• Title/Summary/Keyword: Sampling and analytical method

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The Trends in Research on the Health of North Korean Refugees (북한이탈주민의 건강 관련 연구 동향)

  • Lim, Hyun-Ju;Lee, Guna;Yang, Sook-Ja
    • Research in Community and Public Health Nursing
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    • v.28 no.2
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    • pp.144-155
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    • 2017
  • Purpose: This study aims to identify the general characteristics, subjects, and methods of research on the health of North Korean refugees through a systematic literature review. Methods: A total of 140 studies on health were reviewed using the analytical framework developed by the researchers. Results: The quantitative research comprised 90.7% of the studies, whereas the qualitative research were 7.9% of them. Approximately 81.4% of those reviewed have publication dates spanning 2006 to 2015. Only 13.6% of the studies were conducted with the approval of an institutional review board. The subjects of studies were psycho-social health (151.8%), behavioral health (28.5%), cognitive health (15.0%), physical health (12.2%), integrated health (7.8%), and spiritual health (2.8%). Within the quantitative studies reviewed, the most commonly used study design was survey research (86.0%). The two sampling methods used most often were convenience sampling (53.5%) and snowball sampling (19.4%), and the most commonly used data-collection method were questionnaires (94.6%). As for the qualitative studies, the most commonly used study design was phenomenology. Conclusion: The results suggested that the reviewed studies focused on physical health more than psycho-social health, and physiological measurement more than questionnaires. Ethical considerations need to be expanded.

Development of Continuous Monitoring System of Acidic Pollutants for The Studies of Their Diffusion in The Atmosphere (대기오염의 확산 연구를 위한 산성 오염물질의 연속 측정법의 개발)

  • Chung, Hyung-Keun;Dasgupta, Purnendu K.;Lee, Dai Woon
    • Analytical Science and Technology
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    • v.5 no.3
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    • pp.269-276
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    • 1992
  • An ion-exchange/conductometric method is applied for the determination of total acidity in simulated atmospheric samples. Non-$H^+$ cations and strong acid anions are enriched by the preconcentrator columns in series and eluted through the corresponding parallel suppressor units. The conductivities from each channel correspond to the concentrations of the resulting ionized species in equivalents per unit volume. The difference is the measure of acidity due to strong acids. With 5-min sampling at a flow rate of 0.3 mL/min, the detection limits for ${NH_4}^+$ and ${SO_4}^{2-}$ are 0.3 and $0.1{\mu}equiv/L$, respectively. The acidity for samples composed of various ions can be determined without significant error, usually less than 5%. The proposed method discriminates against the artifact from the $CO_2$ dissolution. Principles of acidity measurements are also presented.

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Study on Development of Analytical Method for Polar Solvents by GC (GC를 이용한 극성용매의 분석방법 개발 연구)

  • Oh, Doe Seok;Kim, Sung Hwa;Lee, Seul;Hwang, Kyung Chul
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.26 no.1
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    • pp.20-29
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    • 2016
  • Objectives: The purpose of this study is to simplify and standardize analytical method of polar solvents(methanol, isopropanol, n-butanol, acetone, methylene chloride and MIBK) in the working environmental by GC. Because NIOSH methods are various and complicated. Methods: The method is using the same stationary phase(5% phenyl 95% dimethylpolysiloxane), absorbent(silica gel) and desorption solvent(DMSO) for above 6 solvents. For the 6 solvents desorption efficiency, calibration curve, and limit of detection were studied Results: As the results, 6 solvents{2 groups ; first group(methanol/isopropanol/butanol) and second group(acetone/methylene chloride/MIBK)} could be separated and quantified within 10 minutes. Desorption efficiency from silica gell of 6 solvents using dimethylsulfoxide(DMSO) was methanol 86.2%, isopropanol 103.2%, n-butanol 101.8%, acetone 98.2%, methylene chloride 103.9% and MIBK 106.2% in the range of 0.2, 0.5, 2.0 times of TWA, consequently, satisfied NIOSH estimation level(beyond 75%). Correlation coefficient(r)in the range of 0.2~2.0 times of TWA, was above 0.999 for 6 solvent. LOD(mg/DMSO ml) using calibration curve in the range of 0.2~2 times of TWA was methanol 0.11, isopropyl alcohol 0.20, n-butanol 0.03, acetone 0.50, methylene chloride 0.05, MIBK 0.04 respectably. Conclusions: This method can be used at the sampling and analytical method for polar solvents by GC. Also, will be able to be applied with NIOSH methods.

Determination of Phthalates Compounds in the Ambient Atmosphere (II) - Evaluation of Experimental Artifacts and Sample Clean-up Procedures - (환경대기 중 프탈레이트 화합물의 농도 측정 (II) - 실험재료 전처리 및 시료정제과정 평가 -)

  • Park, Young-Hwa;Hwang, Yoon-Jung;Seo, Young-Kyo;Baek, Sung-Ok
    • Journal of Korean Society of Environmental Engineers
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    • v.32 no.5
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    • pp.455-460
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    • 2010
  • This study was carried out to find out any inherent problems occurring in the sampling and analytical procedures, and to suggest the relevant solutions to the problems. In addition, an optimal condition of clean-up process was developed, which was based on a method using silica glass column. As a result of experiments to test any artificial contamination of blank samples such as glassware and collection media, artifacts of DBP and DEHP appeared to be detected in various kinds of laboratory tools and apparatuses used in the sampling and analytical works. Therefore, it is necessary to investigate a degree of contamination before laboratory works by conducting a prior check any possible contaminations in all experimental tools and apparatus. It is also necessary to devise a method to avoid a tool, if possible, or to use a substitute of phthalate free. If the use of any plastic tool to cause contamination is inevitable, it should be properly corrected with a blank level, as is equally treated as the sample. The clean-up process demonstrated in this study can give us a significant benefit in terms of the quantity and quality of a target compound by GC/MS analysis.

Study on Distribution of Elemental Concentration with a Different Depth of River Sediment using Neutron Activation Analysis (중성자 방사화 분석을 이용한 하천 침전물의 깊이에 따른 원소의 함량분포 연구)

  • Kim, Hyeon-Soo;Im, Hye-Ran;Kim, Yong-Uhn;Moon, Jong-Hwa
    • Analytical Science and Technology
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    • v.16 no.3
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    • pp.232-239
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    • 2003
  • The river sediments were collected from 4 points of Seoknam river, one point of Miho river and one point of the joining area of two rivers. For preparation of sample, three sediment samples were collected for the surface, middle and lower part of the sediment at each sampling point. The elemental concentrations were analyzed by neutron activation analysis using HANARO research reactor at Korea Atomic Energy Research Institute, and the concentrations of 30 elements were determined by the relative method using standard reference material of NIST. As a result of analysis, it was found that when the examination and prediction of contamination distribution about the site where the contamination site of river is connected to the lower river is done, the specific gravity of elements which is contained in the sediment and the speed of a current of river should be considered and also found that when the samples for concentration analysis in the river sediments are collected, for the establishment of regional representatives in samples, the range of sampling depth should be determined considering the specific gravity of elements and the speed of a current.

Moderating of Religiosity on Reward and Engagement: Empirical Study in Indonesia Public Service

  • SALEH, Choirul;HAYAT, Hayat;SUMARTONO, Sumartono;PRATIWI, Ratih Nur
    • The Journal of Asian Finance, Economics and Business
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    • v.7 no.6
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    • pp.287-296
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    • 2020
  • The study investigates the relationship and influence between religiosity, reward, and engagement in the public administration sector, both directly and causally via moderation. This study involved one hundred and twenty-three respondents in three local government organizations in Malang City, East Java Province, Indonesia, namely, the Malang City General Hospital, the Population and Civil Registry Office, and the Investment Office. The sampling method uses stratified random sampling from the total population of civil servants in Malang in the three institutions. The data analysis model of this study uses a quantitative approach with a unit of data analysis using the path analysis method. The analytical tools used are smart-PLS and SPSS. The results reveal that the direct combined effect of reward and religiosity has a positive and significant influence on the engagement. However, moderation between reward and commitment, which is bridged by religiosity, does not show positive and significant results. The non-positive relationship shown by testing moderation concludes that there is a separation of purpose between the portion of religiosity in the world of work, where religiosity in this study is only described as part of the concept of worship, and the relationship between the person and his God.

Wound-State Monitoring for Burn Patients Using E-Nose/SPME System

  • Byun, Hyung-Gi;Persaud, Krishna C.;Pisanelli, Anna Maria
    • ETRI Journal
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    • v.32 no.3
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    • pp.440-446
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    • 2010
  • Array-based gas sensors now offer the potential of a robust analytical approach to odor measurement for medical use. We are developing a fast reliable method for detection of microbial infection by monitoring the headspace from the infected wound. In this paper, we present initial results obtained from wound-state monitoring for burn patients using an electronic nose incorporating an automated solid-phase microextraction (SPME) desorption system to enable the system to be used for clinical validation. SPME preconcentration is used for sampling of the headspace air and the response of the sensor module to variable concentrations of volatiles emitted from SPME fiber is evaluated. Gas chromatography-mass spectrometry studies prove that living bacteria, the typical infectious agents in clinical practice, can be distinguished from each other by means of a limited set of key volatile products. Principal component analysis results give the first indication that infected patients may be distinguished from uninfected patients. Microbial laboratory analysis using clinical samples verifies the performance of the system.

Estimation of Interaction Effects among Nucleotide Sequence Variants in Animal Genomes

  • Lee, Chaeyoung;Kim, Younyoung
    • Asian-Australasian Journal of Animal Sciences
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    • v.22 no.1
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    • pp.124-130
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    • 2009
  • Estimating genetic interaction effects in animal genomics would be one of the most challenging studies because the phenotypic variation for economically important traits might be largely explained by interaction effects among multiple nucleotide sequence variants under various environmental exposures. Genetic improvement of economic animals would be expected by understanding multi-locus genetic interaction effects associated with economic traits. Most analyses in animal breeding and genetics, however, have excluded the possibility of genetic interaction effects in their analytical models. This review discusses a historical estimation of the genetic interaction and difficulties in analyzing the interaction effects. Furthermore, two recently developed methods for assessing genetic interactions are introduced to animal genomics. One is the restricted partition method, as a nonparametric grouping-based approach, that iteratively utilizes grouping of genotypes with the smallest difference into a new group, and the other is the Bayesian method that draws inferences about the genetic interaction effects based on their marginal posterior distributions and attains the marginalization of the joint posterior distribution through Gibbs sampling as a Markov chain Monte Carlo. Further developing appropriate and efficient methods for assessing genetic interactions would be urgent to achieve accurate understanding of genetic architecture for complex traits of economic animals.

Simple Analytical Method for Acrylamide in the Workplace Air Adsorbed by Charcoal Tube (활성탄관을 사용하여 포집한 작업환경 공기중 아크릴아마이드의 분석법)

  • Yang, J.S.;Lee, M.Y.;Park, I.J.;Kang, S.K.
    • Analytical Science and Technology
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    • v.11 no.2
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    • pp.139-144
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    • 1998
  • For the ambient monitoring of acrylamide, the adequate condition of sampling and analysis was checked. The adequate adsorbents and desorption solvents were tested. The combination of charcoal tube as a adsorbent and acetone as a desorption solvent showed 87% desorption efficiency. Flame ionization detector was used to detect acrylamide. The detection limit was 0.814 mg acrylamide in 1 L acetone. It is the equivalent concentration of 0.0203 mg acrylamide in $1m^3$ air if the volume of air collected was 40L. The permissible exposure level (PEL) of acrylamide in the workplace air recommended by Occupational Safety and Health Administration (OSHA, USA) is 0.3 mg acrylamide in $1m^3$ air. So, it is very simple and economic analytical method for acrylamide to be set in the industrial hygiene laboratories.

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Development of Analytical Method and Monitoring of Organophosphorus Pesticides in the Raw Water and Clean Water by Liquid Chromatography-Tandem Mass Spectrometry (LC/MS/MS를 이용한 유기인계 농약류의 최적 분석법 정립과 원·정수에서의 모니터링)

  • Kim, Gyung-A;Song, Mi-Jeong;Yeom, Hoon-Sik;Son, Hee-Jong;Lee, Sang-Won;Choi, Jin-Tack
    • Journal of Environmental Science International
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    • v.24 no.12
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    • pp.1569-1582
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    • 2015
  • The analytical method for 16 organophosphorus pesticides was developed in this study. The 16 organophosphorus pesticides were analyzed by liquid chromatography-tandem mass spectrometry (LC/MS/MS) using on-line solid phase extraction (on-line SPE) with PLRP- S cartridge. Analysis of all analytes in the MS/MS was processed in the electrospray ioni-zation (ESI) positive mode. They are Azinphos ethyl, Chlorfenvinphos, Ethion, Famphur, Phosmet, Phosphamidon, Terbufos, Aspon, Chlorpyrifos-methyl, Crotoxyphos, Dichlofenthi-on, Dicrotophos, Fonofos, Thionazin, Dimethoate and Iprobenfos. Limits of detection (LODs) and Limits of quantification(LOQs) were obtained as 0.8~2.0 ng/L and 2.6~6.4 ng/L, respectively. All compounds were not detected at the 8 sampling points of the raw water and clean water.