• 제목/요약/키워드: Sample recovery

검색결과 708건 처리시간 0.028초

윈도우 기반 심벌 타이밍 복원 (Window based Symbol Timing Recovery)

  • 이철수;장승현;정의석;김병휘
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2005년도 학술대회 논문집 정보 및 제어부문
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    • pp.487-489
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    • 2005
  • This paper proposes a symbol timing recovery method that is simple in structure and can provide high speed symbol synchronization. Transmitter and receiver are not synchronized in communication systems using digital modulation. Receiver should search the timing variation of transmitter continuously. The proposed timing recovery method searches sample position by comparing previous sample value with next sample value. This method can be applied to digital and optical transceivers with high data rate.

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고성능 커버링기 및 복합연사기를 이용한 연사직물의 물성분석 연구 (Studies on the Physical Properties of Twisted Yam Woven Fabrics by High Functional Covering Machine and Compound Twister)

  • 전병익;송민규;최재우
    • 한국의류산업학회지
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    • 제2권3호
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    • pp.227-233
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    • 2000
  • The purpose of this study was to develop the High Functional Covering machine and the Compound Twister to produce the high value added textile goods and to meet the consumer's needs. For the study, 8 yarns and 12 fabrics were made with two developed machines and the tensile characteristics of the samples were tested and analysed. The result indicated that the sample fabrics kept their elongation regardless of buffering process. Elongation of the sample yarns was higher than those of yarns made with a traditional covering method. Elastic recovery of the sample fabrics was more effected by the recovery rate than by the number of extension and the characteristics of the sample yarns and fabrics were comparable to the yarns and fabrics made with a traditional covering method in terms of the position of Spandex yarns in their yarn structure and buffering effect.

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Polyester사를 이용한 충전용 솜사의 물성 (The Physical Properties of Filling Batt Using Polyester Yarn)

  • 박명수
    • 한국의류산업학회지
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    • 제9권3호
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    • pp.347-350
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    • 2007
  • To analyse basic properties for making packing batt according to doubling condition, packing batt yarn, of $300^D$, $900^D$, $3600^D$ made from DTY yarn $150^D$/48 were produced from KTDI. The results are as follows: The birefringence of the sample yarn increased with increasing the annealing temperature and denier. The initial modulus of the sample yarn decreased with increasing the annealing temperature and denier. The higher than annealing temperature of $160^{\circ}C$, initial modulus of the sample are equilibrated. The strain recovery ratio of samples decreased with increasing the annealing temperature and denier. The lower than annealing temperature of $140^{\circ}C$, strain recovery ratio of the sample are decreased Where the $900^D$, $3600^D$ yarns are at $100^{\circ}C$ the specific bending rigidity value obtained is 0.65kgf/d but the twisted yarn (3,600) obtained 0.006 ($gfcm^2/tex^2$). However, where the heat temperature is $160^{\circ}C$, specific bending rigidity value obtained 0.003($gfcm^2/tex^2$).

FTIR과 XRD를 이용한 α-Quartz 분석법 비교 (Comparison of Analytical Methods for α-Quartz by FTIR and XRD)

  • 김부욱;이종성;최병순
    • 한국환경보건학회지
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    • 제35권2호
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    • pp.130-142
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    • 2009
  • This study compared FTIR with XRD method for the analysis of quartz by % recovery, coefficient of variation (CV) and influence of the interference. the results were as the following. 1. In FTIR method, the coefficient of determination ($r^2$) was 0.9998 in a calibration curve of $695\;cm^{-1}$, and the limit of detection was $4.9{\mu}g/sample$. 2. The highest recovery was $799\;cm^{-1}$ (98.2%). 3. The CVpooled of the FTIR method was approximately 10% in three wave numbers. 4. The analysis of qualitative and quantitative for quartz is difficult with mixed cristobalite and iron oxide. 5. In XRD method with rotating sample holder and LynxEye detector, the coefficient of determination was 0.9996 in a calibration curve, and the limit of detection was $5.9{\mu}g/sample$. 6. The recovery and CV pooled were 104.3%, and 11 %, respectively. 7. In muffle furnace ashing, the quartz weight decreased to 34% when the maximum weight of the iron oxide was more than eight times. In conclusion, the accuracy (% recovery) and precision (CV) of FTIR and XRD method for analyzing $\alpha$-quartz were similar. FTIR method was a disadvantage for sample matrix because it indicates possibility of interference. However, XRD method distinguished specific crystalline forms of silica, and the majority of silicate minerals. In addition, XRD method recommend filter dissolution to pretreatment method.

임상화학검사실에서 회수율 실험의 실증적 연구 (An Empirical Study of the Recovery Experiment in Clinical Chemistry)

  • 장상우;이상곤;송은영;박용원;박병옥
    • 대한임상검사과학회지
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    • 제38권3호
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    • pp.184-188
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    • 2006
  • The purpose of the recovery experiment in clinical chemistry is performed to estimate proportional systematic error. We must know all measurements have some error margin in measuring analytical performance. Proportional systematic error is the type of error whose magnitude increases as the concentration of analyte increases. This error is often caused by a substance in the sample matrix that reacts with the sought for analyte and therefore competes with the analytical reagent. Recovery experiments, therefore, are used rather selectively and do not have a high priority when another analytical method is available for comparison purposes. They may still be useful to help understand the nature of any bias revealed in the comparison of kit experiments. Recovery should be expressed as a percentage because the experimental objective is to estimate proportional systematic error, which is a percentage type of error. Good recovery is 100.0%. The difference between 100 and the observed recovery(in percent) is the proportional systematic error. We calculated the amount of analyte added by multiplying the concentration of the analyte added solution by the dilution factor(mL standard)/(mL standard + mL specimen) and took the difference between the sample with addition and the sample with dilution. When making judgments on method performance, the observed that the errors should be compared to the defined allowable error. The average recovery needs to be converted to proportional error(100%/Recovery) and then compared to an analytical quality requirement expressed in percent. The results of recovery experiments were total protein(101.4%), albumin(97.4%), total bilirubin(104%), alkaline phosphatase(89.1%), aspartate aminotransferase(102.8), alanine aminotransferase(103.2), gamma glutamyl transpeptidase(97.6%), creatine kinase(105.4%), lactate dehydrogenase(95.9%), creatinine(103.1%), blood urea nitrogen(102.9%), uric acid(106.4%), total cholesterol(108.5), triglycerides(89.6%), glucose(93%), amylase(109.8), calcium(102.8), inorganic phosphorus(106.3%). We then compared the observed error to the amount of error allowable for the test. There were no items beyond the CLIA criterion for acceptable performance.

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Optimization of Solid Phase Extraction Method for Quantitative Analysis of Perfluorooctanoic Acid in Serum using Liquid Chromatography-Tandem Mass Spectrometry

  • Lee, Hyun-Seok;Yim, Yong-Hyeon
    • Mass Spectrometry Letters
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    • 제5권1호
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    • pp.30-33
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    • 2014
  • A solid phase extraction (SPE) method was optimized for the quantitative analysis of perfluorooctanoic acid (PFOA) in serum using hydrophilic-lipophilic balance SPE and LC-MS/MS. Fetal bovine serums spiked with $^{13}C_8$-PFOA before or after SPE were used as test samples for evaluation of the SPE efficiency. Simultaneous evaluation of matrix effects and absolute SPE recovery for $^{13}C_8$-PFOA in serum using different sample pre-treatments and SPE conditions allowed optimization of SPE process efficiency with minimal matrix effect and decent SPE recovery. Introduction of protein precipitation as a sample pre-treatment procedure for serum samples before SPE generally decreased matrix effect in LC-MS/MS analysis and provided more stable recovery of PFOA.

Stability characteristics of DyBCO coated conductor stabilized with stainless steel

  • Dixit, Manglesh;Kim, Tae-Hyung;Oh, Sang-Soo;Song, Kyu-Jeong;Kim, Ho-Min;Park, Kwon-Bae
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.288-289
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    • 2005
  • As high temperature superconductor applications became a reality due to increase in coated conductor performance, it is important to understand their stability behavior to design safe electrical power systems. We have experimentally studied the dependence of quench and recovery characteristics of coated conductors on the amplitude of current and duration time. The sample used in the present study is stabilized with stainless steel. Stability tests of 3 cm long sample were performed in a liquid nitrogen bath cooling condition by applying a short period over current pulses for 50 and 100 ms, with amplitude up to ~ 6 times of the critical current. The transport current that follows before and after the current pulse was fixed about ~85% the critical current. We analyzed the quench recovery using the current voltage characteristic.

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폐자동차(廢自動車) 라디에이터로부터 Nylon 회수(回收)를 위한 마찰하전정전선별(摩擦荷電靜電選別) 기술개발(技術開發) (Development of Triboelectrostatic Separation Technique for Recovery of Nylon from Radiator of End-of-Life Vehicle)

  • 백상호;전호석;김수강;이광훈
    • 자원리싸이클링
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    • 제22권1호
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    • pp.29-35
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    • 2013
  • 본 연구에서는 마찰하전정전선별을 적용하여 폐자동차 라디에이터의 Nylon을 회수하기 위한 재질분리 연구를 수행하였다. 시료(Nylon, PP glass)의 효율적인 재질분리를 위하여, 각각의 시료를 대상으로 다양한 하전재질에 따른 하전극성과 하전량을 faraday cage로 조사하였다. 그리고 시료를 분극할 수 있는 재질을 대상으로 기초 분리실험을 수행하여 하전재질을 선정하였다. 선정된 하전재질을 사용하여 연속처리가 가능한 마찰하전정전선별 장치를 개발하였으며, 다양한 조건별로 분리실험을 수행하여 시료의 회수 가능성을 확인하였다.

대마직물(안동포)의 방추가공에 관한 연구 (Study of Crease Resistant Finish on Hemp Fabrics(Andongpo))

  • 최희;김용;홍성학
    • 한국의류산업학회지
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    • 제6권2호
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    • pp.229-233
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    • 2004
  • Andongpo, 100% Korean hemp fabric was treated with the glyoxale resin type finishing agent and/or the soluble urethane type finishing agent to determine the optimum process condition of the crease resistant finish and the crease recovery of treated sample fabrics was evaluated for the study. The treatment conditions for the study were 6 conditions, such as, A-1~A-6, in which A-1 was the condition of treatment glyoxale resin type finishing agent only and A-2~A-6 were the condition of treatment both glyoxale resin type finishing agent and soluble urethane type finishing agent. Among the 6 conditions, the crease recovery of the sample treated with A-4 condition was $148^{\circ}$(angle of recovery method) and grade 3.2(appearance method) and so, these samples showed the excellent crease recovery. From the result, 15g/l of the catalyst conc., 50g/l of the glyoxale resin type finishing agent cone., and 40g/l of the softner were the optimum treatment condition for the crease resistant finish of the andongpo.

주성분분석과 공통요인분석에 대한 비교연구: 요인구조 복원 관점에서 (A Comparative Study on Factor Recovery of Principal Component Analysis and Common Factor Analysis)

  • 정선호;서상윤
    • 응용통계연구
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    • 제26권6호
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    • pp.933-942
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    • 2013
  • 본 연구에서는 시뮬레이션 방법을 사용해서 다양한 조건에서 주성분분석이 얼마나 잘 요인 구조를 복원할 수 있는지를 공통요인분석과 비교하여 체계적으로 평가하였다. 이 연구에서 요인 대 변수 비율, 공통성, 그리고 표본크기를 실험변수로 설정하였다. 주성분분석은 표본의 크기가 200개 이하인 경우 공통적으로 공통요인분석에 비해 더 우수한 요인구조의 복원력을 보여주었다. 특히, 요인 당 변수 수가 적은 경우, 주성분분석은 50개의 표본에서도 만족할 만한 수준의 요인복원능력을 보여주었다. 이와 더불어 공통성 수준 또한 낮은 경우 필요한 표본수는 100개로 늘어난다. 본 연구결과는 요인추출방법으로서 주성분분석의 선택의 근거를 제시하고 타당한 사용에 관한 가이드라인을 제시해 준다.