• Proceedings of the Membrane Society of Korea Conference
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• 2004.05a
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• pp.183-186
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• 2004

Nano particles-containing CMS membranes were prepared by pyrolysis of polyimides dispersed uniformly with precursors and their gas separation performances were examined, to elucidate the permeation mechanism and to further improve the gas separation performance. Consequently, it was suggested that the separation performance could be controlled by doping nano-particles in the CMS membranes, and that optimization of various factors, such as the size, content, and dispersion state of the nano particles would contribute for further improvement of the gas separation performance.

• Progress in Superconductivity and Cryogenics
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• v.24 no.3
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• pp.19-23
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• 2022

We have been developing a magnetic separation device that can be used in low magnetic fields for paramagnetic materials. Magnetic separation of paramagnetic particles with a small particle size is desired for volume reduction of contaminated soil in Fukushima or separation of iron scale from water supply system in power plants. However, the implementation of the system has been difficult due to the needed magnetic fields is high for paramagnetic materials. This is because there was a problem in installing such a magnet in the site. Therefore, we have developed a magnetic separation system that combines a selection tube and magnetic separation that can separate small sized paramagnetic particles in a low magnetic field. The selection tube is a technique for classifying the suspended particles by utilizing the phenomenon that the suspended particles come to rest when the gravity acting on the particles and the drag force are balanced when the suspension is flowed upward. In the balanced condition, they can be captured with even small magnetic forces. In this study, we calculated the particle size of paramagnetic particles trapped in a selection tube in a high gradient magnetic field. As a result, the combination of the selection tube and HGMS (High Gradient Magnetic Separation-system) can separate small sized paramagnetic particles under low magnetic field with high efficiency, and this paper shows its potential application.

• Progress in Superconductivity and Cryogenics
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• v.25 no.3
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• pp.13-17
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• 2023

Magnetic separation technology for small paramagnetic particles has been desired for the volume reduction of contaminated soil from the Fukushima nuclear power plant accident and for the separation of scale and crud from nuclear power plants. However, the magnetic separation for paramagnetic particles requires a superconducting high gradient magnetic separation system applied, hence expanding the bore diameter of the magnets is necessary for mass processing and the initial and running costs would be enormous. The use of high magnetic fields makes safe onsite operation difficult, and there is an industrial need to increase the magnetic separation efficiency for paramagnetic particles in as low a magnetic field as possible. Therefore, we have been developing a magnetic separation system combined with a selection tube, which can separate small paramagnetic particles in a low magnetic field. In the previous technique we developed, a certain range of particle size was classified, and the classified particles were captured by magnetic separation. In this new approach, the fluid control method has been improved in order to the selectively classify particles of various diameters by using a multi-stage selection tube. The soil classification using a multi-stage selection tube was studied by calculation and experiment, and good results were obtained. In this paper, we report the effectiveness of the multi-stage selection tube was examined.

• Journal of ILASS-Korea
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• v.7 no.2
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• pp.7-15
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• 2002

A particle flow visualization, electrostatic charging measurement and separation of triboelectrically charged particles in the external electric field by a fluidized bed tribocharger are conducted for the removal of PVC particles from mixed waste plastics. The laboratory-scale triboelectrostatic separation system consists of the fluidized bed tribocharger, a separation chamber, a collection chamber and a controller. PVC and PET particles can be imparted negative and positive surface charges respectively due to the difference of triboelectric charging series between particles and particles in the fluidized bed tribocharger, and can be separated by passing them through an external electric field. To visualize these charged particles, He-Ne laser is used with cylindrical lenses to generate a sheet beam. In the charging measurement, the particle motion analysis system (PMAS), capable of determining particle velocity and diameter. is used to non-intrusively measure particle behavior in high strength electric field. The average charge-to-mass ratios of PVC and PET particles are $1.4\;and\;1.2{\mu}C/kg$, respectively. The highly concentrated PVC (91.9%) can be recovered with a yield of about 96.1% from the mixture of PVC and PET materials for a single-stage processing. The triboelectrostatic separation system using the fluidized tribocharger shows the potential to be an effective method for removing PVC from mixed plastics for waste plastic recycling.

• Journal of the Korean Applied Science and Technology
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• v.28 no.3
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• pp.306-312
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• 2011

In this study, we are crystallized to the low density polyethylene (LDPE) micro-particles in $n$-dodecanol solution by thermally induced phase separation(TIPS) method. The Low density polyethylene micro-particles is used in a wide variety of polymer coatings and industrial application. The utility of that for a particular application depends on a number of factors such as the particle size and distribution, and chemical composition of the materials. However, there are still needs for new methods of preparation which will provide the structure with unique sizes. The widely used processes for micro-size particles are crystallization method and thermally induced phase separation. TIPS process based on the phase separation mechanism was performed for the LDPE system which undergoes liquid-solid phase separation. Effects of various operating parameters were examined on the structure variation of the particles. Professionality, take-up speed and crystallization rate depended on temperature and concentration of polymer in solution.

• Journal of the Korean Applied Science and Technology
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• v.28 no.4
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• pp.386-392
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• 2011

We are crystallized to the linear low density polyethylene(LLDPE) particles by a thermally induced phase separation(TIPS). TIPS process based on the phase separation mechanism was performed for the LLDPE system which undergoes liquid-solid phase separation. The linear low density polyethylene particle formation occurred by the nucleation and growth mechanism in the metastable region. Although the growth rates depended on the experimental conditions such as the polymer concentration and temperature, the particles were larger when the polymer concentration was higher or temperature was higher. The particles were observed by SEM. The LLDPE particle size distribution became broader when the polymer concentration was higher.

• Resources Recycling
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• v.6 no.1
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• pp.17-22
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• 1997

An electromagnetic fluidized bed was proposed for the continuous separation of magnetic particles from the fine a admixtures with nonHmagnetic particles. The effects of operating variables on the magnetic fraction in the separated p particles were examined, including superficial gas velocity, mixing fraction of magnetic particles (= 100-mixing fraction of n non-magnetic particles) in the admixture, and electric current supplied to the electwmagnet. It was found that the s separation was possible when a magnetic force formed by the electromagnets works on the magnetic particles over the hydrodynamic force caused by a gas stream for fluidizing the fine admixture.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.13 no.6
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• pp.304-308
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• 2003

By controlling the internal pressure in the cyclone separator, we investigated the separation charateristics of $Al_2O_3$, $Fe_2O_3$ particles with the internal pressure variation. 3-dimensional Langrangian approach was applied for the analysis of the particles separation, and then the minimum cut diameter of the separated particles and the separation rate were calculated through tracking the particle trajectories. The density of the argon gas for transporting particles was decreased corresponding the pressure decrease, consequently, caused the internal pressure drop in the cyclone separator. For that reason the finer particles were separated as the pressure was changed from an atmospheric pressure to an low pressure. Specifically, at 50 torr pressure, $Al_2O_3$ particles of the size of about 4 $\mu\textrm{m}$ and $Fe_2O_3$particles of about 3 $\mu\textrm{m}$ could be separated.

• Journal of Mechanical Science and Technology
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• v.18 no.7
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• pp.1236-1245
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• 2004

In this study, an optical imaging method was developed for the measurements of the sizes and velocities of droplets in sprays. Double-exposure single-frame spray images were captured by the imaging system. An image processing program was developed for the measurements of the sizes and positions of individual particles including separation of the overlapped particles and particle tracking and pairing at two time instants. To recognize and separate overlapping particles, the morphological method based on watershed segmentation as well as separation using the perimeter and convex hull of image was used consecutively. Better results in separation were obtained by utilization of both methods especially for the multiple or heavily-overlapped particles. The match probability method was adopted for particle tracking and pairing after identifying the positions of individual particles and it produced good matching results even for large particles like droplets in sprays. Therefore, the developed optical imaging method could provide a reliable way of analyzing the motion and size distribution of droplets produced by various sprays and atomization devices.

• Journal of Korean Society on Water Environment
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• v.37 no.1
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• pp.10-19
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• 2021

In the flotation process to remove microplastic (MP) particles, the attachment and separation efficiency is determined by the basic physicochemical characteristics of MP particles as well as bubbles. To evaluate the flotation characteristics of MP particles, we carried out a series of simulations using the population balance (PB) model. The initial attachment coefficient (αo) of MP particles was in the range of 0.2-0.275, and it was slightly lower than that of typical particles, such as clay, debris and algae particles, which exist in water bodies, αo, 0.3-0.4. The relative bubble number (RBN) attached to the surface of the typical number of bubbles was 0.30 and 0.32 for MP 30 ㎛ and MP 58 ㎛, respectively. In comparison, the RBN of larger MP particles (138 ㎛) was as high as 0.53. Furthermore, smaller microbubbles were required to separate properly or additional treatment needed to be applied to enhance collision and attachment efficiency since the flotation of MP particles was found to be difficult to treat as high-rate. As a result of comparing the removal rate (experimental value) of MP particles obtained from the batch-type flotation apparatus and the flotation removal rate (predicted value) of MP obtained through the PB model, the final particles by the particle size of MP overall except for the initial separation time area. With respect to the removal efficiency, the observed and predicted values were similar, and it was confirmed that the floating separation characteristics and evaluation of the MP particles through the PB model could be possible.