• 한국재료학회지
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• 제26권10호
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• pp.549-555
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• 2016

We have investigated a glass-forming region of $V_2O_5-P_2O_5-ZnO$ glass and the effects of the addition of modifier oxides ($B_2O_3$) to the glass systems as a sealing material to improve the adhesion between the glass frits and a soda lime substrate. Thermal properties and coefficient of thermal expansion were measured using a differential scanning calorimetry, a dilatometer and a hot stage microscopy. Structural changes and interfacial reactions between the glass substrate and the glass frit after sintering (at $400^{\circ}C$ for 1 h) were measured by Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy and scanning electron microscope. The results showed that the adhesion strength increases as the content of $B_2O_3$ at 5 mol% increases because of changes in the structural properties. It seems that the glass structures change with $B_2O_3$, and the $Si^{4+}$ ions from the substrate are diffused to the sealing glass. From these results, we could understand the mechanism of strengthening of the adhesion of soda lime silica substrate by ion-diffusion from the substrate to the glass.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2005년도 International Meeting on Information Displayvol.II
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• pp.1245-1247
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• 2005

Glass frit was selected to be a $Bi_2O_3-RO-R_2O_3$ system as a sealing material to replace the current PbO system in PDP. Fillers such as a zircon, cordierite and ${\beta}-eucryptite$ were added for the control of thermal expansion coefficient (CTE), flowability and strength for sealing. At $450-500^{\circ}C$, reaction of frit and filler and interface were evaluated by a flow button test and SEM observation. The composite (frit and filler) showed CTE in the range of 70-83 x $10^{-7}/K$ and flowability of 14-20mm. It can be a candidate for the replacement of PbO system.

• 대한치과의사협회지
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• 제23권12호통권199호
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• pp.1031-1037
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• 1985

The purpose of this study was to evaluate the marginal sealing ability of 'vivadent.' Using freshly extracted human teeth and 2% aqueous methylene blue, the marginal leakage of dye in restorative materials such as vivadent with acid etching technique, Durafill with acid etching technique, silar with acid etching technique, Adaptic, and Amalgam were investigated at 37℃ and under temperature cycling in range of 4℃-60℃. The results were as follows; 1. All filling materials showed some degree of marginal penetration by 2% methylene blue dye. 2. Vivadent with acid etching technique revealed effective marginal sealing ability, but under temperature cycling it showed increased marginal leakage. 3. All resins showed greater marginal leakage than amalgam restoration. 4. Vivadent had the most effective marginal sealing ability in experimented resins.

• Restorative Dentistry and Endodontics
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• 제8권1호
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• pp.167-172
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• 1982

The purpose of this study was to evaluate the marginal sealing ability of "Silar". Using freshly extracted human teeth and 2% acquous methylene blue, the marginal leakage of dye in restorative materials such as Silar, Silar with acid etching technique, Hi-Pol, Hi-Pol Enamel Bond system, Adaptic and Amalgam were investigated at $37^{\circ}C$ and under temperature cycling in range of $4^{\circ}C-60^{\circ}C$. The results as follows; 1. All filling materials showed some degree of marginal penetration by 2% methylene blue dye. 2. Silar with acid etching technique revealed effective marginal sealing ability, but under temperature cycling it showed increased marginal leakage. 3. All composite resins showed greater marginal leakage than amalgam restoration. 4. Silar had the most effective marginal sealing ability in experimented composite resins.

• 한국전기전자재료학회논문지
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• 제20권3호
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• pp.273-280
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• 2007

In this paper, the ZnO surge arrester performance of power distribution class has been studied under different manufacturing conditions such as housing materials(polymeric, porcelain), interface sealants and one-body molding type. In the recent years, the polymeric ZnO surge arresters have been developed and put into operations based on their excellent characteristics. For polymeric surge arresters, the inner gas volume is extremely small, especially in solid insulation polymeric arresters there are not any gas volume inside arresters in the structure due to polymeric materials are filled into the internal gas volume. The sealing integrity is related to safe operation of surge arrester, the prime failure reason of porcelain housed arresters is moisture ingress. In this paper, the sealing integrity of polymeric surge arresters is investigated with moisture multi-aging test and ingress test. The evaluation techniques are used to inspect the sealing integrity of polymeric arresters, including leakage current, surface temperature, reference voltage and dissipation factor.

• Corrosion Science and Technology
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• 제20권2호
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• pp.45-51
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• 2021

In this work, we describe the effect of pulse anodizing duty ratio on the corrosion resistance of anodic films in magnesium AZ31B. The process involves the application of square pulse potential for a constant period with a duty ratio varying from 40, 60 and 80%. In several samples, a sealing treatment for 30 minutes was conducted after anodization in order to seal the pores available in the anodic layer. After anodizing, the surface morphology of the anodic layer was examined using a scanning electron microscope (SEM Hitachi SU3500). The corrosion characteristics of the sample were evaluated through an open circuit potential (OCP) and potentiodynamic polarization test using potentiogalvanostat. SEM observation shows that the increase of anodization duty ratio (α) results in a more uniform anodic layer, with fewer pores and cracks. The increase of duty ratio (α) decreases the OCP value from approximately -1.475 to about -1.6 Volt, and significantly improves the corrosion resistance of the anodic coating by 68%. The combination of anodization and sealing treatment produces an anodic coating with a very low corrosion rate of 4.4 mpy.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2007년도 춘계학술발표대회 및 제12회 신소재 심포지엄
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• pp.14.2-14.2
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• 2007

• 대한기계학회논문집A
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• 제35권10호
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• pp.1193-1198
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• 2011

연료전지 내의 작동유체는 폭발성을 가지고 있기 때문에 솔레노이드 밸브의 실링특성은 일반적인 시스템에 비해 매우 중요하다 할 수 있다. 하지만, 이 시스템의 경우 작동 온도가 일반적인 경우에 비해 비교적 높으며, 작동 유체의 화학적 특성 때문에 실링에 사용되는 재질은 내화학성이 뛰어나면서도 연료전지 시스템에서 요구하는 수명을 보장해야 하는 어려움이 있다. 본 연구에서는 연료전지 내에서 사용가능한 솔레노이드 밸브의 실링 특성을 확인하기 위하여, 내화학성이 뛰어난 실링용 링의 재질인 불소고무에 대한 수명을 아레니우스(Arrhenius) 관계식을 이용하여 예측하였다. 또한, 수상치환법을 이용하여 실제 제작된 연료전지용 솔레노이드 밸브가 제품으로써 충분히 사용가능함을 확인하였다.

• Tribology and Lubricants
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• 제20권5호
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• pp.231-236
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• 2004

Sulfur Hexafluoride, S $F_{6}$ is widely used for leak detection and as a gaseous dielectric in transformers, condensers and circuit breakers. S $F_{6}$ gas is also effective as a cleanser in the semiconductor industry. This paper presents a numerical study of the sealing force of disk type seal in S $F_{6}$ gas safety valve. The sealing force on the disk seal is analyzed by the FEM method based on the Taguch's experimental design technique. Disk seals in S $F_{6}$ gas safety valve are designed with 9 design models based on 3 different contact length, compressive ratio and gas pressure. The calculated results of Cauchy stress and strain showed that the sealing characteristics of Teflon $^{ }$PTFE is more effective compared to that of FKM(Viton), which is related to the stiffness of the materials. And also, the contact length of the disk seal is important design parameter for sealing the S $F_{6}$ gas leakage in the safety valve.afety valve.

• 한국분말재료학회지
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• 제21권4호
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• pp.260-265
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• 2014

In this study, in order to increase surface ability of hardness and corrosion of magnesium alloy, anodizing and sealing with nano-diamond powder was conducted. A porous oxide layer on the magnesium alloy was successfully made at $85^{\circ}C$ through anodizing. It was found to be significantly more difficult to make a porous oxide layer in the magnesium alloy compared to an aluminum alloy. The oxide layer made below $73^{\circ}C$ by anodizing had no porous layer. The electrolyte used in this study is DOW 17 solution. The surface morphology of the magnesium oxide layer was investigated by a scanning electron microscope. The pores made by anodizing were sealed by water and aqueous nano-diamond powder respectively. The hardness and corrosion resistance of the magnesium alloy was increased by the anodizing and sealing treatment with nano-diamond powder.