• Journal of the Korean Geotechnical Society
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• v.26 no.4
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• pp.37-45
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• 2010

Salt cementation, a typical naturally-cemented phenomenon, may occur due to water evaporation under the change of climate. Capillary force may influence the distribution of cement in granular soils. This study addresses the effect of capillary force on salt cementation using five different techniques: cone penetration test, electrical conductivity measurement, photographic imaging technique, nondestructive imaging technique, and process monitoring by elastic wave. Glass beads modeling a particulate media was mixed with salt water and then dried in an oven to create the cementation condition. Experimental results show that salt cementation highly concentrates at the top of the small particle size specimens and at the middle or the bottom of the large particle specimens. The predicted capillary heights are similar to the locations of high salt concentration in the cemented specimens. Five suggested methods show that the behavior of salt-cemented granular media heavily depends on the capillary force.

• Proceedings of the Korean Geotechical Society Conference
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• 2009.03a
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• pp.255-264
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• 2009

Soils containing vanishing materials lead changes in the microstructure of particulate media due to water inflow. Thus, dissolution renders some local unstability. As the moisture contents decease, the component of the vanished materials may affects on the cementation of paniculate materials. This cementation phenomenon has a huge influence on the stiffness, strength and stability under lower stress level. The goal of this study is to introduce the cementation effects on a compressional wave velocity, a shear wave velocity, and the resonant frequency of shear waves. The glass bead and salt water with different mole contents are used. Test results show that the changes of shear and compressional wave velocities consist of three stages. In the first region, compressional wave velocities increase and shear wave velocities decrease with a decreases in reducing water contents from 100% to 90~95%. In the second region, shear and compressional wave velocities become stable at 90~95% to 10% of the water contents. In the third region, shear and compressional wave velocities increases dramatically with a decrease in the water content due to the capillary force and cementation of salt. Furthermore, the resonant frequency of the shear waves shows similar phenomenon. Specimens prepared by glass beads and salt water are proved to be able to provide a meaningful insight in under structural behaviors of the cementation.

• Proceedings of the Korean Geotechical Society Conference
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• 2009.09a
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• pp.472-481
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• 2009

Cementation phenomenon has a huge influence on geotechnical stiffness and strength under low confining pressure. The goal of this study is to evaluate the characteristics of stiffness according to the depth. The piezo disk elements are installed at each layer of the cell for the detection of the compressional waves. The change of compressional wave velocity is classified by three stages. The compressional wave velocities are shown different according to the depth. The compressional wave velocity is especially influenced by cementation, effective stress, and coordinate number. Furthermore, the electrical conductivity and cone tip resistance are measured according to the depth. The electrical conductivity and the cone tip resistance show the similar trend with the compressional wave velocity. This study shows that the cementation by salt is affected by the depth on the granular materials.

• Proceedings of the Korean Geotechical Society Conference
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• 2010.03a
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• pp.448-456
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• 2010

The mechanical behavior of granular soils is affected by particle bonding including natural cementation. This study addresses a simple model of small strain stiffness and salt concentration based on wave measurements of salt-cemented particulate media. Published models of artificially cemented soils with different curing methods and several types of cementation agents are reviewed. Glass beads with the median diameter of D50 = 0.5mm are prepared in rectangular cells using the water-pluviated method in salt water with different concentrations. Piezo disk elements and bender elements embedded in the cell are used for the measurements of compressional and shear waves. The relationships between elastic wave velocities and salt concentration show an exponential function. The measured small strain stiffness matches well the predicted small strain stiffness based on micromechanics for simple cubic monosized sphere particles. This study demonstrates that the salt concentration in salt-cemented specimen may be evaluated by using elastic wave velocities.

• Journal of the Korean Geotechnical Society
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• v.25 no.5
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• pp.75-86
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• 2009

Salt, one of the most common soluble materials in engineering soil, may have an effect on mechanical behaviors of soils under its cementation process. In order to investigate this natural phenomenon, non-soluble material by using glass beads is mixed with salt electrolyte and cemented by using oven to evaporate water. Three different sizes of glass bead particles, 0.26, 0.5, and 1.29 mm, with different salt concentration, 0, 0.1, 0.2, 0.5, 1.0, and 2.0M, are explored by using P- and S-waves, excited by bender elements and piezo disk elemets, respectively. The velocities of the P-wave and S-wave of the particulate medium cemented by salt show three stages with the degree of saturation: 1) S-wave velocities increase while P-wave velocities reduce with degree of saturation changing from 100% to 90%; 2) Both velocities are stable with degree of saturation varying from 90% to 10%; 3) The velocities change enormously when the specimens are nearly dry with degree of saturation from 10% to 0%. Besides, the resonance frequencies of S-wave show similar stages to the S-wave velocities. This study demonstrates meaningful trends of elastic wave characteristics of geo-materials according to the cementation of dissolved salt.

• Nuclear Engineering and Technology
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• v.54 no.9
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• pp.3235-3241
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• 2022

The Korea Atomic Energy Research Institute (KAERI) is planning the construction of the KIJANG Research Reactor (KJRR) for stable supply of ⁹⁹Mo. The Fission ⁹⁹Mo Production Process (FMPP) of KJRR produces solid waste such as spent uranium cake and alumina cake, and liquid waste in the form of intermediate level liquid waste (ILLW) and low level liquid waste (LLLW). This study thus established the operating range and optimum operating conditions for the cementation of ILLW from FMPP. It also evaluated whether cement waste form samples produced under optimum operational conditions satisfy the waste acceptance criteria (WAC) of a disposal facility in Korea (Korea radioactive waste agency, KORAD). Considering economic feasibility and safety, optimum operational conditions were achieved at a w/c ratio of 0.55, and the corresponding salt content was 5.71 wt%. The cement waste form samples prepared under optimum operational conditions were found to satisfy KORAD's WAC when tested for structural stability and leachability. The results indicate that the proposed cementation conditions for the disposal of ILLW from FMMP can be effectively applied to KJRR's disposal facility.

• Journal of the Korean institute of surface engineering
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• v.19 no.1
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• pp.13-19
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• 1986

Manganese in the Anode slime and the paste-positive material of waste-dry cell was recovered by leaching with the hydrochloric acid solution. The impurities (Zn, Fe, Pb), co-leached with manganese were removed from the leached solution prior to electrolysis by hydrometallurgical techniques such as the neutralization with ammonium hydroxide and cementation on manganese powder. The electrodeposition of manganese from the purified chloride solution with sodium selenate was performed. Cathode current efficiency was found to be affected significantly by the concentration of sodium selenate and ammonium chloride salt, bath temperate, current density and PH. The current efficiency of about 88.7% was obtained by electrolysis manganese chloride solution with sodium selenate (0.1/g) at 10$^{\circ}C$.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.27 no.6
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• pp.343-349
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• 2014

It is summarized that potential causes of performance degradations and failure mechanisms of crystalline silicon photovoltaic (PV) modules installed in Middle East area. In addition, we also reviewed current PV module qualification test (IEC 61215) and the methods for detection of wear-out fault. The failure of PV modules in the extreme environmental conditions such as deserts is mainly due to high temperature, humidity, and dust storms. In particular, cementation phenomenon caused by combination of sand and moisture leads to rapid degradation in the performance of PV modules. In order to evaluate and guarantee the long term reliability of PV modules, specific qualification tests such as sand dust test, salt mist test and potential induce degradation test considering operating environment of PV module should be carried out.

• Journal of the Korean Geotechnical Society
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• v.18 no.6
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• pp.83-101
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• 2002

Elastic waves provide an important information about the soil mass in the near-surface. Soil properties in relation to elastic wave parameters are clarified to facilitate the application of geophysical technique to soil characterization. As an example, experiments are performed to gain further insight into the behavior of unsaturated particulate materials using bender elements. The small strain stiffness is continuously measured on specimens subjected to drying, and changes in stiffness are related to changes in interparticle forces such as capillarity, bonding due to ion sharing, buttress effect due to fine migration, and cementation due to salt precipitation. The rate of menisci regeneration is studied after a perturbation as well. Finally, several phenomena associated with the evolution of capillary forces during drying are identified.

• Journal of the Korean institute of surface engineering
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• v.32 no.1
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• pp.67-77
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• 1999

The Ni base superalloy Mar-M247 substrate was aluminized or aluminized after boronizing by the pack cementation under Ar atmosphere. The hot corrosion resistance and after-heat-treatment effect of aluminized specimens were studied by the cyclic hot corrosion test in $Na_2SO_4$-NaCl molten salt. XRD analysis showed that the $Ni_2Al_3$ phase was formed between the coated layer and substrate below 1273K but the NiAl phase above 1273K. The peak of the NiAl phase was developed after heat treatment. Corrosion test showed that corrosion resistance of the specimen with the NiAl phase was better than that with the $Ni_2Al_3$ phase. Corrosion resistance could be improved by heat treatment to form ductile NiAl phase, where cracks were not formed by thermal shock on coating layer. Moreover, it appeared that heat treatment played a role to improve corrosion resistance of Al diffusion coating above 1273K. The existence of boron in the Al diffusion coating layer obstructed outwared diffusion of Cr from the substrate, and it influenced on corrosion resistance of the coating layer by weakening adherence of the oxide scale.