• Title/Summary/Keyword: Sedimentation of particles

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A Study on the Yeonpyo-beob for the Explanation of the Manufacturing Method of Traditional Pigments (전통 안료 제법 규명을 위한 연표법 연구)

  • Kang, Yeong Seok;Jeong, Hye Young
    • Journal of Conservation Science
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    • v.35 no.6
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    • pp.664-669
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    • 2019
  • Yeonpyo-beob is a method of manufacturing pigments using bamboo trunk and glue solution. Glue solutions of concentrations 1, 5, and 10% were employed to manufacture pigments, and the characteristics of pigment manufacturing were analyzed according to these concentrations. The pigment manufacturing process can be divided into holding and drying phases. The holding phase involves the sedimentation of relatively large particles, whereas the drying phase involves the sedimentation of small particles. The layers formed during the drying phase have almost similar forms regardless of the concentration of the glue solution. If the concentration of the glue solution is low in the holding phase, the particles are mixed and the formation of a layer is difficult. In contrast, when the concentration of the glue solution is higher, the layer of the pigment is more distinct. These results confirmed that the differences in viscosity due to the variation in the concentration of the glue solution affect the sedimentation velocity of the pigment particles, thereby affecting the formation of the layer of the pigment and the pigment manufacture. Consequently, applying 10% glue solution to reduce the sediment velocity is deemed suitable for the stratification of the pigment particles and the manufacture of pigments.

Characterization of CdS-quantum dot particles using sedimentation field-flow fractionation (SdFFF) (침강 장-흐름 분획법을 이용한 CdS 양자점 입자의 특성 분석)

  • Choi, Jaeyeong;Kim, Do-Gyun;Jung, Euo Chang;Kwen, HaiDoo;Lee, Seungho
    • Analytical Science and Technology
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    • v.28 no.1
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    • pp.33-39
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    • 2015
  • CdS-QD particles are a nano-sized semiconducting crystal that emits light. Their optical properties show great potential in many areas of applications such as disease-diagnostic reagents, optical technologies, media industries and solar cells. The wavelength of emitting light depends on the particle size and thus the quality control of CdS-QD particle requires accurate determination of the size distribution. In this study, CdS-QD particles were synthesized by a simple ${\gamma}$-ray irradiation method. As a particle stabilizer polyvinyl pyrrolidone (PVP) were added. In order to determine the size and size distribution of the CdS-QD particles, sedimentation field-flow fractionation (SdFFF) was employed. Effects of carious parameters including the the flow rate, external field strength, and field programming conditions were investigated to optimize SdFFF for analysis of CdS-QD particles. The Transmission electron microscopy (TEM) analysis show the primary single particle size was ~4 nm, TEM images indicate that the primarty particles were aggregated to form secondary particles having the mean size of about 159 nm. As the concentration of the stabilizer increases, the particle size tends to decrease. Mean size determined by SdFFF, TEM, and dynamic light scattering (DLS) were 126, 159, and 152 nm, respectively. Results showed SdFFF may become a useful tool for determination of the size and its distribution of various types of inorganic particles.

Theory of Coagulation(I) Coagulation Theory Including Hydrodynamics and Interparticle Forces (응집의 이론 (I) - 수리동역학과 입자간 작용력을 고려한 응집의 모델 -)

  • Han, Moo Young
    • Journal of Korean Society of Water and Wastewater
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    • v.9 no.3
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    • pp.65-77
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    • 1995
  • The kinetics of flocculation of heterodisperse suspension like those in water treatment plants and natural water system are usually described by the Smoluchowski equation, which incorporates collision frequency functions for particle collisions by Brownian motion, fluid shear, and differential sedimentation. These collisionfrequeney functions have been based on a rectilinear view of collisions, i.e., one that ignores short-range forces and changes in fluid motion as particles approach one another. In this research, a curvilinear approach, i.e., one that accounts for hydrodynamic forces and particle interaction in the collision of two different size particles is developed. Collision efficiency factors of each mechanism can be calculated by trajectory analysis (fluid shear and differential sedimentation) or the solution of diffusion equation (Brownian motion). The results are presented as a set of corrections to the rectilinear collision frequency functions for each mechanism.

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Separation and Characterization of Dust and Ground Water Particulates Using Gravitational SPLITT Fractionation.

  • Lee, Seung Ho;Park, Hui Yeong;Lee, Sang Geun;Yong, Seong Gwon;Eum, Cheol Hun
    • Bulletin of the Korean Chemical Society
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    • v.22 no.6
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    • pp.616-622
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    • 2001
  • Split-flow thin (SPLITT) cell Fractionation(SF) is a technique that allows separation of particulates and macromolecules into two fractions. A gravitational SF(GSF) system is constructed and tested for its applicability for separation of dust and ground water particulates. When tested with polystyrene latex particles, experimental data were in good agreements with theory. The 9.8 and 21.4㎛ polystyrene particles were successuflly separated in a continuous mode, where the mixture is continuously fed into the GSF channel allowing separation in a large sacle. The GSF system is successfully applied to continuous separation of dust and ground water particels based on the sedimentation coefficient, which is closely related to the particle size. The separations were confirmed by microscopy and energy-dispersive X-ray (EDX) analysos.

A study of Sedimentation Processes of Saemangeum Reclamation( I ) - A study of Sedimentation Processes before Saemangeum Reclamation - (새만금간척 퇴적과정에 관한 연구( I ) -새만금간척 시행 전을 중심으로-)

  • Shin, Moon-Seup
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.44 no.4
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    • pp.62-74
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    • 2002
  • The purpose of this study is to find the variation of sedimentation patterns before Saemangeum reclamation. Residual flow before Saemangeum reclamation was calculated diagnostically from the observed water temperature and salinity data in May 1992 by the Marine Development Institute of Kunsan National University and wind data which were obtained from spring 1969 through winter 1977 by the Gunsan Meteorological Observatory. Three dimensional movements of injected particles due to currents, turbulence and sinking velocity are tracked by the Euler-Lagrange method. Calculated sedimentation patterns of riverine materials are highly similar to the observed ones. When suspended sediments with the size of soil grain of 60 ${\mu}m$ are injected from the Mangyeong River, their dispersion range of sediment is about 25km for 24 hours after the injection, while about 35km for 72 hours after the injection. When suspended sediments with the size of soil grain of 200 ${\mu}m$ are injected, their dispersion range of sediment is about 18km for 24 hours after the injection, while about 21km for 72 hours after the injection.

Analysis and Estimation of Reservoir Sedimentation Using Remote Sensing and GIS

  • Sungmin Cho
    • International Journal of Internet, Broadcasting and Communication
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    • v.15 no.4
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    • pp.199-204
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    • 2023
  • Periodic assessment of reservoir capacity is essential for better water resources management and planning for the future water use. Reservoirs and water storage structures raised on the rivers are subjected to sedimentation and he sedimentation is caused by deposition of eroded sediment particles carried by the streams. Knowledge of reservoir sedimentation is important to estimate avaliable storage capacity for optimum reservoir operation and scheduling water release. In recent years, remote sensing and GIS techniques have emerged as an important tool in carrying out reservoir capacity analysis and water management. The reduction in storage capacity as compared to the original capacity at the time of reservoir impounding is indicative of sediment deposition. In this study, the application of GIS and remote sensing techniques were applied to assess the sediment deposition, losses in the reservoir storage and the revised cumulative capacity. Satellite images covering Pyodongdong reservoir were analyzed using Erdas Imagine and ArcGIS softwares.Cumulative capacities at different levels were also calculated and we estimated that the revised live storage was 84.2Mft3 in 2021 and 64.3Mft3 in 2022 while the original capacity was 22.8 and 53.6Mft3 in 2021 and 2022.

Dispersion stability of ultra-fine $BaTiO_3$ suspensions in aqueous medium

  • Chun, M.P.;Chung, Y.B.;Ma, Y.J.;Cho, J.H.;Kim, B.I.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.15 no.6
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    • pp.239-243
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    • 2005
  • The effect of pH and particle size on the dispersion stability of ultra-fine $BaTiO_3$ suspensions in aqueous medium have been investigated by means of zeta potential, sediment experiments, and powder properties (particle analysis, specific surface area) etc. Zeta potential as a function of pH for two particles of different size increases from -75 to +10 mV with decreasing pH from 8.5 to 1.4. The curve of zeta potential for small particle (150 nm) has slow slope than that of large particle (900nm), giving IEP (isoelectric point) value of pH=1.6 for small particle and pH=1.9 for large particle respectively, which means that it is more difficult to control zeta potential with pH fur small particle than large particle. The dispersion stability of $BaTiO_3$ particles in aqueous medium was found to be strongly related with the agglomeration of colloidal suspensions with time through the sedimentation behaviors of colloidal particles with time and pH value.

A Study of Collision Characteristics in differential sedimentation according to variation of Ionic Strength, Zeta Potential and Particle Size (이온화세기, 제타전위, 입자크기에 따른 속도차 침전에서의 입자간 충돌특성에 관한 연구)

  • Han, Moo Young;Dock Ko, Seok;Park, Chung Hyun
    • Journal of Korean Society of Water and Wastewater
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    • v.12 no.1
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    • pp.81-87
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    • 1998
  • The possibility of collision of two particles slowly settling one after another in water can be described using the collision efficiency factor in differential sedimentation (${\alpha}_{DS}$). ${\alpha}_{DS}$ was found to be a function of several parameters particle size, particle size ratio, Hamaker constant, density of liquid and particle, gravity acceleration. Previous researches were limited to the case when there is no electric repulsion assuming that the suspension is destabilized. In this paper, ${\alpha}_{DS}$ is calculated for the stabilized condition. The relative trajectory of two particles are calculated including hydrodynamics, attraction and repulsion forces. Ionic strength and surface potential significantly affect the collision possibility of two settling particles. Depending on the surface potential and ionic strength, ${\alpha}_{DS}$ value is divided into three regions; stable, unstable and transition zone. ${\alpha}_{DS}$ increases as the ionic strength increases, and as the surface charge decreases. This result can be used to model both destabilized and stabilized suspension incorporating the collision efficiency factors of the other coagulant mechanisms such as fluid shear and Browian motion.

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Electrochemical Properties of Sub-micron Size Si Anode Materials Distributed by Wet Sedimentation Method (습식 분급으로 입도 조절된 서브 마이크론 크기의 Si 음극활물질의 전기화학적 특성 분석)

  • Jin-Seong Seo;Hyun-Su Kim;Byung-Ki Na
    • Korean Chemical Engineering Research
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    • v.61 no.1
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    • pp.39-44
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    • 2023
  • In this study, the particle size of Si polycrystals was controlled through wet-sedimentation method, and changes in the capacity and cyclic characteristics of the Si anode material according to the particle size were observed. After wet-sedimentation of Si particles pulverized by a vibration mill, the non-uniform particle distribution of Si was uniformly controlled. The d50 of a sample in which Si was sedimented for 24 hours decreased to 0.50 ㎛. As a result of the electrochemical characteristic analysis, the Rct value representing the resistance in the electrode was significantly reduced due to the decrease in particle size. The unclassified Si sample exhibited a discharge capacity of 2,869 mAh/g in the first cycle, and decreased to 85.7 mAh/g after 100 cycles. The sample in which Si was classified for 24 hours showed a capacity of 3,394 mAh/g initially, and maintained a capacity of 1,726 mAh/g after 100 cycles. As the size of the Si particles decreased, the discharge capacity increased and the cycle life was also increased.

Characterization of Fly Ash by Field-Flow Fractionation Combined with SPLITT Fractionation and Compositional Analysis by ICP-OES

  • Kang, Dong Young;Eum, Chul Hun;Lee, Seungho
    • Bulletin of the Korean Chemical Society
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    • v.35 no.1
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    • pp.69-75
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    • 2014
  • Accurate analysis of fly ash particles is not trivial because of complex nature in physical and chemical properties. SPLITT fractionation (SF) was employed to fractionate the fly ash particles into subpopulations in large quantities. Then the SF-fractions were analyzed by the steric mode of sedimentation field-flow fractionation (Sd/StFFF) for size analysis. The SF-fractions were also analyzed by ICP-OES. The results showed that the fly ash is mainly composed of Fe, Ca, Mg and Mn. No particular trends were observed between the particle size and the concentrations of Fe, Ca, Mg, while Mn, Cu and Zn were in higher concentrations in smaller particles. Sample preparation procedures were established, where the fly ash particles were sieved to remove large contaminants, and then washed with acetone to remove organics on the surface of particles. The sample preparation and analysis methods developed in this study could be applied to other environmental particles.