• Title/Summary/Keyword: Sample Storage Method

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Synthesis of Perforated Polygonal Cobalt Oxides using a Carbon Nanofiber Template (탄소나노섬유 모형을 이용한 천공된 다각형 코발트 산화물 합성)

  • Sin, Dong-Yo;An, Geon-Hyoung;Ahn, Hyo-Jin
    • Journal of Powder Materials
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    • v.22 no.5
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    • pp.350-355
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    • 2015
  • Perforated polygonal cobalt oxide ($Co_3O_4$) is synthesized using electrospinning and a hydrothermal method followed by the removal of a carbon nanofiber (CNF) template. To investigate their formation mechanism, thermogravimetric analysis, field-emission scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy are examined. To obtain the optimum condition of perforated polygonal $Co_3O_4$, we prepare three different weight ratios of the Co precursor and the CNF template: sample A (Co precursor:CNF template- 10:1), sample B (Co precursor:CNF template-3.2:1), and sample C (Co precursor:CNF template-2:1). Among them, sample A exhibits the perforated polygonal $Co_3O_4$ with a thin carbon layer (5.7-6.2 nm) owing to the removal of CNF template. However, sample B and sample C synthesized perforated round $Co_3O_4$ and destroyed $Co_3O_4$ powders, respectively, due to a decreased amount of Co precursor. The increased amount of the CNF template prevents the formation of polygonal $Co_3O_4$. For sample A, the optimized weight ratio of the Co precursor and CNF template may be related to the successful formation of perforated polygonal $Co_3O_4$. Thus, perforated polygonal $Co_3O_4$ can be applied to electrode materials of energy storage devices such as lithium ion batteries, supercapacitors, and fuel cells.

A Motor/Generator for Flywheel Energy Storage System Levitated by Bulk Superconductor (초전도 부상 플라이휠 에너지 저장시스템의 구동을 위한 전동/발전기)

  • Go, Chang-Seop;Yeon, Je-Uk;Choe, Jae-Ho;Jeong, Hwan-Myeong;Hong, Gye-Won;Lee, Ho-Jin
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.49 no.6
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    • pp.411-420
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    • 2000
  • The energy storage systems are being widely researched for the high quality of the electric power. The FES(flywheel energy system) is especially, on the center of the research because it does not make any pollution and its life is long. The FES converts the electrical energy into the mechanical kinetic energy of the flywheel and reconverts the mechanical energy into the electrical energy. In order to store as much energy as possible, the flywheel is supposed to be rotated with very high speed. The motor/generator of the FES should be high efficient at high speed, and generate constant torque with respect to the rotation. In this paper, a motor/generator employing a Halbach array of permanent magnets is designed and constructed to meet the requirements, and its characteristics are examined. The magnetic field is analysed by using the magnetic surface charge method. The armature winding is designed for the harmonic components to be minimized by using the FFT. The sinusoidal current for the motor driving are generated by the hysteresis current controller. A sample superconducting flywheel energy storage system is constructed with a duralumin flywheel which has a maximum rotating speed of 40,000[rpm] and a stored energy of 240[Wh] and its validity is examined through the experiment.

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Reliability Evaluation with Wind Turbine Generators and an Energy Storage System for the Jeju Island Power System (제주도 계통에서의 풍력발전기 및 ESS를 고려한 신뢰도 평가)

  • Oh, Ungjin;Lee, Yeonchan;Lim, Jintaek;Choi, Jaeseok;Yoon, Yongbeum;Chang, Byunghoon;Cho, Sungmin
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.64 no.1
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    • pp.1-7
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    • 2015
  • This paper proposes probabilistic reliability evaluation model of power system considering Wind Turbine Generator(WTG) integrated with Energy Storage System(ESS). Monte carlo sample state duration simulation method is used for the evaluation. Because the power output from WTG units usually fluctuates randomly, the power cannot be counted on to continuously satisfy the system load. Although the power output at any time is not controllable, the power output can be utilized by ESS. The ESS may make to smooth the fluctuation of the WTG power output. The detail process of power system reliability evaluation considering ESS cooperated WTG is presented using case study of Jeju island power system in the paper.

Microstructural Changes of Mayonnaise during Storage (마요네즈 저장 중 미세구조의 변화)

  • Song, Young-Sun
    • Korean Journal of Food Science and Technology
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    • v.22 no.3
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    • pp.300-306
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    • 1990
  • The microstrutural changes of mayonnaise during storage were examined by light microscopy (LM) and scanning electron microscopy (SEM). Fresh mayonnaise was composed of heterogenous population of dispersed spherical oil droplets and droplet size was normally distributed with one mode. During storage at $60^{\circ}C\;and\;-10^{\circ}C$, a shift in droplet size distribution toward larger droplets was observed, as a result of coalescence of lipid droplets. Turbidimetric study also confirmed that coalescence was occurring during this accelerated aging treatments. Measurements obtained from SEM microgrphs provided better determination of smaller droplets and resulted in lower mean diameter of droplets than those obtained from LM. From these results, SEM was found to be an advantageous method of examining emulsion products as compared to LM, providing a better resolution of small droplets and a more representative view of droplet distribution, as dilution of the sample was avoided.

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Evaluation for Loss Rate of Carbon Dioxide by Sample Storage Method (시료 보관 방법에 따른 이산화탄소 시료의 유실율 평가)

  • Cho, Chang-Sang;Lee, See-Hyung;Lim, Ki-Kyo;Yoo, Jung-Hwa;Sa, Jae-Hwan;Jeon, Byung-Gwan;Jeon, Eui-Chan
    • Journal of Climate Change Research
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    • v.2 no.4
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    • pp.309-316
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    • 2011
  • The study evaluated the loss rate of carbon dioxide, which is the prevalent greenhouse gas, according to the method of keeping specimens using standard gases. In order to examine the difference generated by a bag of storing specimens, it checked the loss rate according to concentration and time by making a 2nd set of standard gases in a Tedlar bag and an Aluminium bag. The containers lost gases at a rate of 5% or more after 6 day, and 10% or more after 15 days in both bags. In time, it was confirmed that the loss rate of the Aluminium bag was higher than that of the Tedlar bag. Specifically, there was no significant difference between the two bags after 12 days had passed, but by the 15th day, it was confirmed that the loss in an Aluminium bag was more severe than that in the Tedlar bag. The study went on to check the relations between the humidity in storage and the loss rate. The results showed that there was no significant effect of humidity on the loss rate until 72 hours had passed, when the loss rate in the Tedlar bag with high humidity was about 5% higher than that of the Tedlar bag in dry conditions. This study examined the loss rate of carbon dioxide, a typical greenhouse gas. It is important to note that the loss rate was determined by calculating highly reliable carbon dioxide emission and emission coefficient data, with consideration to the method of keeping specimens.

Physicochemical Characteristics of Gamma Irradiated Changran Jeotkal during Storage at $10^{\circ}C$ (감마선 조사기술을 이용하여 제조된 양념창란젓갈의 이화학적 품질특성)

  • Lee, Na-Young;Jo, Cheo-Run;Lee, Won-Dong;Kim, Jae-Hyun;Byun, Myung-Woo
    • Korean Journal of Food Science and Technology
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    • v.35 no.6
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    • pp.1129-1134
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    • 2003
  • Changran jeotkal, a Korean traditional fermented seafood, was prepared as a pilot scale using a commercial method and irradiated at 0, 2.5, 5.0 and 10 kGy by gamma ray to investigate possibilities for further industrial application. To see the effectiveness and rapid industrialization, hot pepper powder was irradiated at 10 kGy and manufactured the changran jeotkal (HP-10 kGy) as same method since the hot pepper powder was approved legally for gamma irradiation in Korea. The content of volatile basic nitrogen and amino nitrogen was significantly reduced by gamma irradiation in all storage periods. Amino nitrogen contents of 0, 2.5, 5.0, 10 kGy and HP-10 kGy were 98.9, 98.5, 92.4, 88.0 and 93.1mg%, respectively after 12 week of storage at $10^{\circ}C$. In total, 8 kinds of biogenic amines were found from the samples, and the contents in the gamma irradiated changran Jeotkal were lower than those of the control during storage. The sample of HP-10 kGy showed similar physicochemical characteristics to the sample irradiated as $2.5{\sim}5.0\;kGy$. Results indicated that gamma irradiation of fermented seafood products such as seasoned changran jeotkal improved quality stability, thus, we recommend gamma irradiation for industrial application.

Physicochemical Properties of Chaga (Inonotus obliquus) Mushroom Powder as Influenced by Drying Methods

  • Lee, Min-Ji;Seog, Eun-Ju;Lee, Jun-Ho
    • Preventive Nutrition and Food Science
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    • v.12 no.1
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    • pp.40-45
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    • 2007
  • The effects of drying methods on the physicochemical properties of chaga (Inonotus obliquus) mushroom powder were investigated. Scanning electron micrograph revealed that freeze drying produced smaller particle- sized samples which in turn resulted in higher porosity than did vacuum and hot-air drying. Samples prepared by freeze drying showed a significantly higher L*-value as compared with those prepared by hot-air drying and vacuum drying (p<0.05). The lightness (L*-value) significantly decreased with increasing relative humidity and storage temperature regardless of drying method (p<0.05). The yellowness (b*-value) increased significantly with increasing relative humidity (p<0.05). Browning index was significantly lower in samples prepared by freeze drying (p<0.05) but not significantly different between samples dried by hot-air and vacuum drying. Freeze dried sample exhibited a significantly higher degree of rehydration than other samples (p<0.05) probably due to the small particle size. Water solubility of the freeze dried sample was higher than those of the other methods while swelling ratio of the same sample appeared to be lower than those of others. Freeze dried chaga mushroom powder contained significantly lower amount of total phenolics and total sugar as compared to other samples (p<0.05).

Feasibility Study of Environmental and Geographical Data Transfer (EGDT) Device for Wide-Area Environmental Sampling in Undeclared Areas

  • Seungil Ha;Dalhyeon Ryu;Giyoon Kim;Myungsoo Kim
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.22 no.2
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    • pp.145-157
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    • 2024
  • Undeclared nuclear activities are challenging given the lack of information from the sites involved in such activities. Wide-area environmental sampling (WAES) can be an effective method to detect undeclared nuclear activities. However, it is crucial to address the potential risks during the WAES, including sample tampering or extortions. Therefore, tracking and monitoring of various on-site data is imperative to accurately interpret the status of samples and workers throughout the WAES process. 'Environmental and Geographical Data Transfer (EGDT)' was developed for the real-time monitoring of integrated on-site data. EGDT module is equipped with various sensors and can be attached to a worker's uniform or a sample storage box. This study demonstrated the technical effectiveness of EGDT by exploring three experimental methodologies for feasibility assessment. Compared to the Normal Operation case, the inference of the Sample Extortion case was predominantly based on changes in lux and dose rate. The inference of the Out-of-Work-Area case primarily relied on changes in dose rate and acceleration. Finally, the preliminary evaluation of the performance of the developed prototype was conducted, and a foundation was established for enhancing the application in the WAES process.

Effects of vacuum and high-oxygen modified atmosphere packaging on physico-chemical and microbiological properties of minced water buffalo meat

  • Jaberi, Rahimeh;Kaban, Guzin;Kaya, Mukerrem
    • Asian-Australasian Journal of Animal Sciences
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    • v.32 no.3
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    • pp.421-429
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    • 2019
  • Objective: In this study, the effects of vacuum (VP) and high-oxygen modified atmosphere ($80%\;O_2+20%\;CO_2$) packaging (HiOx-MAP) on physico-chemical and microbiological properties of minced water buffalo meat were investigated. Methods: After minced meat preparation, samples were packaged under VP and HiOx-MAP and stored at $2^{\circ}C{\pm}0.5^{\circ}C$ for 14 days. Samples taken on certain days were subjected to total aerobic mesophilic bacteria, total aerobic psychrotrophic bacteria, lactic acid bacteria, Pseudomonas, Enterobacteriaceae and yeast-mold counts as well as pH, color ($L^*$, $a^*$, and $b^*$) and thiobarbituric acid reactive substances (TBARS) analyses. Results: In minced water buffalo meat packaged under HiOx-MAP, TBARS value exceeded 1 mg malondialdehyde/kg on the 4th day of the storage. In VP samples, TBARS value remained close to initial TBARS value during storage. According to the findings, $a^*$ value was determined to be high in the HiOx-MAP samples within initial days of the storage. However, no significant changes in $a^*$ value were observed in VP samples during storage. In contrast, the mean value of $L^*$ was detected as higher in HiOx-MAP sample than VP samples. The count of psychrotrophic bacteria increased more than that of mesophilic bacteria during storage. The growth of Enterobacteriaceae and Pseudomonas was delayed in both the packaging methods. However, lactic acid bacteria exhibited more growth in VP samples compared to MAP samples. Conclusion: The lipid oxidation proceeded faster than expected in minced water buffalo meat packed with HiOx-MAP method. This situation adversely affected the $a^*$ value. On the other hand, similar microbiological results were obtained in both packing methods.

Analysis of an HTS coil for large scale superconducting magnetic energy storage

  • Lee, Ji-Young;Lee, Seyeon;Choi, Kyeongdal;Park, Sang Ho;Hong, Gye-Won;Kim, Sung Soo;Lee, Ji-Kwang;Kim, Woo-Seok
    • Progress in Superconductivity and Cryogenics
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    • v.17 no.2
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    • pp.45-49
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    • 2015
  • It has been well known that a toroid is the inevitable shape for a high temperature superconducting (HTS) coil as a component of a large scale superconducting magnetic energy storage system (SMES) because it is the best option to minimize a magnetic field intensity applied perpendicularly to the HTS wires. Even though a perfect toroid coil does not have a perpendicular magnetic field, for a practical toroid coil composed of many HTS pancake coils, some type of perpendicular magnetic field cannot be avoided, which is a major cause of degradation of the HTS wires. In order to suggest an optimum design solution for an HTS SMES system, we need an accurate, fast, and effective calculation for the magnetic field, mechanical stresses, and stored energy. As a calculation method for these criteria, a numerical calculation such as an finite element method (FEM) has usually been adopted. However, a 3-dimensional FEM can involve complicated calculation and can be relatively time consuming, which leads to very inefficient iterations for an optimal design process. In this paper, we suggested an intuitive and effective way to determine the maximum magnetic field intensity in the HTS coil by using an analytic and statistical calculation method. We were able to achieve a remarkable reduction of the calculation time by using this method. The calculation results using this method for sample model coils were compared with those obtained by conventional numerical method to verify the accuracy and availability of this proposed method. After the successful substitution of this calculation method for the proposed design program, a similar method of determining the maximum mechanical stress in the HTS coil will also be studied as a future work.