• 제목/요약/키워드: Set value test

검색결과 605건 처리시간 0.024초

ABS수지 중 polybrominated diphenyl ether(PBDE)류 분석 숙련도 평가 및 정확도 향상 (Evaluation of proficiency and improvement of accuracy on the analysis of brominated flame retardants (PBDEs) in ABS polymer)

  • 유제훈;김달호
    • 분석과학
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    • 제28권6호
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    • pp.446-452
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    • 2015
  • 본 숙련도 시험 프로그램은 ABS (acrylonitrile-butadiene-styrene) 수지 중 브롬계 난연제 PBDE들에 대한 국내 시험소들의 분석능력을 평가하고 향상시키기 위해 ISO/IEC 17043에 준하여 한국표준과학연구원(KRISS)이 수행하였다. 숙련도시험 물질은 PBDE류 (BDE-154, 183, 206, 209)가 첨가된 10 그램의 알갱이 형 ABS였으며 KRISS에서 균질성과 안정성을 확인한 후 사용되었다. KRISS에서는 확립한 국가 표준을 기반으로 숙련도시험 물질에 포함된 각 PBDE들의 인증값을 계산하였으며 숙련도 시험의 설정값으로 하였다. 숙련도 시험에는 16개 시험소들이 참여하였으며 측정방법은 각 시험소들이 서비스에 사용하는 일상적인 방법을 사용하도록 하였다. 참여 시험소들의 분석 능력을 평가하기 위해 ISO/IEC 17043의 z-score법을 사용하였으며 비밀보장을 위해 각 참여 시험소에 고유번호를 부여하였다. z-score는 이상치를 제외한 참여자들의 표준편차를 사용하여 계산하였다. 본 논문에서는 숙련도 시험의 결과, 참가 실험실 평가결과 그리고 숙련도시험을 통한 정확도 향상에 대하여 기술하였다.

Effect of acidic solutions on the microhardness of dentin and set OrthoMTA and their cytotoxicity on murine macrophage

  • Oh, Soram;Perinpanayagam, Hiran;Lee, Yoon;Kum, Jae-Won;Yoo, Yeon-Jee;Lim, Sang-Min;Chang, Seok Woo;Shon, Won-Jun;Lee, Woocheol;Baek, Seung-Ho;Kum, Kee-Yeon
    • Restorative Dentistry and Endodontics
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    • 제41권1호
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    • pp.12-21
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    • 2016
  • Objectives: To evaluate the effects of three acids on the microhardness of set mineral trioxide aggregate (MTA) and root dentin, and cytotoxicity on murine macrophage. Materials and Methods: OrthoMTA (BioMTA) was mixed and packed into the human root dentin blocks of 1.5 mm diameter and 5 mm height. Four groups, each of ten roots, were exposed to 10% citric acid (CA), 5% glycolic acid (GA), 17% ethylenediaminetetraacetic acid (EDTA), and saline for five minutes after setting of the OrthoMTA. Vickers surface microhardness of set MTA and dentin was measured before and after exposure to solutions, and compared between groups using one-way ANOVA with Tukey test. The microhardness value of each group was analyzed using student t test. Acid-treated OrthoMTA and dentin was examined by scanning electron microscope (SEM). Cell viability of tested solutions was assessed using WST-8 assay and murine macrophage. Results: Three test solutions reduced microhardness of dentin. 17% EDTA demonstrated severe dentinal erosion, significantly reduced the dentinal microhardness compared to 10% CA (p = 0.034) or 5% GA (p = 0.006). 10% CA or 5% GA significantly reduced the surface microhardness of set MTA compared to 17% EDTA and saline (p < 0.001). Acid-treated OrthoMTA demonstrated microporous structure with destruction of globular crystal. EDTA exhibited significantly more cellular toxicity than the other acidic solutions at diluted concentrations (0.2, 0.5, 1.0%). Conclusions: Tested acidic solutions reduced microhardness of root dentin. Five minute's application of 10% CA and 5% GA significantly reduced the microhardness of set OrthoMTA with lower cellular cytotoxicity compared to 17% EDTA.

건조방법에 따른 브라운소스의 품질 특성 (Physicochemical Properties of Brown Sauce according to Drying Methods)

  • 이종필;김동석;최수근;윤광섭;정명훈
    • 한국식품조리과학회지
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    • 제27권1호
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    • pp.75-84
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    • 2011
  • The aim of this study was to develop a convenient brown sauce product with long shelf life that has similar taste and quality characteristics with sauce used in restaurants. Response surface analysis was carried out to optimize brown sauce. Extracted brown sauce powder was subjected to hot air drying, infrared drying, freeze drying, and spray drying to determine the appropriate drying method for brown sauce manufacturing. The optimum extraction conditions were set by superimposing and reading each reaction surface that satisfied all of the sensory characteristics such as color, smell, taste, concentration, and overall preference level in order to set the optimum conditions for brown sauce production. The optimum extraction conditions for brown sauce were determined to be heating time 30 min, gelatin addition quantity 9.00%, and tomato paste addition quantity 11.25%. Reliability test showed a similar value to the predicted scope when compared to the experimental value obtained under the same conditions as the predicted value according to RSM (response surface methodology), enabling verification of the derived regression formula. Product powder of ideal brown sauce by heating, infrared radiation, freezing, and spray drying and investigate result for functional tests of color, flavor, taste, viscosity, overall acceptability and show highly acceptability on powder by infrared rays and freeze-drying methods. Especially, infrared radiation method resulted in favorable color and flavor values while freeze-drying method produced good taste and viscosity values and high overall acceptability. Therefore, infrared radiation drying method and freeze-drying method to product powder.

말뚝 시공관리를 위한 비접촉식 관입량 측정장치 활용에 관한 연구 (A Study on Non-contact Penetration and Rebound Measurement Device for Quality Control in Driven Piles)

  • 서승환;김주형;최창호;정문경
    • 한국지반공학회논문집
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    • 제38권11호
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    • pp.97-106
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    • 2022
  • 국내 매입말뚝 시공방법은 선굴착 후 최종단계의 항타 관입량으로 관리하는 것이 일반적이다. 관입량은 오래전부터 수기 측정방식에 의해 이루어지고 있으며, 작업자의 안전문제와 측정값의 신뢰도 부족 등에도 작업성의 한계와 비용 문제로 자동화 기술이 적용되지 않고 있다. 본 연구에서는 비접촉식 말뚝 관입량 측정 장치를 개발하고 기존 장치와 비교계측을 통해 현장 성능을 검증하였다. 또한 관입량 측정장치를 활용하여 현장 품질관리 방법에 대해 분석하였다. 실제 현장 실험을 통해 개발 장치를 활용한 관입량 측정과 수정 Hiley공식 및 동적감쇠계수 산정을 통해 보다 신뢰도 높은 지지력 추정이 가능한 것을 확인하였다. 연구결과에 따라 각 현장마다 수행된 동재하시험으로 부터 현장 보정 절차가 이루어지면 보다 신뢰성 높은 지지력 추정이 가능하며, 실제 현장에서는 동재하시험이 수행되지 않은 말뚝에 대해서도 지지력 관점의 말뚝 시공관리에 활용할 수 있을 것으로 판단된다.

Evidence gathering for line based recognition by real plane

  • 이재규;류문욱;이장원
    • 한국HCI학회:학술대회논문집
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    • 한국HCI학회 2008년도 학술대회 1부
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    • pp.195-199
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    • 2008
  • We present an approach to detect real plane for line base recognition and pose estimation Given 3D line segments, we set up reference plane for each line pair and measure the normal distance from the end point to the reference plane. And then, normal distances are measured between remains of line endpoints and reference plane to decide whether these lines are coplanar with respect to the reference plane. After we conduct this coplanarity test, we initiate visibility test using z-buffer value to prune out ambiguous planes from reference planes. We applied this algorithm to real images, and the results are found useful for evidence fusion and probabilistic verification to assist the line based recognition as well as 3D pose estimation.

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TFIDF를 이용한 키워드 추출 시스템 설계 (Design of Keyword Extraction System Using TFIDF)

  • 이말례;배환국
    • 인지과학
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    • 제13권1호
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    • pp.1-11
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    • 2002
  • 본 논문에서는 먼저 Anchor Text의 단어들이 키워드로 적합한지 TFIDF를 이용하여 테스트하였다. 그 결과는 가중치가 높아서 키워드로 적합한 단어가 있었는가 하면. 아예 문서에 나오지도 않는 단어가 있어 키워드로 적합하지 않은 단어도 있었다. 이를 해결하기 위하여 새로운 키워드 추출 방법을 제시하였다. 본 논문에서는 적합하지 않은 키워드를 제거함으로써 새로운 키워드를 만들어 내고 TFIDF값을 각 키워드의 가중치로 이용하여 Ranking이 가능하게 하였다. 이렇게 추출된 키워드는 기존의 방법보다 정확도가 높아졌음 증명했다.

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오프셋 인쇄 잉크의 유화 속도에 영향을 미치는 인자에 관한 연구 (A Study on the Factors Determining the Emulsion Velocity of Off-Set Ink)

  • 김인겸;김성빈;김종래
    • 한국인쇄학회지
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    • 제19권1호
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    • pp.28-41
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    • 2001
  • Rheological properties of ink and Ink-Water balance are the important factors in lithographic printing. Laboratory test method which determines the emulsification rate of dampening solution and ink has been described. The emulsification theory and laboratory test method deduced from Surland and it has become a useful tool for the industry. The effects of pH value and surface tension of dampening solution on the emulsification rate has been tested by many researcher. In this paper we focused on the factors which influence in the emulsification such as pH and surface tension of dampening solution and emulsifying temperature. To study on the factors determining the emulsion velocity, we have measured water pickup and calculated emulsion velocity constant 'k' and activation energy.

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철도차량 완충기 패드용 고무소재 수명예측 (Useful Lifetime Prediction of Coupling Rubber Pad for Railway Vehicles)

  • 우창수;박현성;박동철
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2008년도 춘계학술대회 논문집
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    • pp.923-931
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    • 2008
  • Coupling rubber pad are important components in railway vehicles. It can be used for reduce shock, vibration and noise. Simple tension, equi-biaxial tension and pure shear test were performed to acquire the coefficient of rubber material which were Mooney-Rivlin and Ogden model. The finite element analysis was executed to evaluate the behavior of deformation and stress distribution by using the commercial finite element analysis code. Useful life evaluation are very important in design procedure to assure the safety and reliability of the rubber components. In this paper, useful life prediction of rubber pad for railway vehicle were experimentally investigated. Accelerated heat-aging test for rubber material were carried. Compression set results changes as the threshold are used for assessment of the useful life and time to threshold value were plotted against reciprocal of absolute temperature to give the Arrhenius plot.

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프로필렌 냉매의 응축열전달 특성에 관한 실험적 연구 (Condensing Heat Transfer Characteristics of Propylene Refrigerant)

  • 이호생;김재돌;윤정인
    • 설비공학논문집
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    • 제16권7호
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    • pp.639-644
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    • 2004
  • This paper deals with the heat transfer characteristics of R-1270 (Propylene), R-600a (Iso-butane) and R-290 (Propane) as an environment friendly refrigerant and R-22 for condensing. The experimental apparatus has been set-up as a conventional vapor compression type heat pump system. The test section is a horizontal double pipe heat exchanger. A tube diameter of 12.70 mm with 1.32 mm wall thickness is used for this investigation. The test results showed that the local condensing heat transfer coefficients of hydrocarbon refrigerants were higher than that of R-22. The average condensing heat transfer coefficient was obtained with the maximum value in R-1270 and the minimum one in R-22. Comparing the heat transfer coefficient of experimental results with that of other correlations, the presented results had a good agreement with the Cavallini-Zecchin's correlation. It reveals that the natural refrigerants can be used as substitute for R-22.

Evaluation of the reproducibility of various abutments using a blue light model scanner

  • Kim, Dong-Yeon;Lee, Kyung-Eun;Jeon, Jin-Hun;Kim, Ji-Hwan;Kim, Woong-Chul
    • The Journal of Advanced Prosthodontics
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    • 제10권4호
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    • pp.328-334
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    • 2018
  • PURPOSE. To evaluate the reproducibility of scan-based abutments using a blue light model scanner. MATERIALS AND METHODS. A wax cast abutment die was fabricated, and a silicone impression was prepared using a silicone material. Nine study dies were constructed using the prepared duplicable silicone, and the first was used as a reference. These dies were classified into three groups and scanned using a blue light model scanner. The first three-dimensional (3D) data set was obtained by scanning eight dies separately in the first group. The second 3D data set was acquired when four dies were placed together in the scanner and scanned twice in the second group. Finally, the third 3D data set was obtained when eight dies were placed together in the scanner and scanned once. These data were then used to define the data value using third-dimension software. All the data were then analyzed using the non-parametric Kruskal-Wallis H test (${\alpha}=.05$) and the post-hoc Mann-Whitney U-test with Bonferroni's correction (${\alpha}=.017$). RESULTS. The means and standard deviations of the eight dies together were larger than those of the four dies together and of the individual die. Moreover, significant differences were observed among the three groups (P<.05). CONCLUSION. With larger numbers of abutments scanned together, the scan becomes more inaccurate and loses reproducibility. Therefore, scans of smaller numbers of abutments are recommended to ensure better results.