• Title/Summary/Keyword: Sewage samples

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Evaluation and application of pretreatment methods for pharmaceuticals and personal care products in the solid phase of sewage samples (하수처리시설 고상시료 중 잔류의약물질 분석을 위한 전처리법 평가 및 적용)

  • Park, Junwon;Kim, Changsoo;Ju, Byoungkyu;Lee, Wonseok;Chung, Hyenmi;Jeong, Dong-Hwan
    • Journal of Korean Society of Water and Wastewater
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    • v.32 no.6
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    • pp.559-572
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    • 2018
  • The aim of this study was to evaluate pretreatment methods for 27 pharmaceuticals and personal care products (PPCPs) in various sewage samples using a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) and online solid-phase extraction with LC-MS/MS. Extraction efficiencies of PPCPs in the solid phase under different experimental conditions were evaluated, showing that the highest recoveries were obtained with the addition of sodium sulfate and ethylenediaminetetraacetic acid disodium salt dehydrate in acidified conditions. The recoveries of target compounds ranged from 91 to 117.2% for liquid samples and from 61.3 to 137.2% for solid samples, with a good precision. The methods under development were applied to sewage samples collected in two sewage treatment plants (STPs) to determine PPCPs in liquid and solid phases. Out of 27 PPCPs, more than 19 compounds were detected in liquid samples (i.e., influent and effluent) of two STPs, with concentration ranges of LOQ-33,152 ng/L in influents and LOQ-4,523 ng/L in effluents, respectively. In addition, some PPCPs such as acetylsalicylic acid, ibuprofen, and ofloxacin were detected at high concentrations in activated sludge as well as in excess sludge. This methodology was successfully applied to sewage samples for the determination of the target compounds in STPs.

Optimum Sewage Discharge Strategy for Coastal Waters

  • Kang, Yun-Ho;Lee, Moon-Ock
    • Environmental Sciences Bulletin of The Korean Environmental Sciences Society
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    • v.10 no.S_3
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    • pp.97-106
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    • 2001
  • To improve the water quality, particularly for sea bathers, the behaviour of wastewater from sewage outfalls in water adjacent to Swansea, UK, was studied using a mathematical model. The water quality in the sewage receiving basin was determined using factors like the outfall diffuser location(distance from land boundary), sewage treatment scheme, discharge time, and bacteria decay rate, etc. With respect to these factors, an optimal strategy for sewage discharge was then investigated to minimize bacteria levels along the bathing beaches. As water quality criteria, predicted faecal coliform levels were monitored along the coast adjacent to the outfall locations. The resultant values were compared with EC Mandatory(<2000, 95 % of 20 samples) and Guideline Standards(< 100, 80 % of 20 samples). For the advective-diffusion equation, the non linear advective terms were represented using the ULTIMATE algorithm and the third-order accurate QUICKEST scheme to avoid numerical diffusion. Details of the simulation results are then presented as an optimal policy for sewage discharge in the region.

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Fuel Characteristics of Sewage Sludge in a Fluidized Bed Incinerator (유동상 소각로에서 하수 슬러지 연료 특성)

  • Choi, Jin-Hwan;Choi, Sang-Min
    • 한국연소학회:학술대회논문집
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    • 1999.10a
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    • pp.81-91
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    • 1999
  • Fuel characteristics of sewage sludge as required for the fluidized bed incinerators have been evaluated. Sewage sludge is basically a solid fuel with high percentage of moisture. Moisture content of the fuel directly affects the heating value of the fuel and the exhaust gas composition. When the sludge of transported into the incinerator, sludge cake is subject to the mixing, break-up and heat-up. Fluidization process would enhance these physical processes. The sludge fuel could then undergo the moisture evaporation and devolatilization process. Subsequent oxidation of volatiles as well as the remaining char would then follow. Sludge samples are characterized with high percentage of volatiles out of total combustibles. Quantitative understanding of above listed subprocesses would certainly help in the utilization of fluidized bed incinerators. A limited set of fuel characterization tests including calorimetric analysis, proximate analysis, elemental analysis and thermogravimetric analysis were conducted for the selected sludge samples. The measurement reasults of sludge samples were reported along with some published data. Limited experience in the actual incinerator plant is also presented.

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Effect of slag on stabilization of sewage sludge and organic soil

  • Kaya, Zulkuf
    • Geomechanics and Engineering
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    • v.10 no.5
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    • pp.689-707
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    • 2016
  • Soil stabilization is one of the useful method of ground improvement for soil with low bearing capacity and high settlement and unrequired swelling potential. Generally, the stabilization is carried out by adding some solid materials. The main objective of this research was to investigate the feasibility of stabilization of organic soils and sewage sludge to obtain low cost alternative embankment material by the addition of two different slags. Slags were used as a replacement for weak soil at ratios of 0%, 25%, 50%, 75% and 100%, where sewage sludge and organic soil were blended with slags separately. The maximum dry unit weights and the optimum water contents for all soil mixtures were determined. In order to investigate the influence of the slags on the strength of sewage sludge and organic soil, and to obtain the optimal mix design; compaction tests, the California bearing ratio (CBR) test, unconfined compressive strength (UCS) test, hydraulic conductivity test (HCT) and pH tests were carried out on slag-soil specimens. Unconfined compressive tests were performed on non-cured samples and those cured at 7 days. The test results obtained from untreated specimens were compared to tests results obtained from soil samples treated with slag. Laboratory tests results indicated that blending slags with organic soil or sewage sludge improved the engineering properties of organic or sewage sludge. Therefore, it is concluded that slag can be potentially used as a stabilizer to improve the properties of organic soils and sewage sludge.

Gas Transmit Characteristic of Waste Recycling a Large Landfill Cover (폐기물 재활용 대형복토재의 가스투과 특성)

  • Jung, Ha-Ik;Song, Bong-Joon;Kim, Sang-Keun;Kang, Suk-Joo;Lee, Jae-Young
    • Proceedings of the Korean Geotechical Society Conference
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    • 2005.03a
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    • pp.1396-1399
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    • 2005
  • Gas permeability of the solidified sewage sludge needs to be characterized in order to use as a large-scale landfill cover material. Four different types of the samples were prepared for gas permeability experiments: (1) granite soil, (2) dried sewage sludge, (3) solidified sewage mixed with slag and (4) solidified sewage mixed with granite soils. The experimental instrumentation and measurement devices were newly designed and created to effectively evaluate gas permeability of the samples.

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Detection and phylogenetic analysis of norovirus from individual septic tanks in the drainage basin of the coastal area located in the Jaran Bay of Korea

  • Ham, In Tae;Kim, Byeo Ri;Park, Yu Jeong;Jung, Yeun Joong;Park, Kunbawui;Kwon, Ji Young;Mok, Jong Soo;Yu, Hongsik
    • Fisheries and Aquatic Sciences
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    • v.24 no.1
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    • pp.10-18
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    • 2021
  • Norovirus (NoV) prevalence was investigated in 100 sewage samples collected from 35 individual septic tanks around the drainage basin of Jaran Bay, Korea in January, May, and July of 2017. Genotypes and diversity of NoV strains detected in sewage samples were also assessed using the conventional RT-PCR and phylogenetic analysis. NoV GI or GII were detected in 22 (22.0%) and 24 (24.0%) samples, respectively. Thirteen genotypes were identified with three dominant genotypes (GI.9, GII.5 and GII.17) and GII.17 showed relatively higher prevalence during the survey period. GII.17 strains were clustered into recombinant type variant or NoV GII.17 Kawasaki variant. NoV GII.17 strains were considered emergent epidemic variants with widespread circulation. NoV surveillance strategy should include both environmental (sewage) and clinical data to reveal minor NoV genotypes likely cause of asymptomatic or underreported infections in the local population.

Estimation of polycyclic aromatic hydrocarbons emission from sewage sludge of sewerage treatment plants in Korea

  • Kim, Dong-Hwan;Hwang, Jong-Seob;Lee, Min-Hee;Ok, Gon
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2003.11a
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    • pp.85-88
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    • 2003
  • Polycyclic aromatic hydrocarbons (PARs) are an important group of organic contaminants present in sewage sludge, due to their persistence, toxic, bioaccumulative and long range transfer. These characters make themselves as Persistent Organic Pollutants(POPs) in Long Range Transboundary Air Pollutions convention(LRT AP) of Europe. A method of the gas chromatographic-mass spectrometric (GC-MS) determination of PARs present in sewage sludge was developed and applied to analyzed samples from five sewerage treatment plants (SWTPs), having different treatment types. PARs were extracted from freeze-dried samples by toluene 16 hours in a soxhlet extraction system. The sludge extracts were cleaned-up by an activated silica gel column chromatography. The sum of the 16 US Environmental Protection Agency PARs sewage sludge samples varied from 2.44 to 4.82 ${\mu}g$/g. Concentration of emission carcinogen PARs(PARcarc), such as Benzo(a)anthracene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Benzo(a)pyrene, Dibenzo(a, h)anthracene and Indeno(1, 2, 3-cd)pyrene ranged from 0.62 to 1.03 ${\mu}g$/g. The total amount of PAHs emission from sewage sludge in Korea was calculated as a top-down approach. PARs and $\sum$PAHcarc from sewage treatment plants had several pathway each by-products. In the ocean dumping, PAHs and $\sum$PAHcarc emissions were 1155.95 kg/year and 5040.32 kg/year. In recycle, PAHs and $\sum$PAHcarc emissions were 98.36 kg/year and 428.87 kg/year. In the landfill, PAHs and $\sum$PAHcarc emissions were 190.40 kg/year and 830.21 kg/year. In the incineration, PAHs and $\sum$PAHcarc emission were 33.10 kg/year and 830.21 kg/year. (In case of incineration, the whole provisions of PARs and $\sum$PAHcarc contained to flowed in sludge was supposed to be exhausted to environment through exhaust after incineration.)

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Estimation of polycyclic aromatic hydrocarbons emission from sewage sludge of sewerage treatment plants in Korea

  • Kim, Dong-Hwan;Hwang, Jong-Seob;Lee, Min-Hee;Ok, Gon
    • Journal of Environmental Science International
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    • v.12 no.11
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    • pp.1167-1171
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    • 2003
  • Polycyclic aromatic hydrocarbons (PAHs) are an important group of organic contaminants present in sewage sludge, due to their persistence, toxic, bioaccumulative and long range transfer. These characters make themselves as Persistent Organic Pollutants(POPs) in Long Range Transboundary Air Pollutions convention(LRTAP) of Europe. A method of the gas chromatographicmass spectrometric (GCMS) determination of PAHs present in sewage sludge was developed and applied to analyzed samples from five sewerage treatment plants (SWTPs), having different treatment types. PAHs were extracted from freeze-dried samples by toluene 16 hours in a soxhlet extraction system. The sludge extracts were cleaned-up by an activated silica gel column chromatography. The sum of the 16 US Environmental Protection Agency PAHs sewage sludge samples varied from 2.44 to 4.82 $\mu\textrm{g}$/g. Concentration of emission carcinogen PAHs(PAHcarc), such as Benzo(a)anthracene, Benzo(b)f1uoranthene, Benzo(k)f1uoranthene, Benzo(a)pyrene, Dibenzo(a,h)anthracene and Indeno( 1,2,3-cd)pyrene ranged from 0.62 to 1.03 $\mu\textrm{g}$/g. The total amount of PAHs emission from sewage sludge in Korea was calculated as a top-down approach. PAHs and $\Sigma$PAHcarc from sewage treatment plants had emitted to environment by several pathway. The highest amount of emission to the environment was remarked in the ocean dumping(PAHs and $\Sigma$PAHcarc emissions were 1155.95 kg/year and 5040.32 kg/year, respectively).

Bacterial load and drug resistance in sewage from industrially polluted regions of South Gujarat region

  • Aneree Desai;Srivathsa Nallanchakravarthula
    • Advances in environmental research
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    • v.12 no.1
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    • pp.1-15
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    • 2023
  • Wastewater of anthropogenic origin is known to harbor various bacteria that are known to be of potential risk to human health and environment. It is of utmost importance to monitor such water sources. Coliforms present in the sewage water samples of municipal sewage treatment plants located at three different places in the South Gujarat region (Surat, Navsari and Vapi) of India were analyzed for their coliforms load as well as tested for their drug resistance. Using cultivation-based techniques microbial load and drug resistance (Amoxicillin, Tetracycline, Ciprofloxacin, Erythromycin, Trimethoprim and Sulphamethoxazole) were analyzed. Water treatment statistically significantly decreased the bacterial load in Vapi and Navsari samples. The optical density of with and without antibiotics of all the three locations was shown to increase significantly after 72 hours. Of all the isolates tested, except isolate 'VA5' (resisted up to 90 ㎍ of Ampicillin) all other isolates resisted 256 ㎍ concentration of antibiotics tested. This study indicates that the sewage water is being contaminated with drugs and/or antibiotics due to industrial and/or anthropogenic activities. Regular monitoring of the water quality is required followed by implementation of environmental laws for reducing the pollutants, that are of human health and environment concern.

Distribution of sewage-derived organic matter using fecal sterol in Masan Bay, Korea (마산만의 하수기인 유기물 fecal sterol의 분포)

  • Choi Min-Kyu;Moon Hyo-Bang;Kim Sang-Soo;Lee Yoon
    • Journal of Environmental Science International
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    • v.14 no.5
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    • pp.481-490
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    • 2005
  • Surface sediments and seawater were sampled at Masan and Haengam Bays of Korea, to evaluate contamination by sewage-derived organic matter using fecal sterols, Six stream-water samples into Masan and Haengam Bays were also sampled. Total concentrations of eight sterols (coprostanol, epichloestanol, epicoprostanol, cholesterol, cholestanol, brassicasterol, stigmasterol and $\beta-sitosterol$) were in the range of $1,274\~4,768{\mu}g/g$ dry weight in suspended particulate from the stream-water, $292\~2,244{\mu}g/g$ dry weight in suspended particulate from the seawater and $4.5\~27.2{\mu}g/g$ dry weight in the sediments. Although sterol compositions in sediments, seawater and stream-water were different, cholesterol was the predominant sterol in all samples. The proportion and concentration of coprostanol, a sewage tracer, in stream-water was much higher than those in sediment and seawater. The sterol levels including coprostanol in the sediments and seawater were higher at inner basin than at the outer bay. Some molecular indices and multivariate statistical analysis were used to assess the origin of these sterols and sewage contamination in the study area. The sterol composition patterns in stream-water were mainly associated with contamination by sewage-derived organic matters and those of seawater were associated with the activities of marine-originated organisms. Sterol levels in the sediments were both from the sewage input through stream-water and the marine- originated organisms. This survey suggests that the main source/route of sewage-derived organic matters in Masan Bay is the input of stream-water into the bay.