• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.11a
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• pp.181-181
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• 2009

전자부품용 Pb-free sealing frit의 열팽창계수를 기판에 matching 시키기 위하여 음의 열팽창계수를 가지고 있는 $\beta$-Eucryptite, $\beta$-Spodumene를 합성하여 filler로 첨가하였다. 합성된 filler는 저온소성용 유리프리트의 높은 열팽창계수를 조절하기 용이하고, 유리프리트와 복합화 하여 소성하면 낮은 열팽창계수로 인한 우수한 열충격 저항성을 갖는다. Filler로써 $\beta$-Eucryptite, $\beta$-Spodumene의 결정성을 향상시키기 위해 $1250^{\circ}C$에서 5 시간 동안 유지하는 합성공정을 3회 반복 진행한 후 XRD를 사용하여 결정성을 분석하였고, TMA를 이용하여 filler 첨가량에 따른 유리프리트의 열팽장계수의 변화를 측정하였다. 또한, filler 입도와 함량에 따른 melting 특성을 분석하기 위해 Pill test를 진행하였으며, soda-lime glass 기판과의 접합면을 SEM을 사용하여 관찰하였다.

• 한국정보디스플레이학회:학술대회논문집
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• 2005.07b
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• pp.1245-1247
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• 2005

Glass frit was selected to be a $Bi_2O_3-RO-R_2O_3$ system as a sealing material to replace the current PbO system in PDP. Fillers such as a zircon, cordierite and ${\beta}-eucryptite$ were added for the control of thermal expansion coefficient (CTE), flowability and strength for sealing. At $450-500^{\circ}C$, reaction of frit and filler and interface were evaluated by a flow button test and SEM observation. The composite (frit and filler) showed CTE in the range of 70-83 x $10^{-7}/K$ and flowability of 14-20mm. It can be a candidate for the replacement of PbO system.

• Journal of Power System Engineering
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• v.14 no.4
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• pp.37-42
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• 2010

This paper deals with the sealing mechanism of the gasket component and the effects of design parameters for the exhaust manifold. The finite element model includes hot-end exhaust system and a simplified gasket model supplied by ABAQUS software. The mechanical behaviors of bead and body of a gasket are measured after several times of cyclic loads by gasket supplier. From the finite element analysis due to the cyclic thermal loads, the flange of exhaust manifold shows thermal expansion and contraction in longitudinal direction as well as convex and concave deformations with respect to the engine cylinder head. And, the contact pressures of the gasket beads suddenly changes by normal deformation of inlet flanges. Therefore, the magnitudes of contact pressures could be used to determine the sealing characteristics of the exhaust gas in the exhaust system. The distributions of contact pressures in gasket bead lines shows a good agreement with the engine test results.

• The Journal of the Korean dental association
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• v.23 no.12 s.199
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• pp.1031-1037
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• 1985

The purpose of this study was to evaluate the marginal sealing ability of 'vivadent.' Using freshly extracted human teeth and 2% aqueous methylene blue, the marginal leakage of dye in restorative materials such as vivadent with acid etching technique, Durafill with acid etching technique, silar with acid etching technique, Adaptic, and Amalgam were investigated at 37℃ and under temperature cycling in range of 4℃-60℃. The results were as follows; 1. All filling materials showed some degree of marginal penetration by 2% methylene blue dye. 2. Vivadent with acid etching technique revealed effective marginal sealing ability, but under temperature cycling it showed increased marginal leakage. 3. All resins showed greater marginal leakage than amalgam restoration. 4. Vivadent had the most effective marginal sealing ability in experimented resins.

• Restorative Dentistry and Endodontics
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• v.8 no.1
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• pp.167-172
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• 1982

The purpose of this study was to evaluate the marginal sealing ability of "Silar". Using freshly extracted human teeth and 2% acquous methylene blue, the marginal leakage of dye in restorative materials such as Silar, Silar with acid etching technique, Hi-Pol, Hi-Pol Enamel Bond system, Adaptic and Amalgam were investigated at $37^{\circ}C$ and under temperature cycling in range of $4^{\circ}C-60^{\circ}C$. The results as follows; 1. All filling materials showed some degree of marginal penetration by 2% methylene blue dye. 2. Silar with acid etching technique revealed effective marginal sealing ability, but under temperature cycling it showed increased marginal leakage. 3. All composite resins showed greater marginal leakage than amalgam restoration. 4. Silar had the most effective marginal sealing ability in experimented composite resins.

• Journal of the Korean Ceramic Society
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• v.54 no.5
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• pp.400-405
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• 2017

$P_2O_5-ZnO-SiO_2-R_2O$ glasses were synthesized as a sealing material for large scale dye-sensitized solar cells (DSSC). Compositional effects of $P_2O_5$ and ZnO were examined by varying their contents. Their viscosity and glass stability at sintering temperatures of less than $550^{\circ}C$ were examined by flow button test. Glass transition temperature and structural change upon compositional change were investigated. Chemical stability against electrolyte was also examined by immersing the glasses in the electrolyte for 72 h at $85^{\circ}C$.

• Journal of the Korean Society for Precision Engineering
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• v.23 no.1 s.178
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• pp.145-151
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• 2006

Wheel bearing unit has been exclusively applied to car wheel supporting device. The seal for wheel bearing is required to have both high sealing effects and low reaction forces because wheel bearing are operated on adverse environmental conditions such as mud and splash water. High sealing effects are for the protection of bearing ball wear from dust influx. In order to ensure high sealing effects, it is a easiest way to increase contact force which are affected by geometric characteristics, material properties and interferences between seal and inner bearing but induces higher wear phenomena. Interferences in all variables are most important factor to determine the performance of wheel bearing. In this study, optimization of interference amount was performed with finite element analysis with commercial code ABAQUS. For the sake of finite element analysis, tensile tests of rubber material were conducted and governing equation of nonlinear behavior was achieved. Hock-up bearing was manufactured with optimized interference amount. Results of torque and mud spray tests using this bearing unit are performed. Less torque and moisture influx of bearing with optimized interference amount is evidence to validity of this study.

• 한국정보디스플레이학회:학술대회논문집
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• 2003.07a
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• pp.870-873
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• 2003

We have fabricated a carbon nanotube field emission display(CNT FED) panel with a 2 inch diagonal size by using screen printing method and vacuum in-line sealing technology. The sealing temperature of the panel was around 390 $^{\circ}C$ and the leak test was carried out for 72 hrs after sealing process. When field emission properties of fabricated and sealed CNT FED panel were characterized and compared with those of unsealed panel which was located in vacuum chamber of vacuum level similar with the sealed panel, the sealed panel showed more improved field emission properties.

• Corrosion Science and Technology
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• v.20 no.2
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• pp.45-51
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• 2021

In this work, we describe the effect of pulse anodizing duty ratio on the corrosion resistance of anodic films in magnesium AZ31B. The process involves the application of square pulse potential for a constant period with a duty ratio varying from 40, 60 and 80%. In several samples, a sealing treatment for 30 minutes was conducted after anodization in order to seal the pores available in the anodic layer. After anodizing, the surface morphology of the anodic layer was examined using a scanning electron microscope (SEM Hitachi SU3500). The corrosion characteristics of the sample were evaluated through an open circuit potential (OCP) and potentiodynamic polarization test using potentiogalvanostat. SEM observation shows that the increase of anodization duty ratio (α) results in a more uniform anodic layer, with fewer pores and cracks. The increase of duty ratio (α) decreases the OCP value from approximately -1.475 to about -1.6 Volt, and significantly improves the corrosion resistance of the anodic coating by 68%. The combination of anodization and sealing treatment produces an anodic coating with a very low corrosion rate of 4.4 mpy.

• Restorative Dentistry and Endodontics
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• v.26 no.5
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• pp.379-386
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• 2001

This study was performed to evaluate the sealing ability of various retrograde filling materials by using bacterial penetration and dye penetration test. One hundred and forty extracted human teeth with single, straight canals and mature apiece were collected and used for this study. All canals were instrumented using an engine driven Ni-Ti file (ProFile). After removing 3mm from the apex of tooth, a standardized 3mm root end cavity was prepared using an ultrasonic instrument. The 70 teeth were randomly divided into 7 groups : 6 groups for retrograde filling using Super-EBA, ZOE, Chelon-Silver, IRM, ZPC and amalgam. The 7th group was used as a negative control. Nail varnish was applied to all external root surfaces to the level of the reseated root ends to prevent lateral microleakages. The specimens were then sterilized in an ethylene oxide sterilizer for 24 hours. 2 mm of the reseated root was immersed in a culture chamber containing a Tripticase Soy Broth with a phenol red indicator. The coronal access of each specimen was inoculated every 72 hours with suspension of Proteus vulgaris. The culture media were observed every 24hours for color change indicating bacterial contamination. The specimens were observed for 4weeks. The remaining 70 teeth were submitted to a dye penetration test. The canals of all teeth were first sealed with AH26 and obturated using an Obtura II system. Root resection, root end preparation and retrograde filling was performed as above. All specimens were suspended in 2% methylene blue dye for 72 hours before being ion gitudinally split. The degree of dye penetration was then measured using a stereomicroscope at 10 magnification and evaluated. The results were as floows : 1. In the bacterial penetration, the degree of leakage was the lowest in the Super-EBA, followed by, in ascending order, ZOE, Chelon-Silver IRM and ZPC. The amalgam showed highest bacterial leakage of all(p<0.01). 2. In the dye penetration, the degree of microleakage was the lowest in the Chelon-Silver and Super-EBA, followed by, in ascending order, IRM, ZPC. The ZOE and amalgam showed the highest microleakage of all (p<0.05). These results suggested that the eugenol based cement, Super-EBA, have excellent sealing ability as a retrograde filling material.