• Title/Summary/Keyword: Sample preparation effect.

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반용융 성형가공한 SiCp/AZ91HP Mg복합재료의 피로 및 내마모 특성 (Fatigue and Wear Properties of Semi-Liquid Formed SiCp/AZ91HP Mg Composites)

  • 하홍수;김명균;안선규;임병수;김영직
    • 한국주조공학회지
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    • 제17권5호
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    • pp.472-479
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    • 1997
  • The effect of size and mass fraction of SiC particulate on the fatigue and wear have been investigated for semi-liquid formed SiCp/AZ91HP Mg composites. In the study, different particulate sizes of 7, 20, $50 {\mu}m$ were prepared with various mass fraction for sample preparation. By tension-tension fatigue tests, whose procedures are standardized in ASTM standard 647E-93, the da/dN vs. ${\Delta}K$ curves were obtained. Also, the crack propagation paths were observed by optical microscope. As a result of wear test, specific wear loss is decreased with increasing mass fraction and particulate size. Specific wear loss of 30 mass% $50 {\mu}m$ SiC reinforced Mg composite is compared to SKD11.

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Preparation and Characterization of $Pd/CeO_2/Ta/Si$ model catalysts

  • 김도희;우성일
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2000년도 제18회 학술발표회 논문개요집
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    • pp.145-145
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    • 2000
  • M-CeO2 (M : noble metal) catalysts have been widely studied as three-way catalysts and methanol synthesis catalysts. Ceria is thought to play a number of roles in these catalysts. The Ce(IV)/Ce(III) redox pair may store/release gases under oxidizing/reducing conditions, extending the operational window. Additionally, metal-ceria interactions lead to several effects, including the dispersion of the active components and promoting the activation of molecules such as CO or NO. Pd is a promising component to current TWC formulations and behaves particularly well when compared with Pt and Rh-based catalysts for low-temperature oxidation of Co and hydrocarbon. However the effect of Pd-ceria interactions on the physicochemical properties of Pd and the redox properties of Ce is not elucidated yet. In order to know exactly about the metal-ceria interactions, the model study are expecting to give a better environment, resulting in the wide use of the surface science tools. The substrate was Si(100) wafer, on which Ta metal was sputtered as a thickness of 100nm. The CeO2 thin film of 30nm was deposited by using the magnetron sputtering. Spin coating and magnetron sputtering methods were used to make the Pd thin film layer. The prepared sample was investigated by in-situ XPS, AES, SEM and AFM analysis.

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Equo-Tip 경도값에 미치는 실험변수의 영향 (The Effect of Test Variables on the Accuracy of Equo-Tip Hardness)

  • 남승훈;전승범;김종집
    • 열처리공학회지
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    • 제3권2호
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    • pp.32-36
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    • 1990
  • For the accurate measurements of hardness in a material, it is necessary to have a thorough understanding of the effects of test variables on the accuracy of hardness value. For the rebound hardness test, major test variables are the radius of hammer ball tip, type of backing materials, size and roughness of the specimen. In this study, effects of these variables on Equo-Tip hardness value were investigated. Hardness measurements were carried out using WC balls with various sizes of worn-ot zone. The sample materials chosen for the experiments were commercial standard hardness blocks and SM45C steel bars subjected to either normalization or quench and temper treatments. As backing materials, aluminum, steel and rubber plates were used in all the experiments. Experimental results show that for the accurate measurements of Equo-tip hardness, it is necessary to use the hammer ball with a worn-out zone parameter of less than 0.23, and the recommended minimum thickness and width of the specimen are 25mm and 70mm, respectively. Further for the surface preparation, the specimens need to be polished with an emery paper of No. 400 or finer, and for the backing matrials, it is recommended to use steels or rubbers.

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Influence Factor on Magnetization Property of Carbonyl Iron-based Magnetorheological Fluids

  • Wang, Daoming;Zi, Bin;Qian, Sen;Qian, Jun;Zeng, Yishan
    • Journal of Magnetics
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    • 제21권4호
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    • pp.622-628
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    • 2016
  • Magnetization property is a critical factor for magnetorheological fluids (MRFs) to achieve the liquid-solid transition. The main focus of this study is on exploring the influence factors on magnetization properties of MRFs. In this paper, a theoretical analysis is performed to discuss the magnetization characteristics of MRFs firstly. Then, a method for the preparation of carbonyl iron-based MRFs is illustrated and five MRFs samples with various material parameters are prepared. It is succeeded by a series of experiments on testing the hysteresis loop and the magnetization curve of each sample and the influence factors are compared and analyzed. Experimental results indicate that there is basically no hysteresis phenomenon on MRFs which exhibits superparamagnetic behavior at room temperature. A surfactant coating on magnetic particles can slightly improve the MRFs magnetization. Additionally, the magnetic susceptibility and the saturation magnetization both increase with the particle concentration, whereas the influence of particle diameter is relatively very small. Moreover, as the temperature increases, the magnetization decreases and the declining rate accelerates gradually.

노인요양 시설 입소 노인 삶의 질 구조모형 (A Structural Equation Model of Quality of Life in Nursing Home Residents)

  • 신소홍;박정숙
    • 노인간호학회지
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    • 제20권3호
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    • pp.193-203
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    • 2018
  • Purpose: This study was done to develop a predictive model for quality of life of elderly residents in long-term care facilities (LTCF). The study was based on Brofenbrenner's ecological system theory and a literature review. Methods: Data were collected using a convenience sample of 205 elderly residents in 2 nursing homes located in D city and 1 nursing home located in K province. The exogenous variables were individual factors, family support, and facility environmental factors. The endogenous variables were self-esteem, accommodation adaptation and quality of life of elderly residents in LTCF. Collected data were analyzed through structural equation modeling using AMOS 20.0. Results: Eleven of the twelve hypotheses were supported, but the hypothesis that facility environment factors effect self-esteem was not supported. Quality of life of elderly residents in LTCF was explained first by facility environmental factors, followed by self-esteem, individual factors, accommodation adaptation, and family support with an explanatory power of 83.0%. Conclusion: To improve the quality of life of elderly residents in LTCF, the service and environment preparation provided by facilities is important, and it is necessary to provide emotional counseling to improve the self-esteem of these elders.

MWCNT와 여러가지 티탄알콕사이드 전구체를 사용하여 CNT/TiO2 복합체의 제조와 광촉매분해 (Preparation and photocatalytic degradation of CNT/TiO2 composites using MWCNT and various titanium alkoxide precursors)

  • 진명량;장봉군;오원춘
    • 분석과학
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    • 제21권6호
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    • pp.553-561
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    • 2008
  • MWCNT 와 여러 가지 티탄 알콕사이드 전구체를 사용하여 $CNT/TiO_2$ 복합제를 제조하였다. 이들 복합체들은 SEM, FE-SEM, XRD, EDX 및 UV-vis 분광기를 사용하여 종합적으로 분석하였다. UV 조사하에서 MB모델 수용액의 변이에 대한결과로부터 제조된 물질에 대한 광활성을 시험하였다. 마지막으로 MB 제거 실험의 결과에 따르면, 시료 CTOS의 경우 시료 CTIP 및 CTPP의 경우보다 우수한 MB제거 효과를 나타내었다.

난백분말과 카제인을 이용한 요구르트의 제조 (The Preparation of Yogurt from Egg White Powder and Casein)

  • 고영태;이은주
    • 한국식품과학회지
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    • 제28권2호
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    • pp.337-344
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    • 1996
  • 본 연구에서는 난백분말과 카제인에 포도당을 첨가하여 만든 기질을 젖산균(Lactobacillus)으로 발효하여 호상의 요구르트를 만든 후, 난백분말젖산균의 생육과 산생성 및 요구르트의 품질 (관능성, 휘발성 향기 성붕)에 미치는 영향을 조사하엿다. L. acidophilus로 24시간 발효된 시료의 경우 산도는 우유 시료(대조군)에 비하여 난백분말 1-3% 시료는 유의적으로 낮았으며(p<0.05), 난백분말 시료 가운데는 난백분말의 농도를 1%에서 3%로 증가시킴에 따라 산생성이 증가하였다. 새균구는 우유 시료가 $3.1{\times}10^9/ml$인데 비하여 난백분말 시료는 ${8.3\times}10^7/-36{\times}10^8/ml$으로 현저하게 낮았으며 대체적으로 낮은 농도의 단백분말이 첨가 된 시료에서 낮은 생균수를 나타냈다. L. acidophilus로 16.5시간 발효시켜 만든 호상요구르트 관능성을 보면, 전반적으로 기호도는 우유 요쿠르트 (표준시료)보다 난백분말 요구르트가 유의적으로 낮았으며 (p<0.05) 난백분말 요구르트 가운데는 2%와 3% 시료는 표준시료와 비교하여 큰 차이가 없었으나 1% 시료는 현저하게 저조하였다. 본 실험에서 사용된 L. acidophilus(KCTC 2182)는 시료에 따라서 다소 차이가 있으나 발효 과정에서 acetone, ethanol, diacetyl, acetoin을 생성하였다.

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시료 전처리 방법이 근적외선분광법을 이용한 이탈리안 라이그라스 사일리지의 화학적 조성분 및 발효품질 평가에 미치는 영향 (Effect of Sample Preparation on Predicting Chemical Composition and Fermentation Parameters in Italian ryegrass Silages by Near Infrared Spectroscopy)

  • 박형수;이상훈;최기춘;임영철;김종근;서성;조규채
    • 한국축산시설환경학회지
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    • 제18권3호
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    • pp.257-266
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    • 2012
  • 본 연구는 조사료 품질평가에서 근적외선 분광법의 현장 이용성 확대를 위하여 시료 전처리 방법에 따른 이탈리안 라이그라스 사일리지의 사료가치 및 발효품질의 예측정확성을 평가하기 위하여 수행되었으며 검량식 개발을 위하여 이탈리안 라이그라스 사일리지를 전북지역에서 174점을 수집하였다. 시료 전처리 방법은 사일리지를 건조 후 분쇄하는 방법과 원물 (생) 시료를 건조 분쇄하지 않는 방법을 두었으며 각각의 시료는 근적외선 분광기를 이용하여 스펙트럼을 측정한 후 측정된 스펙트럼과 실험실 분석값간에 상관관계를 이용한 다변량회귀분석법을 통하여 검량식을 유도한 다음 각 성분별로 예측 정확성을 평가하였다. 시료 전처리 방법에 따른 이탈리안 라이그라스 사일리지의 수분함량의 예측 정확성은 건조 분쇄하지 않은 원물(생)시료를 그대로 측정하는 방법 (SECV 1.37%, $R^2$=0.96)이 건조 분쇄처리 방법 (SECV 4.31%, $R^2$=0.68) 보다 예측 정확성이 높게 나타났다. ADF와 NDF 함량의 예측 정확성은 건조 후 분쇄처리한 방법이 개발된 검량식을 상호검증 (SECV)한 결과 각각 0.72% ($R^2$=0.97)와 0.85% ($R^2$=0.94)로 높게 나타났으며 조회분함량 평가에 대한 검량식개발 결과는 건조분쇄하지 않은 원물(생) 시료 전처리 방법에서 가장 낮은 정확성 (SECV 1.17%, $R^2$=0.66)을 나타내었다. pH와 젖산함량은 건조 분쇄 전처리 방법에서 각각 0.48 ($R^2$=0.87)와 0.24% ($R^2$=0.87)로 우수한 결과를 나타내었다. 이상의 연구결과를 종합해보면 근적외선분광법을 이용한 시료 전처리 방법에 따른 이탈리안 라이그라스 사일리지의 사료가치 및 발효품질 평가에 대한 예측정확성은 수분함량을 제외하고는 건조 후 분쇄하는 시료 전처리 방법이 예측 정확성 측면에서는 우수한 것으로 나타났으나 시료 전처리가 필요치 않은 원물(생) 시료의 측정 방법도 매우 양호한 예측 정확성을 보임으로써 실제 근적외선분광법의 현장 활용측면에서는 매우 유용한 전처리 방법으로 판단되어진다.

B3O2-TiO2-환원제-입자제어제계에서 자전연소합성법에 의한 BaTiO3분말의 제조 및 유전특성 (Preparation of BaTiO3 Powder in $BaO2-TiO2-Reduction Agent-PSCA (Particle Size Control Agent) System by SHS and Its Dielectric Properties)

  • 윤기석;임성재;;원창환
    • 한국세라믹학회지
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    • 제41권11호
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    • pp.842-850
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    • 2004
  • BaO$_2$-TiO$_2$-환원제-입자제어제계에서 자전연소합성법을 이용한 BaTiO$_3$ 분말의 제조에 대하여 고찰하였다. 환원제로서 C, Mg를 사용하였고, 입자제어제로서 NaCl을 사용하였다. 자전연소합성법을 이용한 BaTiO$_3$ 분말의 제조에 있어 최적의 반응계에서 환원제의 종류와 농도, 입자제어제, 반응량의 변화에 따른 생성물의 영향을 조사하였다. 최적의 반응계 및 조성은 Ae반응 분위기에서 BaO$_2$+TiO$_2$+0.1Mg+0.2C+0.75NaCl이었다. 희석제로서 첨가된 NaCl은 연소온도의 조절 뿐 아니라 반응생성물의 입도를 제어하는 효과를 나타냄을 알 수 있었다. 최적의 조건에서 제조된 순수 BaTiO$_3$ 분말의 입도는 약 0.5 $mu extrm{m}$ 이하였으며, 반응량을 증가시킬수록 균일한 반응성을 나타내었다 제조된 BaTiO$_3$ 분말의 유전특성을 측정하기 위하여 130$0^{\circ}C$, 2시간동안 대기중에서 소결실험을 행하였고 이때 상온에서의 유전상수는 약 2290이었고, 큐리점(129$^{\circ}C$)에서의 유전상수는 약 13800을 나타내었다.

국내 제조기업의 ERP 시스템 도입의 정량적 성과에 관한 연구 (The Quantitative Effects of ERP Systems in Korean Manufacturing Industry)

  • 장활식;박광오;최우혁;한정희
    • 경영과정보연구
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    • 제26권
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    • pp.27-60
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    • 2008
  • Researches on the introduction of ERP system kept on examining the critical successful factors (CSFs) that focus on factors to achieve effectively successful projects, and trying to measuring the actual effectiveness of the introduction of ERP system. However, most of the preceding researches on the effectiveness of the introduction of ERP system that was searching devoted effects has been ceased, and actually even researches on the economical results have just done the basic cognitive evaluation of result indicators by many questionnaires instead of objective measuring values, because of the difficulty of measuring the evaluation of the result. Moreover, researches on positive effects of the introduction of ERP on enterprise results and researches that failed to give advantageous effects showed different results each other. And a part of researches reported that only a part of result indicators were partially affected. In this research, we investigated Korean large enterprises or middle-sized enterprises in manufacture industry that introduces SAP R/3 and Oracle package to compare their quantitative financial results after the introduction of ERP system, in order to measure the effects of the ERP system. First, we evaluated the difference of the quantitative financial results before and after the introduction of the ERP system. Second, we evaluated the opportunities shown by the effects after the introduction of the ERP system. Third, we removed the sample of the exchange crisis (IMF) and executed the additional analysis to reflect the average increasing and decreasing rate in the industry, so that pure evaluation can be achieved. Inherent limits of precedent researches are removed and practical effects of the pure introduction of the ERP system are evaluated, so the research of this research is significant. The result of this research is as follows. Because of the introduction of ERP, the rate of turnover of inventory property has increased and sales of preparation inventory property have decreased so that more effective inventory property management has been achieved. Moreover, preparation sales of labor costs and preparation sales of the number of employees have decreased to show the effect of the reduction of labor costs. However, it could no be concluded that we could increase the profit due to the introduction of ERP system. Due to the introduction of ERP, although we concluded that the return on assets (ROA) and the additional value of one-person employee statistically showed obvious differences and increased, the return on equity failed to show obvious differences after the process of introduction of ERP.

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