• 제목/요약/키워드: Sample array

검색결과 204건 처리시간 0.023초

당약의 swertiamarin 분석을 위한 추출조건 최적화 (Optimization of Extraction Conditions for Swertiamarin in Swertia japonica Makino)

  • 김태희;장설;이아름;이아영;최고야;김호경
    • 대한본초학회지
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    • 제29권1호
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    • pp.13-18
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    • 2014
  • Objectives : Iridoid glycoside, swertiamarin is a well known bioactive component found in Swertia japonica Makino (SJ). In this study, we tried to optimize a suitable method which would extract swertiamarin effectively. Methods : Extraction of SJ was carried out by various conditions of time (5 - 60 min), temperature ($30-70^{\circ}C$), solvent (from non-polar to polar), and ratio of solvnet / sample (10 : 1 - 40 : 1) using ultrasonic extractor. Swertiamarin in SJ extracts was quantified by high performance liquid chromatography - Phtodiode array detector (HPLC-PDA) using C18 column and the analytical procedure was validated by evaluation of specificity, range, linearity, accuracy (recovery), precision (intra- and inter day variability), limit of detection (LOD), and limit of quantification (LOQ). Results : An efficient extraction condition for swertiamarin in SJ was optimized using sonicator extraction (temperature $40^{\circ}C$, solvent 20% methanol, solvent / sample (20 : 1), and time 10 min. Analytical procedure was optimized by HPLC-PDA using isocratic solvent system of acetonitrile and water (9 : 91), and the method was validated in regard to linearity (correlation coefficient, $R^2$ > 0.9999), range ($50-1000{\mu}g/mL$), intra- and inter-precision (RSD < 5.0 %), and recovery (99 -103 %). LOD and LOQ were 0.051 and $0.155{\mu}g/mL$, respectively. Conclusion : An optimized method of extraction for swertiamarin in SJ was established through conditions of diverse extraction and the validation result indicated that the method is suited for the determination of swertiamarin in SJ.

HI gas kinematics of paired galaxies in the cluster environment from ASKAP pilot observations

  • Kim, Shin-Jeong;Oh, Se-Heon;Kim, Minsu;Park, Hye-Jin;Kim, Shinna
    • 천문학회보
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    • 제46권2호
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    • pp.70.1-70.1
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    • 2021
  • We examine the HI gas kinematics and distributions of galaxy pairs in group or cluster environments from high-resolution Australian Square Kilometer Array Pathfinder (ASKAP) WALLABY pilot observations. We use 32 well-resolved close pair galaxies from the Hydra, Norma, and NGC 4636, two clusters and a group of which are identified by their spectroscopy information and additional visual inspection. We perform profile decomposition of HI velocity profiles of the galaxies using a new tool, BAYGAUD which allows us to separate a line-of-sight velocity profile into an optimal number of Gaussian components based on Bayesian MCMC techniques. Then, we construct super profiles via stacking of individual HI velocity profiles after aligning their central velocities. We fit a model which consists of double Gaussian components to the super profiles, and classify them as kinematically cold and warm HI gas components with respect to their velocity dispersions, narrower or wider 𝜎, respectively. The kinematically cold HI gas reservoir (M_cold/M_HI) of the paired galaxies is found to be relatively higher than that of unpaired control samples in the clusters and the group, showing a positive correlation with the HI mass in general. Additionally, we quantify the gravitational instability of the HI gas disk of the sample galaxies using their Toomre Q parameters and HI morphological disturbances. While no significant difference is found for the Q parameter values between the paired and unpaired galaxies, the paired galaxies tend to have larger HI asymmetry values which are derived using their moment0 map compared to those of the non-paired control sample galaxies in the distribution.

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Comparison of terrestrial insect communities associated with the crabgrass (Digitaria ciliaris) community, Korea

  • Jeong Ho Hwang;Jong-Hak Yun
    • Journal of Ecology and Environment
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    • 제47권4호
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    • pp.250-260
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    • 2023
  • Background: Crabgrass (Digitaria ciliaris, Poaceae) is a globally distributed weed, including in Afro-Eurasia, America, and Australia. As a highly gregarious plant, crabgrass is an important habitat for a diverse array of insects, and a potential habitat for agricultural pests. To compare the insect communities associated with the crabgrass community, insects were sampled using sweep sampling (100 sweeps per sample) at five sites, including Daejeon (Daejeon and Gap rivers), Anseong, Namhae, and Inje, with a focus on the Daejeon River. Results: A total of 5,888 individual insects belonging to eight orders, 42 families, and 115 species were collected from the five sites. Both the number of species and individuals of Hemiptera were the highest at all of the sites. In the present study, 73% of the insect population fed on D. ciliaris as a host plant. The dominant species in the D. ciliaris community was Laodelphax striatellus (Delphacidae), being ubiquitous at all the sites which showed a high abundance of rice pests in the communities and the suitability of D. ciliaris as an alternative host plant for them. The Shannon-Wiener diversity index was highest in Inje on 17 September (2.88), and the Chao1-bc diversity index was highest in the Gap River on 5 September (80). The sampling efficiency of 100 sweep samples (sample coverage) was calculated to be as high as 90%. The results of the samples taken from September to November in the Daejeon River showed that the number of species and individuals decreased gradually over time, and the number of dominant species decreased sharply between September and October. Similarity analysis indicated that sampling dates that were closer together yielded sampled assemblages with higher faunal similarity. In addition, in each sampling, the difference in the minimum temperature during the two-week period prior to sampling and faunal similarities were negatively correlated. Conclusions: This study provides foundational data that could enhance our understanding of insect diversity in D. ciliaris. The data can facilitate ecological conservation and management of Korean grasslands generally, as well as identification of potential pests that may disperse from D. ciliaris communities to nearby farmland.

Identifying Young AGNs using the Korean VLBI Network

  • Jeong, Yongjin;Sohn, Bong Won;Chung, Aeree
    • 천문학회보
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    • 제40권1호
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    • pp.42.2-42.2
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    • 2015
  • High frequency peakers (HFPs) are promising candidates for young active galactic nuclei (AGNs). Their small physical scale (< 1 kpc) and radio spectrum peaked at high frequency (> 5 GHz) are suggestive that it has been only about $10^2-10^3$ years since a central massive black hole in their host galaxies was launched. Until recently however, long-term monitoring radio observations at frequencies which are high enough to cover the true peak of HFP candidates were rare. Therefore, previous HFP samples are often contaminated by blazars, which are highly variable, hence may show a similar radio spectrum as HFPs depending on the observational epoch. In this work, we challenge to identify genuine young AGNs by monitoring HFP candidates at high radio frequencies. We performed single-dish monitoring of 19 candidates in 18 epochs over 2.5 years at 22 and 43 GHz using the Korean VLBI Network (KVN). Also, using KaVA, a combined array of the KVN and the VERA in Japan, we carried out 22 GHz VLBI observations of two HFPs and one blazar selected from our sample in order to compare their parsec scale (milli-arcsecond scale) morphology. HFPs are expected to have double/triple features, so called compact symmetric objects, which are scaled-down versions of extended radio galaxies, while blazars typically show core-jet morphology. We discuss the properties of AGNs at their very early evolutionary stage based on the results of the KVN and KaVA observations.

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영상 신호 처리용 8-bit 10-MHz A/D 변환기 (8-bit 10-MHz A/D Converter for Video Signal Processing)

  • 박창선;손주호;이준호;김종민;김동용
    • 한국음향학회:학술대회논문집
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    • 한국음향학회 1999년도 학술발표대회 논문집 제18권 2호
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    • pp.173-176
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    • 1999
  • In this work, a A/D converter is implemented to obtain 8bit resolution at a conversion rate of 10Msample/s for video applications. Proposed architecture is designed low power A/D converter that pipelined architecture consists of flash A/D converter. This architecture consists of two identical stages that consist of sample/hold circuit, low power comparator, voltage reference circuit and MDAC of binary weighted capacitor array. Proposed A/D converter is designed using $0.25{\mu}m$ CMOS technology The SNR is 76.3dB at a sampling rate of 10MHz with 3.9MHz sine input signal. When an 8bit 10Msample/s A/D converter is simulated, the Differential Nonlinearity / Integral Nonlinearity (DNL/ INL) error are ${\pm}0.5/{\pm}2$ LSB, respectively. The power consumption is 13mW at 10Msample/s.

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신호부각에 의한 신호 부공간 회전을 이용한 광대역 인코히어런트 신호의 공간 스펙트럼 추정 (Spatial Spectrum Estimation of Broadband Incoherent Signals using Rotation of Signal Subspace Via Signal Enhancement)

  • 김영수;이계산;김정근
    • 한국전자파학회논문지
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    • 제15권7호
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    • pp.669-676
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    • 2004
  • 등 간격 선형 어레이로 입사하는 광대역 인코히어런트 신호의 도래각을 효율적으로 추정하는 새로운 알고리즘을 제안한다. 변환행렬을 구성하기 위하여 CSM 방법이 초기 추정각을 요구하는 반면에 제안된 방법은 전혀 초기 추정각을 필요로 하지 않는다. 이 방법의 연산과정은 먼저 신호부각 방법에 의하여 중심주파수에서의 신호 부공간을 추정 한 다음 신호 부공간 회전 방법을 통한 직교변환행렬을 구성하는 것이다. 시뮬레이션 결과 제안된 방법이 CSM 방법보다 표본바이어스 면에서 우수한 성능을 제공함을 알 수 있었다.

산조인의 수치에 따른 Spinosin 함량 비교 (A Comparison of Spinosin Content in Zizyphi Semen and Its Processed Products by Roasting)

  • 서창섭;김정훈;신현규;김병수
    • 생약학회지
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    • 제47권4호
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    • pp.360-365
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    • 2016
  • The aim of this study was to compare the amount of spinosin in the 70% ethanol extracts of non-processed Zizyphi Semem (ZS) and processed ZS by roasting using a high-performance liquid chromatography equipped with photodiode array detector. Separation of the spinosin was used $SunFire^{TM}$ $C_{18}$ analytical column ($5{\mu}m$, $4.6{\times}150mm$) using two mobile phase consisting of distilled water and acetonitrile, both with 1.0% (v/v) acetic acid. The flow rate was 1.0 mL/min and injection volume was $10{\mu}L$. Calibration curve of the spinosin was y = 22339.45x+483.99 in tested concentration range ($1.28-20.00{\mu}g/mL$) and correlation coefficient was 1.0000. In non-processed ZS sample, the amount of the spinosin was 0.94 m/g, while, the amount of the marker compound in processed ZS samples were 0.66-1.10 mg/g.

NEW DEVELOPED PORTABLE NEAR INFRARED (NIR) SYSTEM USING MICROSPECTROMETER

  • Woo, Young-Ah;Ha, Tae-Kyu;Kim, Jae-Min;Kim, Hyo-Jin
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1123-1123
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    • 2001
  • In recent years, a miniature spectrometer has been extensively developed due to the marriage of fiber optics and semiconductor detector array. This type of miniature spectrometer has advantages of low price and robustness due to the capability of mass production and no moving parts are required such as lenses, mirrors and scanning monochromator. These systems are ideal for use in teaching labs, process monitoring and field analyses. A portable near infrared (NIR) system has been developed for qualitative and quantitative analysis. This system includes a tungsten halogen lamp for light source, a fiber optics connected a light source, and a sample module to the microspectrometer, The size of spectrometer can be as small as 2.5 cm x 1.5 cm x 0.1 cm. Wavelength ranges can be chosen as 360-800 nm, 800-1100 nm and 1100-1900 nm depending on the type of detector. The software consists of various tools for multivariate analysis and pattern recognition techniques. To evaluate the system, long and short-term stability, wavelength accuracy, and stray light have been investigated and compared with conventional scanning type NIR spectrometer. This developed system can be sufficiently used for quantitative and qualitative analysis for various samples such as agricultural product, herbal medicine, food, petroleum, and pharmaceuticals, etc.

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Design, Implementation and Testing of HF transformers for Satellite EPS Applications

  • Zahran, Mohamed
    • Journal of Power Electronics
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    • 제8권3호
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    • pp.217-227
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    • 2008
  • The electric power subsystems (EPS) of most remote sensing satellites consist of a solar array as a source of energy, a storage battery, a power management and control (PMC) unit and a charge equalization unit (CEU) for the storage battery. The PMC and CEU use high frequency transformers in their power modules. This paper presents a design, implementation and testing results of a high frequency transformer for the EPS of satellite applications. Two approaches are used in the design process of the transformer based on the pre-determined transformer specifications. The transformer is designed based on an ETD 29 ferrite core. The implemented transformer consists of one center-tapped primary coil with eleven center-tapped secondary coils. The offline calculation results and measured values of R, L for transformer coils are convergence. A test circuit for measuring the transformer parameters like voltage, current and B-H hysteresis was implemented and applied. The test results confirm that the voltage waveforms of both primary and secondary coils were as desired. No overlapping occurred between the control signal and the transformer, which was not saturated during testing even during a short circuit test of the secondary channels. The dynamic B-H loop characteristics of the used transformer cores were measured. The sample test results are given in this paper.

수치에 따른 건강 중 6-Gingerol의 함량 비교 (Content of 6-Gingerol in Zingiberis Rhizoma by Roasting)

  • 서창섭;김정훈;신현규;김병수
    • 생약학회지
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    • 제48권3호
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    • pp.226-231
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    • 2017
  • Zingiberis Rhizoma (ZR, Zingiberaceae) is one of the foods for a long time and contains various biological activities including anti-cancer, anti-inflammatory, anti-oxidant, and anti-platelet activities. The present study was to compare the amount of 6-gingerol in the 70% ethanol extracts of non-processed ZR and processed ZR by roasting using a high-performance liquid chromatography equipped with photodiode array detector. The 6-gingerol was separated on a Gemini $C_{18}$ analytical column ($5{\mu}m$, $4.6{\times}250mm$) using two mobile phase consisting of distilled water and acetonitrile. The flow rate was 1.0 mL/min and injection volume was $10{\mu}L$. In non-processed ZR sample, the amount of the 6-gingerol was 0.43% and the amount of the marker compound in processed ZR samples by roasting were 0.16-0.55%.