• Title/Summary/Keyword: SURFACE MORPHOLOGY

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Morphology and Characteristic change of $LiMn_2O_4$ Powder Prepared by Precipitation-Evaporation Method (침전-증발법에 의해 제조된 $LiMn_2O_4$ 분말의 특성과 형태 변화)

  • Kim, Guk-Tae;Shim, Young-Jae
    • Korean Journal of Crystallography
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    • v.15 no.1
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    • pp.44-50
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    • 2004
  • Spinel structured lithium managanese oxide $(LiMn_2O_4)$ powder with well defined facetted morphology was prepared by precipitation-evaporation method. {111}, {110}, and {100} planes are mainly observed in the $LiMn_2O_4$ powder. And powder shape of tetradecahedron and octahedron was observed depending on the calcinations temperature. The observed powder morphology observed seemed to be related to the nonstoichiometry of the oxygen in the $LiMn_2O_4$ spinel structure. Oxygen nonstoichiometry might be responsible for the Jahn-teller effect and structure transition which in turn affects the surface energy of the {111}, {110}, and {100} planes. Powder shape transition from tetradecahedron to octahedron seemed to be related to the surface energy of the {111}, {110}, and {100} planes with oxygen nonstoichiometry.

Inspection and Subpixel Alignment of SMD's U sing Fuzzy Morphology (훠지형태학을 이용한 SMD의 검색 및 부화소단위 정렬)

  • 정홍규;박래홍
    • Journal of the Korean Institute of Telematics and Electronics B
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    • v.31B no.9
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    • pp.112-123
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    • 1994
  • In this paper, inspection and subpixed alignment algorithms of SMD's (Surface Mounting Devices) using fuzzy morphology are proposed. First, camera calibration is performed and then the inspection algorithm detects defects such as lead bending and breaking using the ruler generated by fuzy morphology. The SMD having no defects is tested whether it is mounted in the specified position or not. The proposed subpixel alignment algorithm detects accurately orientation and position using subpixel interpolation. It consists of two parts: preprocessing and main processing steps, in which corner points and coarse orientation of a SMD are detected, and interpolation is used to obtain final parameters with wubpixel accuracy. The computer simulation shows that the proposed algorithms give more accurate parameters, and they can be applied to fast and accurate automatic surface mounting systems.

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Effect of Collector Temperature on the Porous Structure of Electrospun Fibers

  • Kim Chi Hun;Jung Yoon Ho;Kim Hak Yong;Lee Douk Rae;Dharmaraj Nallasamy;Choi Kyung Eun
    • Macromolecular Research
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    • v.14 no.1
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    • pp.59-65
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    • 2006
  • We report a new approach to fabricate electrospun polymer nonwoven mats with porous surface morphology by varying the collector temperature during electrospinning. Polymers such as poly(L-lactide) (PLLA), polystyrene (PS), and poly(vinyl acetate) (PVAc) were dissolved in volatile solvents, namely methylene chloride (Me) and tetrahydrofuran (THF), and subjected to electrospinning. The temperature of the collector in the electrospinning device was varied by a heating system. The resulting nonwoven mats were characterized by using scanning electron microscopy (SEM), field emission SEM (FESEM), and atomic force microscopy (AFM). We observed that the surface morphology, porous structure, and the properties such as pore size, depth, shape, and distribution of the nonwoven mats were greatly influenced by the collector temperature.

Nanoscopic Morphological Changes in Yeast Cell Surfaces Caused by Oxidative Stress: An Atomic Force Microscopic Study

  • Canetta, Elisabetta;Walker, Graeme M.;Adya, Ashok K.
    • Journal of Microbiology and Biotechnology
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    • v.19 no.6
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    • pp.547-555
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    • 2009
  • Nanoscopic changes in the cell surface morphology of the yeasts Saccharomyces cerevisiae (strain NCYC 1681) and Schizosaccharomyces pombe (strain DVPB 1354), due to their exposure to varying concentrations of hydrogen peroxide (oxidative stress), were investigated using an atomic force microscope (AFM). Increasing hydrogen peroxide concentration led to a decrease in cell viabilities and mean cell volumes, and an increase in the surface roughness of the yeasts. In addition, AFM studies revealed that oxidative stress caused cell compression in both S. cerevisiae and Schiz. pombe cells and an increase in the number of aged yeasts. These results confirmed the importance and usefulness of AFM in investigating the morphology of stressed microbial cells at the nanoscale. The results also provided novel information on the relative oxidative stress tolerance of S. cerevisiae and Schizo pombe.

Morphology Observation of Nanostructured Ti-25Ta-xZr Alloys

  • Kim, Hyun-ju;Ko, Yeong-Mu;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2012.05a
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    • pp.331-331
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    • 2012
  • In this study, we investigated morphology observation of nanostructured Ti-25Ta-xZr alloys. Ti-25Ta-(3wt%~15 wt%) Zr alloys were prepared by a vacuum arc-melting furnace. Formation of nanotubular structure was achieved by an electrochemical method in 1M $H_3PO_4$ electrolytes containing 0.8%wt.% NaF. Nanotube morphology depended on alloying elements.

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Improved light extraction efficiency of vertical AlGaInP-based LEDs by n-AlGaInP surface roughening (n-표면 거칠기가 형성된 AlGaInP 수직형 적색 발광다이오드의 광추출효율 증가)

  • Seo, Jae-Won;Oh, Hwa-Sub;Song, Hyun-Don;Park, Kyung-Wook;Ryu, Seong-Wook;Park, Yung-Ho;Park, Hae-Sung;Kwak, Joon-Seop
    • Journal of the Korean Vacuum Society
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    • v.17 no.4
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    • pp.353-358
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    • 2008
  • In order to increase extraction efficiency of AlGaInP-based vertical RED LEDs, chemical wet etching technique was produced by using a roughened surface with triangle-like morphology. A commonly used $H_3PO_4$-based solution was applied for chemical wet etching. The light extraction of AlGaInP LED was related to the n-side roughed surface morphology. The morphology of roughed surface is analyzed by the atomic force microscope (AFM). As a result, the roughed surface AlGaInP LED has a root-mean-square (RMS) roughness of 44 nm. The brightness shows 41% increase after roughening n-side surface, as compared to the ordinary flat surface LED.

Preparation and Surface Properties of Polysulfone/Organophilic Layered Silicate Nanocomposites (폴리설폰/친유기화 층상실리케이트 나노복합체의 제조 및 표면 특성)

  • Sul, Kyung-Il;Ma, Seung Lac;Kim, Yong Seok;Lee, Jae Heung;Won, Jong Chan
    • Journal of Adhesion and Interface
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    • v.4 no.4
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    • pp.15-21
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    • 2003
  • Polysulfone/organophilic layered silicate nanocomposites were prepared in the range of 0.25 to 9 wt% of organophilic-layered silicate by solution blend. Nano-hybridized films were cast from the blend solution. Exfoliation and intercalation of the polysulfone/organophiliclayered silicate nanocomposite films were confirmed by an X-ray diffractometer and a transmission electron microscope. Surface morphologies of polysulfone/organophilic layered silicate nanocomposite films were determined by a scanning electronic microscope and an atomic force microscope. When the organophilic layered silicate was added more than 1.5 wt%, the surface roughness (RMS) was rapidly increased because clusters of intercalated organophilic layered silicate particles existed on the polysulfone/organophilic-layered silicate film surface. Surface tension revealed an upward tendency over the contents of 1.5 wt% organophilic layered silicate in polysulfone/organophilic layered silicate nanocomposite. The change of surface morphology in polysulfone/organophilic layered silicate nanocomposite were affected by nano scale dispersed and intercalated organophilic layered silicate particles.

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Pollen Morphology of Genus Sedum in Korea

  • Kim, Jeong-Hee
    • Journal of Plant Biology
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    • v.37 no.2
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    • pp.245-252
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    • 1994
  • Pollens of 20 species of Sedum were investigated with a scanning electron microscope. The pollen morphology of Sedum was rather variable, within particular species or even within a single inflorescence. Differences occurred in the number and shape of apertures and surface sculpture. Besides 3-colporate, various aperture types including 2-syncolporate, 3-syncolporate, 40stephanocolporate, 5-stephanocolporate, zonate, and irregular types were found in a single specimen. Also, striate-rugulose and psilate sculpture were found in S. viviparum. No correlation was found between the pollen morphology and the floral formula. Pollen characters appeared to be not useful for infrageneric classification of Korean Sedum.

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Investigations on Relationship between Fractal Dimension and 3-D Surfaces Topography of C.G. Irons under Dry Sliding

  • Yongzhen, Zhang;Gesen, Sun;Lemin, Sun;Weimin, Liu;Bao, Shangguan;Yue, Chen
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.253-254
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    • 2002
  • Based on 3-D surface morphology measurements of C.G. irons, the fractal analyses were made on relationship between dry sliding surface morphology and the fractal dimension. It is revealed that the values of fractal dimensions ($D_f$) of sliding surfaces are in the range between 1-2, which are closely related to the surface morphologies. With the increase in depths of grooves or pits, the $D_f$ values increase. At the same time, the increases in densities of the grooves also cause the $D_f$ values to increase. At last, relationship among $D_f$ and friction coefficient as well as wear rate is discussed.

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Preparation of cross-linked silk fibroin film by γ-irradiation and their application as supports for human cell culture

  • Park, Hyean-Yeol;Kim, Yoon-Seob;Choi, Seong-Ho
    • Analytical Science and Technology
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    • v.27 no.1
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    • pp.27-33
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    • 2014
  • This study described about preparation of the cross-linked silk fibroin (SF) film by ${\gamma}$-irradiation of the casted SF film, which is fabricated from aqueous solution regenerated via fibers of cocoons and their application as supports for human cell culture. The properties of cross-linked SF film were evaluated by FT-IR spectroscopy, contact angle, solubility to water, thermal analysis, surface area analyzer, and morphology via scanning electron microscopy (SEM). The cross-linked SF films were not dissolved in water and exhibited the rough surface morphology, large surface area, and good thermal properties. The human fibroblast cell (CCD-986sk) and embryo kidney-ft cell were well growed on the surface of cross-linked SF film supports prepared by ${\gamma}$-irradiation. The cross-linked SF film prepared by ${\gamma}$-irradiation can be used as biomaterials for human cell culture.