• Title/Summary/Keyword: SEM morphology

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Relationship between the maxillofacial skeletal pattern and the morphology of the mandibular symphysis: Structural equation modeling

  • Ahn, Mi So;Shin, Sang Min;Yamaguchi, Tetsutaro;Maki, Koutaro;Wu, Te-Ju;Ko, Ching-Chang;Kim, Yong-Il
    • The korean journal of orthodontics
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    • v.49 no.3
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    • pp.170-180
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    • 2019
  • Objective: The purpose of this study was to investigate the relationship between the facial skeletal patterns and the shape of the mandibular symphysis in adults with malocclusion by using a structural equation model (SEM). Methods: Ninety adults who had malocclusion and had records of facial skeletal measurements performed using cone-beam computed tomography were selected for this study. The skeletal measurements were classified into three groups (vertical, anteroposterior, and transverse). Cross-sectional images of the mandibular symphysis were analyzed using generalized Procrustes and principal component (PC) analyses. A SEM was constructed after the factors were extracted via factor analysis. Results: Two factors were extracted from the transverse, vertical, and anteroposterior skeletal measurements. Latent variables were extracted for each factor. PC1, PC2, and PC3 were selected to analyze the variations of the mandibular symphyseal shape. The SEM was constructed using the skeletal variables, PCs, and latent variables. The SEM showed that the vertical latent variable exerted the most influence on the mandibular symphyseal shape. Conclusions: The relationship between the skeletal pattern and the mandibular symphysis was analyzed using a SEM, which showed that the vertical facial skeletal pattern had the highest effect on the shape of the mandibular symphysis.

Formation Mechanism and Corrosion-Resistance of Magnesium Film by Physical Vapour Deposition Process (물리증착법에 의해 제작한 마그네슘 박막의 형성기구와 내식특성)

  • 이명훈
    • Journal of Advanced Marine Engineering and Technology
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    • v.18 no.2
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    • pp.54-63
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    • 1994
  • Mg thin films were prepared on SPCC(cold-rolled steel) substrates by vasuum evapoaration and ion-plating. The influence of argon gas pressure and substrates bias voltage on the crystal orientation and morphology of the film was determined by using X-ray diffraction and scanning electron micrography (SEM), respectively. And the effect of crystal orientation and morphology of the Mg thin films on corrosion behavior was estimated by measuring the anodic polarization curves in deaerated 3% NaCl solution. The crystal orientation of the Mg films deposited at high argon gas pressure exhibited a (002) preferred orientation, regardless of the substrate bias voltage. Film morphology changed from a columnar to a granular structure with the increase of argon gas pressure. The morphology of the films depended not only on argon gas pressure but also bias voltage ; i.e., the effect of increasing bias voltage was similar to that of decreasing argon gas pressure. The influences of argon gas pressure and bias voltage were explained by applying the adsorption inhibitor theory and the sputter theory. And also, this showed that the corrosion resistance of the Mg thin films can be changed by controlling the crystal orientaton and morphology.

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Morphology Effect on Electrocatalytic Activity of TiO2 Spheres Synthesized by Binary Ionic Liquids in Water Electrolysis

  • Hong, Ki-Won;Pak, Dae-Won;Yoo, Kye-Sang
    • Bulletin of the Korean Chemical Society
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    • v.33 no.6
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    • pp.1829-1833
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    • 2012
  • Titania spheres were synthesized using binary ionic liquids to examine the electrocatalytic activity in acid solution. The morphology of $TiO_2$ particles was significantly different with the composition of ionic liquids. Among the binary ionic liquids, four set of mixtures led to the formation of $TiO_2$ sphere with various sizes. The morphology and structure of $TiO_2$ particles were characterized by XRD, $N_2$ physisoption and SEM analysis. All samples possessed an anatase phase after calcinations at $500^{\circ}C$. The structural properties of the samples were varied significantly with the morphology. In cyclic voltammograms, the morphology of $TiO_2$ spheres affected the electrocatalytic activity in water electrolysis. Among the samples, [Omim][$BF_4$]+[Hmim][$BF_4$] was the most effective ionic liquid to synthesize $TiO_2$ sphere with optimum morphology showing the highest electocatalytic performance.

Morphology and Chemical Composition Analysis of Individual Particles at Large Anthropogenic Emissions by SEM-EDS (인위적 대형 배출원에서 SEM-EDS법을 이용한 개별 입자상 물질의 형태와 화학적 조성 분석)

  • 양수명;박정호;정재우;서정민;최금찬
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2003.11a
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    • pp.368-369
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    • 2003
  • 각종 배출원에서 배출된 입자상 물질은 대기 중 확산, 이동, 침착 등을 통해 국지적 도시오염 뿐만 아니라 장거리까지도 이동함으로서 광역적 대기오염의 원인이 되고 있는 등 입자상 물질의 발생원 추적에 관한 연구가 필요한 실정이다. 지금까지 입자상 물질의 발생원 추적은 대부분 배출원의 발생량 조사나 필터에 포집된 시료의 전체적인 화학적 분석의 개념으로 단시간의 시간변동과 개개의 입자가 가지는 정보가 무시되고 평균화되고 있다. (중략)

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Methanol fixation for scanning electron microscopy of plants

  • Ki Woo Kim
    • Applied Microscopy
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    • v.50
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    • pp.10.1-10.6
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    • 2020
  • Plant specimens for scanning electron microscopy (SEM) are commonly treated using standard protocols. Conventional fixatives consist of toxic chemicals such as glutaraldehyde, paraformaldehyde, and osmium tetroxide. In 1996, methanol fixation was reported as a rapid alternative to the standard protocols. If specimens are immersed in methanol for 30 s or longer and critical-point dried, they appear to be comparable in preservation quality to those treated with the chemical fixatives. A modified version that consists of methanol fixation and ethanol dehydration was effective at preserving the tissue morphology and dimensions. These solvent-based fixation and dehydration protocols are regarded as rapid and simple alternatives to standard protocols for SEM of plants.

The Effects of Electrode Distance on the Formation of $(ZnS)_{1-x}(SiO_2)_x$ Protective Films in Phase Change Optical Disk by R.F. Sputtering Method (R.F. Sputtering 방법에 의한 상변화형 광디스크의 $(ZnS)_{1-x}(SiO_2)_x$ 보호막 형성에 미치는 전극거리의 영향)

  • Lee, Jun-Ho;Kim, Do-Hun
    • Korean Journal of Materials Research
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    • v.9 no.12
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    • pp.1245-1251
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    • 1999
  • Phase-change optical disk very rapid recording, high densification of data, resulting in high feedback rate and good C/N(carrier to noise) ratio of a feedback signal. However, repetitive thermal energy may cause the deformation of a disk or the lowering of an eliminability and a cyclability of the recording. The lowering of the cyclability can be reduced by insertion of thin layer of ZnS-$SiO_2$ dielectric thin film in appropriate disk structure between the upper and lower part of the recording film. Using the Taguchi method, optimum conditions satisfying both the optimized quality characteristic values and the scattering values for film formation were found to be the target R.F. power of 200W, the substrate R.F. power of 20W, the Ar pressure of 6mTorr, and the electrode distance of 6cm. From the refractive index data, the existence of the strong interaction between the electrode distance and Ar pressure was confirmed, and so was the large effect of the electrode distance on transmittance. According to the analysis of TEM and XRD, the closer the electrode distance was, the finer was the grain size due to the high deposition rate. However, the closer electrode distance brought the negative effect on the morphology of the film and caused the reduction of transmittance. AFM and SEM analyses showed that the closer the electrode distance was, the worse was the morphology due to the high rate of the deposition. Under optimum condition, the deposited thin film showed a good morphology and dense microstructure with less defects.

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Characterization of Synthesized Strontianite: Effects of Ionic Strength, Temperature, and Aging Time on Crystal Morphology and Size (온도, 이온세기 및 결정성장시간에 따른 합성 스트론티아나이트(SrCO3) 특성 연구)

  • Lee, Seon Yong;Lee, Choong Hyun;Hur, Hyuck;Seo, Jieun;Lee, Young Jae
    • Journal of the Mineralogical Society of Korea
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    • v.28 no.2
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    • pp.195-207
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    • 2015
  • Physical properties of strontianite ($SrCO_3$) synthesized under variable conditions such as different ionic strength, temperature, and aging time were investigated by X-ray diffraction (XRD) and scanning electron microscopy (SEM). All synthesized samples show a single phase of strontianite. Crystallinity of the synthesized strontianite increases with increasing temperature and ionic strength with $NaNO_3$. Crystal sizes of the samples increase dramatically, and their morphology changes from rod or dendritic to prismatic shape as ionic strength and temperature of the solution increase. In addition, crystal sizes increase, and their morphology changes from rod or prismatic crystals to spheroidal aggregates with increasing aging time. These results suggest that changes in conditions of the synthesis for strontianite play an important role in controlling the crystallinity and morphology of results provide crucial information on the prediction for the physical properties of strontianite under different conditions during the formation of strontianite crystals.

Evaluation of Morphology and Water Flux for Polysulfone Flat Sheet Membrane with Conditions of Coagulation Bath and Dope Solution (응고조와 도프조성에 따른 폴리술폰 평막의 모폴로지 및 수투과도 평가)

  • Woo, Seung Moon;Chung, Youn Suk;Nam, Sang Yong
    • Membrane Journal
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    • v.22 no.4
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    • pp.258-264
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    • 2012
  • In this study, to research effect of coagulation bath and composition of dope solution, polysulfone flat sheet membrane was fabricated by phase inversion method. PEG and PVP were used as additive. Concentration of polymer and additive, composition of coagulation bath was controlled to prepare flat sheet membrane. And then the morphology and water flux of prepared membrane were measured by FE-SEM and water flux testing apparatus. The highest value of water flux was measured at the membrane prepared under a 15 wt% PSF, 25 wt% PEG conditions, and water as coagulation bath. The pure water flux of the membrane composed of PSf/PEG was drastically decreased with increasing amount of DMAc. We confirmed that change of amount in additive and composition in coagulation bath influence the morphology and water flux performance of the membrane.

Morphology and Molecular Phylogeny of Raillietina spp. (Cestoda: Cyclophyllidea: Davaineidae) from Domestic Chickens in Thailand

  • Butboonchoo, Preeyaporn;Wongsawad, Chalobol;Rojanapaibul, Amnat;Chai, Jong-Yil
    • Parasites, Hosts and Diseases
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    • v.54 no.6
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    • pp.777-786
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    • 2016
  • Raillietina species are prevalent in domestic chickens (Gallus gallus domesticus) in Phayao province, northern Thailand. Their infection may cause disease and death, which affects the public health and economic situation in chicken farms. The identification of Raillietina has been based on morphology and molecular analysis. In this study, morphological observations using light (LM) and scanning electron microscopies (SEM) coupled with molecular analysis of the internal transcribed spacer 2 (ITS2) region and the nicotinamide adenine dinucleotide dehydrogenase subunit 1 (ND1) gene were employed for precise identification and phylogenetic relationship studies of Raillietina spp. Four Raillietina species, including R. echinobothrida, R. tetragona, R. cesticillus, and Raillietina sp., were recovered in domestic chickens from 4 districts in Phayao province, Thailand. LM and SEM observations revealed differences in the morphology of the scolex, position of the genital pore, number of eggs per egg capsule, and rostellar opening surface structures in all 4 species. Phylogenetic relationships were found among the phylogenetic trees obtained by the maximum likelihood and distance-based neighbor-joining methods. ITS2 and ND1 sequence data recorded from Raillietina sp. appeared to be monophyletic. The query sequences of R. echinobothrida, R. tetragona, R. cesticillus, and Raillietina sp. were separated according to the different morphological characters. This study confirmed that morphological studies combined with molecular analyses can differentiate related species within the genus Raillietina in Thailand.

SEM Images of Naphthalic Amide Derivatives Appearing by the Substituent Effect of Ending Group

  • Phung, Doan Minh;Jeong, Woo-Chul;Choi, Chang-Shik;Lee, Ki-Hwan
    • Rapid Communication in Photoscience
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    • v.1 no.1
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    • pp.11-12
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    • 2012
  • The naphthalic amide derivatives were synthesized by simple condensation and were crystallized by acetonitrile solution. The SEM images of products with methyl group and nitro group, respectively, showed rod shape while the SEM images of products with other groups ($N(CH_3)_2$, $OCH_3$, H, F, and Cl), respectively, showed plate shape. We were known from these results that the substituent of ending group played an important role in the crystallization of single molecule and the morphology of naphthalic derivatives could be controlled by only change of ending group in single molecule.