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Nondestructive determination of physico-chemical properties in compost by NIRS

  • Seo, Sang-Hyun;Lee, Chang-Hee;Park, Sung-Hun;Cho, Rae-Kwang;Park, Woo-Churl
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1622-1622
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    • 2001
  • The purpose of this research was to develop a the reflection technique with near infrared (NIR) radiation for estimating physico-chemical properties in compost. The composts (cattle, pig, chicken and waste composts) were air dried and then ground to pass through a 0.5 or 2mm sieve for the physico-chemical properties and spectroscopic determinations. The physico-chemical properties of compost were shown high values ; moisture(30-60%), T-N(0.8-2.9%), organic matter(29-89%), pH(5.89-9.60) K$_2$O(0.27-5.66%), P2O$\sub$5/(0.07-2.62%), CaO(0.03-4.80%), MgO(0.09-1.56%), NaCl(0.01-1.13%), EC(1.41-13.76dS/m). Generally, we should select a simple calibration and prediction method for determining physico-chemical properties in compost under similar accuracy and precision of prediction. It should be remembered that the NIRS approach will never replace the traditional methods. However, NIRS technique may be an effective method for rapid and nondestructive measurements of a large number of compost samples. Near infrared reflectance spectra of composts was obtained by Infra Alyzer 500 scanning spectrophotometer at 2-nm intervals from 1100 to 2500nm. Multiple linear regression(MLR) or partial least square regression (PLSR) was used to evaluate a NIRS method for the rapid and nondestructive determination of physico-chemical properties and humic acid contents in composts. The standard error of prediction(SEP) for finely sized sample(<0.5mm) and coarsely sized sample(<2mm) did not show much difference. The NIR instrument of filter type showed the same accuracy of the monochromator scanning type to estimate the compost properties. The results summarized that NIR spectroscopy can be used as a routine testing method to determine quantitatively the OM, moisture, T-N, color, pH, cation content in the compost samples nondestructively.

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Effect of Kumquat on N-nitrosodimethylamine Formation (금귤이 N-nitrosodimethylamine의 생성에 미치는 영향)

  • 이수정;신정혜;성낙주
    • Journal of Food Hygiene and Safety
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    • v.17 no.4
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    • pp.201-205
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    • 2002
  • When it added to each designed diet groups such as control, nitrate rich, amine rich and nitrate-amine rich diet under simulated gastric conditions, effect of kumquat (Fortunella mararita) juice on formation of N-nitrosodimethylamine (NDMA) was studied. Inhibition on NDMA formation was the highest in the amine rich diet, as 69.4 $\pm$2.4%, when the juice of 10m1 added to its digestate. Phenolic portion of $C_{18}$ sep-pak cartridge in kumquat juice were separated into 20 kinds of a phenolic compounds using HPLC. These phenolic fractions such as faction no. 1, 2, 3, 4 and 5 inhibited from 3.0 $\pm$ 1.2% to 66.5 $\pm$2.0% NDMA formation in the reaction system which was mixture of nitrite and dimethylamine.

Detection of Foodborne Pathogens and Analysis of Aflatoxin Levels in Home-made Doenjang Samples

  • Kim, Myung-Hee;Kim, Yo-Sep
    • Preventive Nutrition and Food Science
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    • v.17 no.2
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    • pp.172-176
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    • 2012
  • Doenjang is a traditional Korean fermented soybean product that provides a major source of protein. In this study, a total of 18 different home-made doenjang samples were examined for the presence of foodborne pathogens and the total aflatoxin levels. Using an enzyme-linked immunosorbent assay to assess microbial quality and potential public health risk, we showed that total coliform levels in the doenjang samples ranged from 0 to $4.43{\pm}2.32{\times}10^6\;CFU/g$, and the maximum limit of Bacillus cereus was $4.67{\pm}2.0{\times}10^5\;CFU/g$. However, other foodborne pathogens, such as Staphylococcus aureus, Escherichia coli O157:H7 and Salmonella spp., were not detected among the tested samples. One of the samples (S3) showed a maximum limit of $42.2{\pm}9.1\;{\mu}g/kg$ for aflatoxin levels, which was above the safety limit allowed by the Codex Alimentarius Commission (CAC) regulatory agency. Further research is necessary to determine whether and how doenjang safety can be improved via elimination/reduction of microbial contamination during fermentation and storage or using microbial starter cultures for its fermentation.

Study on Prediction of Internal Quality of Cherry Tomato using Vis/NIR Spectroscopy (가시광 및 근적외선 분광기법을 이용한 방울토마토의 내부품질 예측에 관한 연구)

  • Kim, Dae-Yong;Cho, Byoung-Kwan;Mo, Chang-Yeun;Kim, Young-Sik
    • Journal of Biosystems Engineering
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    • v.35 no.6
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    • pp.450-457
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    • 2010
  • Although cherry tomato is one of major vegetables consumed in fresh vegetable market, the quality grading method is mostly dependant on size measurement using drum shape sorting machines. Using Visible/Near-infrared spectroscopy, apparatus to be able to acquire transmittance spectrum data was made and used to estimate firmness, sugar content, and acidity of cherry tomatoes grown at hydroponic and soil culture. Partial least square (PLS) models were performed to predict firmness, sugar content, and acidity for the acquired transmittance spectra. To enhance accuracy of the PLS models, several preprocessing methods were carried out, such as normalization, multiplicative scatter correction (MSC), standard normal variate (SNV), and derivatives, etc. The coefficient of determination ($R^2_p$) and standard error of prediction (SEP) for the prediction of firmness, sugar, and acidity of cherry tomatoes from green to red ripening stages were 0.859 and 1.899 kgf, with a preprocessing of normalization, 0.790 and $0.434^{\circ}Brix$ with a preprocessing of the 1st derivative of Savitzky Golay, and 0.518 and 0.229% with a preprocessing normalization, respectively.

Effects of Planting Date and Density on Yield and It’s Components of Fritillaria thungergii MIQUEL (패모(貝母)의 파종기(播種期) 및 재식밀도(栽植密度)가 수양구성(收量構成) 형질(形質) 및 수양(收量)에 미치는 영향(影響))

  • Choi, In-Sik;Cho, Jin-Tae;Son, Seok-Yong;Park, Jae-Seong;Han, Dong-Ho;Jeong, In-Myeong
    • Korean Journal of Medicinal Crop Science
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    • v.4 no.3
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    • pp.218-223
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    • 1996
  • This experiment was carried out to investigate the effect of planting date and planting density on yield and yield components of Fritillariae bulbus from 1989 to 1991. The Chungbuk local variety was used, and the experimental materials were planted six times with 10 days interval from Aug. 20 to Oct. 10. 33, 22, 17 and 13 bulbs were planted by the square meter, respectively. The compound fertilizer for garlic $(N\;-\;P_2O\;-\;K_2O_5=9\;-\;14\;-\;10)$ was applied by 80kgs to the 0.1ha before planting. The experimental design was randomized block design with 3 replications. As the planting dates were earlier, the emerging dates were earlier, too. But the delay of 50 days in the planting affected to the delay of 14 days in the em­erging dates. The plant height was 22.7cms in the Aug. 20 plot. As the planting were later, the plant heights were shorter by $2.4{\sim}5.6cms$ than that. As compared with the 829kgs by the 0.1ha of Aug. 30 plot, the others recorded 1 percent increase in the Aug. 20 plot, 4 percent decrease in the Sep. 10 plot, 26 percent decrease in the Sep. 20 plot, 35 percent decrease in the Sep 30 plot, and 38 percent decrease in the Oct. 10 plot. So, the suitable planting dates were from Aug. 20 to Aug. 30.The emerging date of 33 bulb plot by the square meter was March 7, but as the planting densities were sparse, the emerging dates delayed by one to three days. The plant height of the 33 bulb plot by the square meter was 21. 8cms, but the other plots were short by $0.7{\sim}1.8cms$. The number of shoots of the 33 bulb plot by the square meter was 6.1. but the other plots recorded 0.4 increase in the 22 bulb plot, 0.6 increase in the 17 bulb plot and 0.5 increase in the 13 bulb plot compared with that of the 33 bulb plot. Accordingly, the number of shoots in the sparse planting plot was more than that in the dense planting plot. As compared with the 854kgs by the 0.1ha of the 22 bulb plot, the other plots recored 2 percent in­crease in the 33 bulb plot, 16 percent decrease in the 17 bulb plot and 34 percent decrease in the 13 bulb plot. All things considered, for the culture of Fritillaria thungergii MIQUEL in the middle region, Aug. 25 and 22 bulbs by the square meter were suitable for the planting date and density.

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A study on the determination of residual Antibiotics and Synthetic Antibacterial Agents in Meat(III) Simultaneous Gas Chromatography/Mass Spectrometry Analysis of Erythromycin and Tylosin (식육중의 잔류 항생.항균제의 검정에 관한 연구(III) Macrolide계 항생물질인 Erythromycin과 Tylosin의 Gas Chromatography/Mass Spectrometry 동시분석)

  • 류재천;송윤선;양종순;서지원;김명수;박종세
    • Journal of Food Hygiene and Safety
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    • v.8 no.1
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    • pp.17-23
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    • 1993
  • In an attempt to quantitate and qualitate residual antibiotics and antibacterial agents n meat simultaneously, we studied a gas chromatogrphy-mass spectrometry (GC/MS) analysis. For a simultaneous analysis of macrolide antibiotics such as erythromycin and tylosin in meat, the homogenization with MeOH, defatting with n-hexane, extraction with CHCl3, elution with CHCl3 : MeOH=2:1 from Sep-Pak silica cartridge, acid gydrolysis, back extraction with CHCl3, and quantitation by selected ion monitoring(SIM) mode after trimethylsilyl derivatization were performed. The recoveries of erythromycin and tylosin (CV,%) at 10 ppm fortification level were 90.59(4.89) and 45.91(0.20) , and the detection limits of those were 0.02 and 2.0 $\mu\textrm{g}$/g beef, respectively. From these results, the developed analytical method using GC/MS-SIM mode allows excellent detection and quantitation of residual macrolide antibiotics in meats, using complementary method with bio-assay.

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Development of Near-Infrared Reflectance Spectroscopy (NIRS) Model for Amylose and Crude Protein Contents Analysis in Rice Germplasm (근적외선 분광광도계를 이용한 벼 유전자원 아밀로스 및 단백질 함량분석을 위한 모델개발)

  • Oh, Sejong;Lee, Myung Chul;Choi, Yu Mi;Lee, Sukyeung;Oh, Myeongwon;Ali, Asjad;Chae, Byungsoo;Hyun, Do Yoon
    • Korean Journal of Plant Resources
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    • v.30 no.1
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    • pp.38-49
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    • 2017
  • The objective of this research was to develop Near-Infrared Reflectance Spectroscopy (NIRS) model for amylose and protein contents analysis of large accessions of rice germplasm. A total of 511 accessions of rice germplasm were obtained from National Agrobiodiversity Center to make calibration equation. The accessions were measured by NIRS for both brown and milled brown rice which was additionally assayed by iodine and Kjeldahl method for amylose and crude protein contents. The range of amylose and protein content in milled brown rice were 6.15-32.25% and 4.72-14.81%, respectively. The correlation coefficient ($R^2$), standard error of calibration (SEC) and slope of brown rice were 0.906, 1.741, 0.995 in amylose and 0.941, 0.276, 1.011 in protein, respectively, whereas $R^2$, SEC and slope of milled brown rice values were 0.956, 1.159, 1.001 in amylose and 0.982, 0.164, 1.003 in protein, respectively. Validation results of this NIRS equation showed a high coefficient determination in prediction for amylose (0.962) and protein (0.986), and also low standard error in prediction (SEP) for amylose (2.349) and protein (0.415). These results suggest that NIRS equation model should be practically applied for determination of amylose and crude protein contents in large accessions of rice germplasm.

Open heart surgery in the first two years of life (2 세 이하 유아기의 개심술)

  • 성숙환
    • Journal of Chest Surgery
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    • v.15 no.4
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    • pp.373-380
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    • 1982
  • Experience with intracardiac surgery in infants indicates that for most anomalies the operation and late mortality after primary total correction is lower than the combined mortality after early palliation and delayed correction. In addition, there are secondary benefits of primary total correction in terms of reversal of retarded physical growth and social development and alleviation of parental anxiety. One hundred and fifteen infants under 2 years of age with congenital cardiac anomalies underwent primary surgical intervention at Seoul National University Hospital from Jan. `78 to Sep. `82. There were 70 patients with VSD, 17 patients with TOF, 10 patients with TGA, 4 patients with ASD, 4 patients with TA, 3 patients with TAPVR, and the remainders are Coronary AV Fistula, partial ECD+COA, SV, DORV, PA, Trilogy+PDA. The overall surgical mortality was 18.3%. In acyanotic group 6 patients died among 76 operated patients, and surgical mortality was 6.6%. But in cyanotic group, the mortality was very high as41.0% [16 patients among 39 patients]. This poor surgical result in cyanotic group was due to Improper pre-, intra- and post-operative care, and we are convincing that these factors soon be improved as experiences accumulated.

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Effects of Fertilizer Levels on Dry Matter Yield and Nutritional Quality of Forage Rye

  • Kwon, Byung-Sun
    • Plant Resources
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    • v.7 no.3
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    • pp.181-186
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    • 2004
  • To find out the optimum fertilizer level for high yielding variety, Paldanghomil, experiment was conducted with 15 compositions of fertilizer levels at the experiment field of forage rye in Sunchon National University from Sep. 1998 to Aug. 1999. The effects of nitrogen fertilizer on plant growth were large significant but increasing rate of application in potassium and phosphate fertilizers above 10kg/10a had negligible effects on plant growth. Raising nitrogen application rate of fertilizers turned out to be 18-10-10kg/l0a of N-P$_2$O$_{5}$-K$_2$O. Content of crude protein was the highest and that of crude fiber such as NDF, ADF, cellulose and lignin were lowest at this rate. Furthermore, IVDMD was high and dry matter yield were the highest at the optimum rate.e.

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Turnover intention and Its Influencing factors among care workers (요양보호사의 이직의도 및 영향요인)

  • Sung, kyoung-Ja
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.5
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    • pp.285-293
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    • 2017
  • This study examined the causal relationship among job stress, fatigue, and job satisfaction, which affect the turnover intention of elderly nursing home care workers. Data were collected from Sep.15 to Sep. 30, 2014. Structured self-administered questionnaires were delivered and collected without the respondents' personal information. The subjects were 232 female care workers working in nursing homes in D city. The data were analyzed using the SPSSWIN 21.0 and AMOS 21.0 programs. Covariance structure analysis was performed to estimate the causal relationship between the variables affecting the turnover intention of care workers. The results of the analysis were as follows. The variables included in this study were fatigue, which comprised 4.9% of job stress. Job satisfaction explained 54.6% of job stress and fatigue. The turnover intention was 46.2% due to job stress, fatigue, and job satisfaction. In other words, job stress, fatigue, and job satisfaction had a direct or indirect effect on the turnover intention of care workers. In conclusion, job stress, fatigue, and job satisfaction affect the turnover intention. Therefore, a policy to improve the work environment and working conditions is needed to reduce the turnover intention of care workers, and fulfill their duties in a stable life time workplace.