ti_3Ni_4$ precipitates formed by aging treatments are believed to vary the shape memory and mechanical properties. In this study, the effect of aging temperature and aging time on shape memory properties and fatigue life were investigated using Ti-50.9 at% Ni alloy wires. The specimens were solution-treated at 1073 K for 3.6 ks followed by aging at 573 K, 673 K and 773 K for periods between 3.6 ks and 3600 ks. It was found that the fatigue life under a constant stress decreased with increasing aging temperature. When the specimens were aged at 573 K for periods between 36 ks and 360 ks, superior shape memory and fatigue properties were obtained. The fatigue life also decreased when the test temperature and strain amplitude increased. It was concluded that the fatigue life exhibited a linear relationship with the critical stress for slip.

• Korean Journal of Metals and Materials
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• v.47 no.12
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• pp.881-886
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• 2009

Research into the replacement of injured systems and tissue in the human body is advancing rapidly. Recently, Ti-Ni shape memory alloys have shown excellent biofunctionality related to their shape memory effect and superelasticity. In this study, the effect of an acid or an alkali treatment on the bioactivity in 49Ti-Ni and 51.5Ti-48.5Ni alloys is investigated in an effort to utilize Ti-Ni alloy as a biomaterial. In addition, the biocompatibility in a SBF solution is assessed through in vitro testing. A porous surface was formed on the surface of both alloys after a chemical treatment. According to the in vitro test, apatite formed on the surfaces of both alloys. The forming rate of apatite in the Ti-rich alloy was faster that in the Ni-rich alloy. The formation of apatite provided proof of the bioactivity of the Ti-Ni alloy. A small quantity of Ni was eluted at the initial stage, whereas Ni was not found for 12 days in the Ti-rich alloy and for 8 days in the Ni-rich alloy. In the case of the treated 51.5Ti-Ni alloy, the shape memory property was worsened but the biocompatibility was improved.

• 보존과학연구
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• s.30
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• pp.5-19
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• 2009

This study is about the conservation treatment from 2008 through 2009 of Gilt-Bronze Cap excavated from Andong tumulus at Guildu-ri, Podumyeon, Goheung, Jeonnan. The whole shape of Gilt-Bronze Cap was distorted and destroyed by the earth pressure. For the conservation treatment, first, soil and pollutants came from the findspot were removed. And then to assemble the whole shape of Gilt-Bronze Cap, we carried out the jointing work forming the shape after dismantling. Under that process, the rust of bronze was removed through the microscope at every moment and the gold-plated surface was revealed. Now the conservation treatment was completed and it is expected to perform the scientific research on the manufacturing methods and composition analysis of Gilt-Bronze Cap.

• Journal of the Korean Society for Heat Treatment
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• v.16 no.2
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• pp.71-77
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• 2003

We investigate the phase formation in the compound layer of cast irons during the gaseous nitrocarburising of four different cast irons, that contain different types of graphites in the shape and size. We examine the change in the surface roughness with the nitrocarburising time. The observation of cross-sectional microstructure and X-ray diffraction analysis indicate that the compound layer consists of single ${\varepsilon}-Fe_{2-3}(N,C)$ phase and that its thickness increases in a parabolic manner with the treatment time. The surface roughness parameters, Rz and Ra increase with increasing treatment time. In other words, the roughness parameters increase as the thickness of compound layer increases. The parameters also depend on the shape and size of graphite in the individual cast irons.

• Journal of the Korean Society for Precision Engineering
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• v.19 no.10
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• pp.52-59
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• 2002

The thermo-mechanical characteristics of high temperature NITINOL shape memory alloy were evaluated using DSC with small samples and DMA with three-point bending specimens. The shape memory alloy of 54.4Ni/45.5Ti wt.% was used so that the phase transformation temperatures were in the range of 50~11$0^{\circ}C$. Two types of sample were tested in the experiments corresponding to as-received and annealed conditions. Simple beam bending theory was used to calculate the dynamic moduli of the shape memory alloy. According to the results, a large discrepancy in transformation temperatures was found between DSC and DMA techniques. Annealing treatment was found to suppress the R-phase transformation during cooling and the secondary plateau in the austenite transformation. Such a heat treatment was also significantly influenced to raise the transformation temperatures and the moduli of the shape memory alloy.

• Textile Coloration and Finishing
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• v.13 no.1
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• pp.9-17
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• 2001

The purpose of this study is to present basic data for the enzymatic modification of acetate fabrics. The weight loss and rate of weight loss of acetate fabrics increased with increasing NaOH concentration and treating time. Acetyl value decreased as the weight loss became higher. The weight loss of alkaline-treated acetate fabrics were directly proportional to the concentration and treating time of cellulase. The optimum temperature and pH in cellulase treatment were $55^\circ{C}$ and pH 3.5. The surface shape revealed that density of fiber decreased by alkaline-treatment. With the treating time of cellulase, fibrillation occurred. In case of higher weight loss in alkaline treatment, fibril is removed after 180 min. The tensile strength decreased by alkaline and cellulase treatment. Especially, in case of higher weight loss of alkaline treatment, tensile strength decreased suddenly. Alkaline treatment increased the drapability of acetates, while cellulase treatment increased it initially but decreased gradually with treatment time. The dyeability after alkaline treatment was improved for reactive dye, but deteriorated for disperse dye. The cellulase treatment of acetate lowered the dyeability for both types of dyes.

• Journal of the Korean Society for Heat Treatment
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• v.16 no.5
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• pp.275-280
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• 2003

• Transactions of the Korean Society of Automotive Engineers
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• v.18 no.6
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• pp.38-45
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• 2010

Welding structures are designed to endure its expected life. The most important factors are life. Especially on welded structure, fatigue strength is critical. So this study performed a research on Box and T shape weldment specimen to examine the influence of welding type. In this experiment, the results indicate Box shape was available in more than T shape. Fatigue tests were performed to evaluate the fatigue strength of the both as-welded and statically pre-loaded specimens by 3 point bending load. Fatigue life can be improved by using Ultrasonic Impact Treatment(UIT) effect. Ultrasonic Impact Treatment(UIT) is excellent for eliminating the tensile residual stresses and generating compressive residual stresses which elevate fatigue strength of welded structures. Also, this shows that welding part has better fatigue life and welding was performed well. In this study, to evaluate the Ultrasonic Impact Treatment(UIT) effect, for welding structure, the experiment was conducted at various levels of stress range between 100MPa and 500MPa. From the test results, it was indicated that fatigue performance was improving by Ultrasonic Impact Treatment(UIT)

• Korean Journal of Materials Research
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• v.32 no.10
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• pp.414-418
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• 2022

Magnesium alloy is the lightest practical metal. It has excellent specific strength and recyclability as well as abundant reserves, and is expected to be a next-generation structural metal material following aluminum alloy. This paper investigated the possibility of thin plate fabrication by applying a overheating treatment to the melt drag method, and investigating the surface shape of the thin plate, grain size, grain size distribution, and Vickers hardness. When the overheating treatment was applied to magnesium alloy, the grains were refined, so it is expected that further refinement of grains can be realized if the overheating treatment is applied to the melt drag method. By applying overheating treatment, it was possible to fabricate a thin plate of magnesium alloy using the melt drag method, and a microstructure with a minimum grain size of around 12 ㎛ was obtained. As the overheating treatment temperature increased, void defects increased on the roll surface of the thin plate, and holding time had no effect on the surface shape of the thin plate. The fabricated thin plate showed uniform grain size distribution. When the holding times were 0 and 30 min, the grain size was refined, and the effect of the holding time became smaller as the overheating treatment temperature increased. As the overheating temperature becomes higher, the grain size becomes finer, and the finer the grain size is, the higher the Vickers hardness.